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55results about How to "Improves antioxidant stability" patented technology

High-quality coconut-oil microencapsulated powder grease and high-efficiency preparation method thereof

The invention discloses high-quality coconut-oil microencapsulated powder grease and a high-efficiency preparation method thereof. The preparation method of the high-quality coconut-oil microencapsulated powder grease comprises the following steps of treating a wall material solution by adopting combination of an ultrasonic device, a heater, a controllable stirring device and a vacuuming device; treating a mixed solution of a wall material and a core material by adopting combination of high-speed shearing and an injector; upper-layer foam in coarse emulsion is removed by connected a reducing hole-type defoaming paddle and a stirrer; and high-pressure homogenization treatment and spray-drying are performed so as to obtain a powder grease product. According to the preparation method of the high-quality coconut-oil microencapsulated powder grease, dissolution rate and sterilization effect of the wall material solution are improved by utilizing high temperature and stirring effects; and the high-speed shearing process and the injection method are combined so as to efficiently remove foam by adopting the ultrasonic device, the vacuuming device and the reducing hole-type defoaming paddle. And thus, the prepared high-quality coconut-oil microencapsulated powder grease is stable and uniform in particle size. The high-quality coconut-oil microencapsulated powder grease prepared by adopting the method has the characteristics of high yield, high encapsulation rate, high storage stability and high anti-oxidation capability; and thus, the high-quality coconut-oil microencapsulated powder grease is suitable for the fields of instant foods, health foods, baked foods and the like.
Owner:文昌东郊阿婆椰子加工专业合作社

POSS (Polyhedral Oligomeric Silsesquioxane) crosslinking type sulfonated polyimide proton exchange membrane as well as preparation method thereof

The invention belongs to the technical field of functional high molecular materials and electrochemistry, and specifically relates to a POSS (Polyhedral Oligomeric Silsesquioxane) crosslinking type sulfonated polyimide proton exchange membrane as well as a preparation method thereof. The preparation method comprises the following steps: firstly, synthesizing a sulfonated polyimide polymer with a crosslinkable group imidazole group on a main chain, wherein the degree of sulfonation is controlled within 10-190%; and preparing a membrane forming liquid, adding a functional POSS crosslinking agent, carrying out reaction with the imidazole group, crosslinking the sulfonated polyimide polymer in a membrane forming process to form the crosslinking type sulfonated polyimide proton exchange membrane. The crosslinking membrane is endowed with good mechanical property and has higher hydrolytic stability and anti-oxidation stability. The method disclosed by the invention is good in controllability of the preparation process. Compared with conventional sulfonated polyimide membranes, the crosslinking type sulfonated polyimide proton exchange membrane is high in mechanical strength, strong in hydrolytic resistance and oxidation resistance, and good in dimensional stability, and has a broad application prospect in polymer electrolyte membrane fuel cells.
Owner:TONGJI UNIV

Preparing method of high saturation magnetization strength Mn0.8Zn0.2Fe2O4 nanoparticles and magnetic liquid of nanoparticles

The invention relates to the field of novel nanometer functional materials, in particular to a preparing method of high saturation magnetization strength Mn0.8Zn0.2Fe2O4 nanoparticles and magnetic liquid of the nanoparticles. The preparing method specifically comprises the steps of dispersing salts of Mn2+, Zn2+ and Fe3+ into ultrapure water and quickly adding a NaOH solution under mechanical stirring; then placing the reaction liquid into a drying oven to be heated at high temperature, promoting the growth of crystal grains and completing the second step of sediment; then taking out the reaction liquid, adding fluorine ether acid, covering particles under mechanical stirring to avoid aggregation of the particles and then washing and drying the particles; finally, grinding the dried particles and dispersing the particles into fluorine ether oil base carrier liquid under mechanical stirring to prepare magnetic liquid. The prepared Mn0.8Zn0.2Fe2O4 nanoparticles have the advantages of high saturation magnetization strength, superparamagnetism, high antioxidant stability and the like, and the prepared fluorine ether oil base magnetic liquid can be applied in the field of rotary shaft sealing under the high temperature, corrosion and oxidation environment for a long term.
Owner:SICHUAN UNIV +1

Sulfonated polyaryletherketone copolymer containing benzothiazole group and preparation method thereof

The invention discloses a sulfonated poly(aryle ether ketone) copolymer containing benzothiazole groups and a preparation method of the sulfonated poly(aryle ether ketone) copolymer. The copolymer is prepared through steps as follows: bisphenol monomers, 2,6-dichlorobenzothiazole, 4,4'-difluorobenzophenone and 3,3'-disulfonic acid sodium salt-4,4'-difluorobenzophenone are taken as raw materials, a salt-forming agent and a water-carrying agent are added after the raw materials are dissolved and mixed by a solvent, solid content of a reaction system is adjusted to be 15%-30%, the reaction system carries water for 3-6 h at the temperature of 120-140 DEG C, and reacts for 6-20 h at the temperature of 140-200 DEG C after the water-carrying agent is steamed out, a mixture is discharged to acetone or distilled water after the reaction is finished, a coarse product is obtained and washed, and the sulfonated poly(aryle ether ketone) copolymer containing the benzothiazole groups is obtained. An electrolyte membrane prepared from the copolymer has better dimensional stability, lower methanol permeability, higher antioxidative stability and good proton conduction performance, and compared with a traditional aromatic polyelectrolyte membrane, the electrolyte membrane prepared from the copolymer is a novel proton exchange membrane material with excellent performance and has good application prospect in the field of the electrolyte membrane of a fuel cell.
Owner:INST OF CHEM MATERIAL CHINA ACADEMY OF ENG PHYSICS

Sulfonated poly(aryle ether ketone) copolymer containing benzothiazole groups and preparation method of sulfonated poly(aryle ether ketone) copolymer

The invention discloses a sulfonated poly(aryle ether ketone) copolymer containing benzothiazole groups and a preparation method of the sulfonated poly(aryle ether ketone) copolymer. The copolymer is prepared through steps as follows: bisphenol monomers, 2,6-dichlorobenzothiazole, 4,4'-difluorobenzophenone and 3,3'-disulfonic acid sodium salt-4,4'-difluorobenzophenone are taken as raw materials, a salt-forming agent and a water-carrying agent are added after the raw materials are dissolved and mixed by a solvent, solid content of a reaction system is adjusted to be 15%-30%, the reaction system carries water for 3-6 h at the temperature of 120-140 DEG C, and reacts for 6-20 h at the temperature of 140-200 DEG C after the water-carrying agent is steamed out, a mixture is discharged to acetone or distilled water after the reaction is finished, a coarse product is obtained and washed, and the sulfonated poly(aryle ether ketone) copolymer containing the benzothiazole groups is obtained. An electrolyte membrane prepared from the copolymer has better dimensional stability, lower methanol permeability, higher antioxidative stability and good proton conduction performance, and compared with a traditional aromatic polyelectrolyte membrane, the electrolyte membrane prepared from the copolymer is a novel proton exchange membrane material with excellent performance and has good application prospect in the field of the electrolyte membrane of a fuel cell.
Owner:INST OF CHEM MATERIAL CHINA ACADEMY OF ENG PHYSICS

A high saturation magnetization mn 0.8 zn 0.2 fe 2 o 4 Preparation method of nanoparticle and magnetic liquid thereof

The invention relates to the field of novel nanometer functional materials, in particular to a preparing method of high saturation magnetization strength Mn0.8Zn0.2Fe2O4 nanoparticles and magnetic liquid of the nanoparticles. The preparing method specifically comprises the steps of dispersing salts of Mn2+, Zn2+ and Fe3+ into ultrapure water and quickly adding a NaOH solution under mechanical stirring; then placing the reaction liquid into a drying oven to be heated at high temperature, promoting the growth of crystal grains and completing the second step of sediment; then taking out the reaction liquid, adding fluorine ether acid, covering particles under mechanical stirring to avoid aggregation of the particles and then washing and drying the particles; finally, grinding the dried particles and dispersing the particles into fluorine ether oil base carrier liquid under mechanical stirring to prepare magnetic liquid. The prepared Mn0.8Zn0.2Fe2O4 nanoparticles have the advantages of high saturation magnetization strength, superparamagnetism, high antioxidant stability and the like, and the prepared fluorine ether oil base magnetic liquid can be applied in the field of rotary shaft sealing under the high temperature, corrosion and oxidation environment for a long term.
Owner:SICHUAN UNIV +1
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