9 results about "Acetylpyrazine" patented technology

According to the invention, pyrazine is used as a raw material, acetic anhydride is used as an acetylation reagent, and 2-acetylpyrazine is prepared under the condition of a metal supported catalyst. The method has the advantages of simple operation, few steps, good selectivity, few by-products and high product quality, and avoids the process route which easily causes by-products and impurities, such as high reagent toxicity, more reaction components, violent reaction and the like in the prior art. The product system is simple to purify, high in purity and stable in process route.

The invention belongs to the technical field of molecular photoswitch materials, and provides a pyrazine coordination ruthenium complex, a preparation method thereof and application of the pyrazine coordination ruthenium complex as a ratio type molecular photoswitch, the pyrazine coordination ruthenium complex is composed of positive ions and negative ions, the structural formula of the positive ions is shown in the formula (I), and the negative ions are shown in the specification. The preparation method comprises the following steps: firstly, reacting 2-acetylpyrazine with benzimidazole-2-formaldehyde to prepare a ligand L; and filtering after the reaction, adding a ligand L into the filtrate for heating reflux reaction, and purifying the product to obtain the pyrazine coordination ruthenium complex. The complex provided by the invention has unique dual emission and ratio type response, can realize high-precision and anti-interference ratio type pH sensing, and eliminates the influence of factors such as probe concentration, instrument efficiency and the like.

The invention discloses a preparation method of composite roasted peanut essence, which belongs to the technical field of essence, and comprises the following steps: preheating peanut oil and caprylic / capric triglyceride; the preparation method comprises the following steps: dissolving ethyl maltol, vanillin, methyl cyclopentenolone, 2, 3, 5-trimethylpyrazine and 2-acetylpyrazine; vanillin propylene glycol acetal, isovaleraldehyde propylene glycol acetal, triethyl citrate, delta-decalactone, delta-dodecalactone and 5-hydroxyethyl-4-methylthiazole are fused to obtain a mixture; dispersing the roasted peanut extract; 2, 3-dimethylpyrazine, 2-methoxyl-5-methylpyrazine and 4-methylthiazole are fused, and then the mixture is subjected to a reaction; the preparation method comprises the following steps: fusing cocaal, dimethyl sulfide, 2-ethyl-3, 5, 6-dimethylpyrazine, 2, 3, 5, 6-tetramethylpyrazine, 2-methylpyrazine, 2-acetylpyridine, 2-methoxy-3. 5. 6-isopropyl pyrazine, 2-methylthio-3-methylpyrazine, isovaleric acid, 1-octylene-3-alcohol, 5-methylfurfural and 3, 4-dimethyl-1, 2-cyclopentanedione; standing is performed; filtering is performed; the fragrance of the roasted peanuts is closer to that of the roasted peanuts which are just taken out of a furnace, and the natural flavor of the roasted peanut essence is increased.

The utility model discloses a rapid sample pretreatment instrument for acetylpyrazine detection, and relates to the technical field of acetylpyrazine detection. The device comprises a cylinder body, a panel is inserted into the top of the cylinder body, an extraction assembly is arranged above the panel, a pipeline is fixedly connected to the right side of the cylinder body, a pressure gauge is installed on the pipeline, a waste liquid tank is inserted into the cylinder body, and the left side and the right side of the inner wall of the waste liquid tank are each fixedly connected with two positioning insertion strips. A sample placing rack is inserted into the waste liquid tank through four positioning insertion strips. The positioning insertion strips are arranged, specifically, the waste liquid tank is placed in the cylinder body, the sample placement frame is inserted into the waste liquid tank, and the sample placement frame is positioned through the positioning insertion strips on the inner wall of the waste liquid tank, so that the waste liquid tank and the sample placement frame can be placed at the same time, and liquid cannot be influenced to enter the waste liquid tank; therefore, the frequency of opening the panel is reduced, and the working efficiency during extraction is improved.

The invention discloses walnut essence and a preparation method thereof. The essence comprises furanone, methyl cyclopentenolone, 2-acetylpyrazine and benzaldehyde acetal compounds as core components, and the four components synergistically provide vivid and stable roasted walnut characteristic aroma; preferably, the formula also contains auxiliary materials such as butanedione, ethyl maltol, ethyl 2-methylbutyrate, dimethyl sulfide and the like, and ethanol and propylene glycol are used as solvents. According to the invention, benzaldehyde acetal (such as benzaldehyde PGA) is adopted to replace free benzaldehyde, so that the stability of the essence in high-temperature processing is remarkably improved. The prepared essence is rich in fragrance level and lasting in fragrance, and can be widely applied to foods, beverages and daily chemical products.

The invention belongs to the field of food additive essence. The invention discloses pot gas essence and a preparation method and application thereof, and the pot gas essence comprises the following components: caprylic / capric triglyceride, benzyl alcohol, black pepper oil, 2-acetylpyrazine, methylcyclopentenolone, ethyl maltol, 4-hydroxy-2, 5-dimethyl-3 (2H) furanone, 2-tridecanone, acetic acid, 2, 5-dimethylpyrazine, furfuryl mercaptan, 1, 3, 4-trimethyl-1, 3-pentanediol, 1, 3, 4-trimethyl-1, 3-pentanediol, 1, 3, 4-trimethyl-1, 3-pentanediol, 1, 3, 4-trimethyl-1, 3-pentanediol, 1, 3, 4-trimethyl-1, 3-pentanediol, 1, 3, 4-trimethyl-1, 3- The invention relates to an anti-rust oil which is prepared from 1, 8-cineole, 3-(methylthio) propionaldehyde, oleic acid, phenethyl alcohol, sesame oil, 2-decenal, 2, 4-undecadienal, phenylacetaldehyde, 3-(methylthio) butyraldehyde, 3-(methylthio) propanol, bis (2-methyl-3-furyl) disulfide, 2-methyl-3-mercaptofuran and 2, 3-pentanedione. The pot gas essence can simulate real pot gas flavor, and prepared food is good in temperature resistance, high in verisimilitude, lasting and stable in flavor, small in dosage and low in cost and has high application value.

The invention discloses a method for simultaneously determining seven spices and essences in rice, which adopts a liquid chromatography-tandem mass spectrometry method, and comprises the following steps: 1) mixing a rice sample with an extracting agent, carrying out vortex, ultrasonic extraction and low-temperature high-speed centrifugation, passing the supernatant through a 0.2 mu m wwPTFE (polytetrafluoroethylene) microfiltration membrane, and loading the supernatant into a machine for determination, the extracting agent is a mixture of water and 0.1% formic acid methanol in a volume ratio of 3: 7; (2) separating by using a Bipheyl chromatographic column under the chromatographic condition, and carrying out gradient elution by using 0.1% formic acid water and 0.1% formic acid methanol as mobile phases; the mass spectrometry is detected in a positive ion scanning multi-reaction monitoring mode, and is quantified by an external standard method. According to the method, seven spices such as 2-acetylpyrazine, 2-acetylpyridine, ethyl maltol, vanillin, methyl vanillin, ethyl vanillin and coumarin which may be maliciously added in the rice can be simultaneously determined, and the seven spices are simultaneously determined by adopting the same detection means, so that the cost is saved, the efficiency is improved, and the method is suitable for large-scale popularization and application. The method has high separation degree and good accuracy and precision.

The application discloses coffee essence, atomized liquid and electronic atomization device, and belongs to the field of electronic atomizers. The coffee essence comprises 2-acetylpyrrole, vanillin, methylcyclopentenolone, maltol, furfuryl acetate, guaiacol, isopentyl alcohol propylene glycol solution, furfuryl mercaptan, 2-ethyl-3,5-dimethylpyrazine, isovaleric acid propylene glycol solution, 2,3,5-trimethylpyrazine, isobutyraldehyde, 2-methyl-3-(methylthio)pyrazine, isoamyl aldehyde, trigonellin, 4-hydroxy-2,5-dimethyl-3(2H)-furanone, 5-methylfurfural, dimethyl sulfide, 2-acetylfuran, 5-hydroxyethyl-4-methylthiazole, 2-acetylpyrazine, 4-ethylguaiacol, acetic acid, propionic acid, acetaldehyde propylene glycol solution, 4-methyl-5-(2-acetyloxyethyl)-thiazole and propylene glycol. The coffee essence has good stability, good compatibility and can accurately restore the real coffee roasting aroma.

This invention provides a coffee flavoring and its preparation method, comprising 0.1 parts of furanone, 2-acetylpyrazine, vanillin, ethanol, 3-methylthiopropional, 2-methoxy-4-vinylphenol, 2-ethyl-3-methylpyrazine, 2-ethyl-3,5-dimethylpyrazine, furfuryl mercaptan, β-damascone, p-cresol, hexanoic acid, 2-methylbutyric acid, 2,3-pentanedione, methyl furfuryl disulfide, 3-mercapto-3-methylbutyl formate, terpineol, 1-octen-3-ol, isobutyraldehyde, furfural, 5-methylfurfural, isovaleraldehyde, linalool, 2-methoxy-3-isobutylpyrazine, phenylacetaldehyde, eugenol, 2,3,5-trimethylpyridinium, guaiacol, 4-ethylguaiacol, an amino acid composition, glycerol, water, and coffee extract. The coffee flavoring of this invention has a strong three-dimensional aroma, rich layers, and high overall aroma realism and harmony.