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65 results about "Hydrogen peroxide product" patented technology

Its structural formula is: Pure hydrogen peroxide is a colourless liquid, but it is sold on the market as solutions in water, containing up to 33 – 37% pure hydrogen peroxide and other additives to stop the product decomposing.

Slurry bed loop reactor, application and method for producing hydrogen peroxide

The invention relates to a slurry bed loop reactor, application and a method for producing hydrogen peroxide. The slurry bed loop reactor comprises a riser, a separation tank and a downcomer which are communicated sequentially, wherein an expansion section with expanded pipe diameter is arranged at the upper part of the riser, the upper part of the expansion section is communicated with the separation tank, a liquid phase outlet in the upper part of the separation tank is communicated with the upper part of the downcomer, the bottom of the downcomer is communicated with the bottom of the riser, and the bottom of the separation tank is communicated with the lower part of the downcomer; and a raw material inlet is formed in the bottom of the riser, gas outlets are formed in the top of the expansion section of the riser and in the top of the separation tank, a filtration component is arranged in the downcomer and a clear liquid outlet is formed in the upper part of the downcomer via the filtration component. According to a hydrogenation method for producing hydrogen peroxide by an anthraquinone method with the adoption of the slurry bed loop reactor, the gas-liquid-solid three-phase separation efficiency is high, the excess local liquid holdup of a catalyst is avoided, the possibility of excessive hydrogenation is reduced, the hydrogenation efficiency is further effectively improved and a hydrogen peroxide product with relatively high concentration can be obtained.
Owner:CHINA PETROLEUM & CHEM CORP +1

Loop reaction device in slurry bed, application and method for producing hydrogen peroxide

The invention relates to a loop reaction device in a slurry bed, application and a method for producing hydrogen peroxide. The loop reaction device comprises a slurry bed reactor and a solid-liquid separator, wherein the upper part of the slurry bed reactor is communicated with the upper part of the solid-liquid separator, and the bottom of the slurry bed reactor is communicated with the bottom of the solid-liquid separator; and a coaxial inner sleeve is arranged in the slurry bed reactor, an outer sleeve is arranged between the inner sleeve and the outer wall of the slurry bed reactor at the upper part of the slurry bed reactor, a raw material inlet and a fluid distributor are arranged in the inner sleeve and at the bottom, a gas outlet is formed in the top of the slurry bed reactor, a filtration component is arranged in the solid-liquid separator, and a clear liquid outlet is formed in the wall of the solid-liquid separator via the filtration component. According to a hydrogenation method for producing hydrogen peroxide by an anthraquinone method with the adoption of the slurry bed loop reactor, the gas-liquid-solid three-phase separation efficiency is high, the excess local liquid holdup of a catalyst is avoided, the possibility of excessive hydrogenation is reduced, the hydrogenation efficiency is further effectively improved and a hydrogen peroxide product with relatively high concentration can be obtained.
Owner:CHINA PETROLEUM & CHEM CORP +1

System and method for concentrating and purifying hydrogen peroxide

The invention relates to a system and a method for concentrating and purifying hydrogen peroxide. A hydrogen peroxide concentration rectifying tower T101 is provided with a feed port; the tower top is connected with an inlet of a condenser E101; one part at the outlet of the condenser E101 is recovered and the other part at the outlet of the condenser E101 returns to a tower top reflux substance inlet of the hydrogen peroxide concentration rectifying tower T101; one part at the bottom of the hydrogen peroxide concentration rectifying tower T101 is recovered and the other part at the bottom of the hydrogen peroxide concentration rectifying tower T101 is connected with an inlet of a hydrogen peroxide concentration tower bottom reboiler E102; and an outlet of the hydrogen peroxide concentration tower bottom reboiler E102 is connected with a reflux substance inlet at the bottom of the hydrogen peroxide concentration rectifying tower T101. The method comprises the following steps: mixing 25 to 35 weight percent of hydrogen peroxide serving as a raw material with a stabilizing agent; feeding into the hydrogen peroxide concentration rectifying tower T101; and allowing the top gas phase to enter the condenser E101 to obtain the hydrogen peroxide product at the concentration of more than or equal to 50 weight percent. The system and the method adopts continuous operation and are suitable for large-scale industrial production; heating mediums are steam and soft water, so contact of organic materials and the hydrogen peroxide is avoided and the system and the method are safe and reliable; and the afterheat in a factory serves as the heat source of the rectifying tower, so low-grade energy is utilized, the public engineering investment is saved, and energy consumption is reduced.
Owner:TIANJIN UNIV

Preparation technique and device for ultra-pure hydrogen phosphide

The invention provides a continuous production process for ultra-pure hydrogen peroxide, comprising the following steps: mixing the industrial hydrogen peroxide material with the modified active carbon; then classifying filter by microfiltration membrane and ultrafiltration membrane in sequence; the filtrate is pumped into the distillation column formed by a plurality of columns connected in series; adding metal ion complexing agent into the primary column; performing reverse osmosis on the semi-finished products out of the column before filtering by nanofiltration membrane to get ultra-pure hydrogen peroxide products. The device comprises the following parts: a raw material chute, an active carbon pre-mixer, a microfiltration and ultrafiltration filter, a distillation column formed by a plurality of columns connected in series, a reverse osmosis device, a nanofilter, a finished product receiver, a pump and a shaft; wherein, the raw material chute outlet is connected with the active carbon pre-mixer inlet; the microfiltration and ultrafiltration filter outlet is connected with the pump, the outlet of which is connected with the inlet of the distillation column formed by a plurality of columns connected in series; the outlet of the distillation column formed by a plurality of columns connected in series is connected with the inlet of the reverse osmosis device, the outlet of which is connected with the shaft; the outlet of the shaft is connected with the inlet of the nanofilter, the outlet of which is connected with the finished product receiver.
Owner:JIANGYIN RUNMA ELECTRONICS MATERIAL

Slurry-bed circulation flow reactor and application and method for producing hydrogen peroxide

The invention discloses a slurry-bed circulation flow reactor and an application and a method for producing hydrogen peroxide. The slurry-bed circulation flow reactor comprises an ascension pipe, an expanding section used for expanding pipe diameter of the upper part of the ascension pipe and a solid-liquid separator, wherein the expanding section is communicated with the upper part of the solid-liquid separator; the bottom of the solid-liquid separator is communicated with the bottom of the ascension pipe; a three-phase separator of a double sleeve structure is arranged in the expanding section; a raw material inlet is formed in the bottom of the ascension pipe; a gas outlet is formed in the top of the expanding section; a filtration component is arranged in the solid-liquid separator; and a clear liquid outlet is arranged at the upper part of the solid-liquid separator by virtue of the filtration component. According to a method for producing hydrogen peroxide by taking the slurry-bed circulation flow reactor as a hydrogenation reactor, the gas-liquid-solid three-phase separation efficiency is high; the local excessive hydrogenation of the catalyst is avoided; the excessive hydrogenation possibility is reduced; the hydrogenation efficiency is high; and hydrogen peroxide products with high concentration can be produced.
Owner:CHINA PETROLEUM & CHEM CORP +1

Oxidation-extraction technology for production of hydrogen peroxide by anthraquinone process

The invention discloses an oxidation-extraction technology for production of hydrogen peroxide by anthraquinone process. The oxidation-extraction technology for production of hydrogen peroxide by anthraquinone process comprises the following contents: (1) introducing hydrogenation liquid and oxygen-containing gas from the bottom of an oxidation-extraction reactor to carry out concurrent-flow oxidation reaction from the bottom to the top inside the reactor so as to continuously generate H2O2; (2) introducing an extraction agent through the upper middle part of the oxidation-extraction reactor while the reaction in the step (1) is carried out, letting the extraction agent flow from the top to the bottom in the reactor, and gradually extracting out the H2O2 generated by the oxidation reaction; and (3) carrying out gas-liquid separation on the material from the bottom to the top, removing residual moisture with a working solution and flowing out, settling the material from the top to the bottom in the settling section, removing the residual working solution in water, and purifying or concentrating to obtain a hydrogen peroxide product. According to the technology, the two processes of oxidation and extraction are coupled to each other. The oxidation reaction is carried out while extraction of H2O2 is conducted. Meanwhile, oxidation reaction rate and extraction efficiency are enhanced, the technological process is simplified, and the technology is beneficial to save investments and reduce energy consumption.
Owner:CHINA PETROLEUM & CHEM CORP +1

Multi-component all-acid fixed bed hydrogen peroxide production process

The invention relates to a multi-component all-acid fixed bed hydrogen peroxide production process which comprises the following steps: (1) in a hydrogenation tower, carrying out hydrogenation reaction on raw material hydrogen and a carrier anthraquinone under the action of a palladium-gold catalyst to generate a hydroanthraquinone hydrogenation solution; (2) adding phosphoric acid into the hydroanthraquinone hydrogenation solution to adjust the pH value to 3.5 + / -0.2, and reacting with oxygen in the air to obtain an oxidation liquid; and (3) taking pure water as an extraction agent, carryingout countercurrent extraction in an extraction tower to obtain an extraction solution containing hydrogen peroxide, and then purifying with heavy aromatics in a purification tower to obtain a qualified hydrogen peroxide product. According to the production process, a full-acid fixed bed process technology is adopted, balanced regeneration of a working solution system is optimally controlled, partial aluminum peroxide adsorption regeneration is adopted, dust entrainment is reduced, meanwhile, the filtering precision is improved, dust and salt entrainment in a product is greatly reduced, and indexes such as free acid, organic carbon and non-volatile matter are far away; and the product purity is superior to the national standard and companies.
Owner:PINGHU PETROCHEM

High-efficiency extraction process in hydrogen peroxide production process

The invention discloses a high-efficiency extraction process in a hydrogen peroxide production process. According to the invention, in an extraction process of an anthraquinone method for producing hydrogen peroxide; an extraction tower I and an extraction tower II are arranged; an oxidation liquid is divided into two parts which are an oxidation liquid I and an oxidation liquid II; pure water is introduced from the top of the extraction tower I, and the oxidation liquid I is introduced from the bottom of the extraction tower I; the two phases are subjected to countercurrent extraction in the extraction tower I; raffinate is discharged from the top of the extraction tower I, and is subjected to separation in a liquid/liquid separator, such that a heavy phase and a light phase are obtained; the heavy phase is mixed with extract liquid from the bottom of the extraction tower I, and the mixture of the heavy phase and the extract liquid from the bottom of the extraction tower I is introduced from the top of the extraction tower II; the light phase is mixed with the oxidation liquid II, and the mixture of the light phase and the oxidation liquid II is introduced from the bottom of the extraction tower II; the two phases are subjected to countercurrent extraction in the extraction tower II; a tower top raffinate phase is introduced into a post-treatment process; and the tower bottom extraction liquid is the high-concentration hydrogen peroxide product. The high-efficiency extraction process provided by the invention is provided aiming at the defects of prior arts. The process has the advantages of high mass transfer rate, high Murphree efficiency, high product concentration, low raffinate content, and the like.
Owner:CHINA PETROLEUM & CHEM CORP +1

Fluidized bed hydrogenation reaction and separation process and device for producing hydrogen peroxide by virtue of anthraquinone method

The invention discloses a fluidized bed hydrogenation reaction and separation process and device for producing hydrogen peroxide by virtue of an anthraquinone method. A working solution and hydrogen are continuously added into a fluidized bed reactor with a catalyst for hydrogenation reaction, reacting materials are driven by gas to upwards move to the top of a draft tube, and are downwards filtered through a membrane separator, filtered hydrogenation liquor flows to a hydrogenation liquor storage tank, and the catalyst is retained on a filter element, and returns into the reactor to continue participating in reaction through backflush operation. On the upper part of the reactor, incompletely reacted hydrogen mixed up with a small amount of working solution overflows, and returns to the reactor to participate in reaction through a circulating compressor after the working solution is separated through a circulating gas separator. During regeneration of the built-in membrane separator, an external membrane separator is adopted for separation. According to the process and the device, the raw materials and the catalyst are uniformly mixed, the reaction homogeneity is high, the utilization efficiency of the catalyst is high, and a high-concentration hydrogen peroxide product can be obtained with fewer side reactions. The device is simple in structure, and can run stably.
Owner:河北美邦工程科技股份有限公司

System and method for producing hydrogen peroxide through anthraquinone method

The invention discloses a system and method for producing hydrogen peroxide through an anthraquinone method. The system comprises the four unit processes of hydrogen dissolving, hydrogenation, oxidation and extraction, wherein a hydrogenation unit comprises a series fixed bed and upflow-type tubular reactors, and working liquid and hydrogen are subjected to a hydrogenation reaction in the hydrogenation unit to obtain hydrogenation liquid; an oxidation unit comprises an oxidation tower, the hydrogenation liquid and oxygen-containing gas are subjected to an automatic oxidation reaction to obtainoxidation liquid; and an extraction unit comprises an extraction tower, hydrogen peroxide in the oxidation liquid is extracted by the water, and thus a high-concentration hydrogen peroxide product isobtained. According to the system and method, the anthraquinone hydrogenation reaction rate can be significantly improved, the anthraquinone hydrogenation reaction efficiency can be significantly improved, the uniformity of the reaction process is maintained, side reactions are less, the obtained hydrogenation liquid is good in quality, small in by-product number and low in viscosity, the gas-liquid mass transfer rate in the oxidation process is increased, the extraction efficiency in the extraction process is improved, the oxidation time is significantly shortened, and the number of actual tower plates of the extraction tower is decreased.
Owner:CHINA PETROLEUM & CHEM CORP +1

Preparation technique and device for ultra-pure hydrogen phosphide

The invention provides a continuous production process for ultra-pure hydrogen peroxide, comprising the following steps: mixing the industrial hydrogen peroxide material with the modified active carbon; then classifying filter by microfiltration membrane and ultrafiltration membrane in sequence; the filtrate is pumped into the distillation column formed by a plurality of columns connected in series; adding metal ion complexing agent into the primary column; performing reverse osmosis on the semi-finished products out of the column before filtering by nanofiltration membrane to get ultra-pure hydrogen peroxide products. The device comprises the following parts: a raw material chute, an active carbon pre-mixer, a microfiltration and ultrafiltration filter, a distillation column formed by a plurality of columns connected in series, a reverse osmosis device, a nanofilter, a finished product receiver, a pump and a shaft; wherein, the raw material chute outlet is connected with the active carbon pre-mixer inlet; the microfiltration and ultrafiltration filter outlet is connected with the pump, the outlet of which is connected with the inlet of the distillation column formed by a plurality of columns connected in series; the outlet of the distillation column formed by a plurality of columns connected in series is connected with the inlet of the reverse osmosis device, the outlet of which is connected with the shaft; the outlet of the shaft is connected with the inlet of the nanofilter, the outlet of which is connected with the finished product receiver.
Owner:JIANGYIN RUNMA ELECTRONICS MATERIAL
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