The invention discloses an
acid etching solution recycling regeneration method. The
acid etching solution recycling regeneration method comprises following steps that (1) an
acid etching solution recycling regeneration
system is prefabricated; (2) an
etching waste solution produced by an
etching production line is stored in a waste solution
barrel, and the
etching waste solution in the waste solution
barrel is added into an ionic membrane
electrolysis circulation device in an automatic detection adding mode; (3) a regenerated solution and elemental
copper are produced in the mode that the etching waste solution is electrolyzed by the ionic membrane
electrolysis circulating device, the regenerated solution is stored in a regenerated solution
barrel, and the elemental
copper is removed out in the form of a
copper plate; and (4) an oxidant,
hydrochloric acid and the regenerated solution stored in the regenerated solution barrel are correspondingly added into a regenerated solution dispensing monitoring device, the regenerated solution is tested and dispensed by a plurality of detectors in the regenerated solution dispensing monitoring device, the
redox potential range of the regenerated solution is between 480 mv and 520 mv, the copper concentration is within the range of 30-60 g / L, and then the regenerated solution flows back into the etching
production line to be used. The invention further discloses an acid etching solution recycling regeneration
system for implementing the method.