The invention discloses a preparation method of novel two-dimensional material reinforced 
polyethylene glycol lubricating oil. The preparation method comprises the following steps: step I, adding Ti3AlC2 
powder into an HF solution, performing the 
corrosion reaction, magnetically stirring for a plurality of time, then centrifugally washing, 
vacuum drying, and obtaining Ti3C2 
powder; step II, mixingthe Ti3C3 
powder in step I and an intercalating 
solvent, stirring, washing, 
drying, and obtaining the processed Ti3C2 powder; step III, dissolving the Ti3C2 powder processed in step II in the deionized water, ultrasonically 
processing, centrifuging, collecting supernatant, 
drying, and obtaining Ti3C2 two-dimensional nanosheets; and step IV, stirring and mixing the Ti3C2 two-dimensional nanosheetsobtained in the step III and 
polyethylene glycol, preparing different solutions of different concentrations, ultrasonically 
processing, and then performing the friction abrasion experiment. The preparation method has the advantages of excellent cooling performance, difficulty in 
combustion, low 
pollution, low cost and the like.