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44results about How to "Low peroxide content" patented technology

Whitening traditional Chinese medicine composition as well as preparation method and application thereof

The invention discloses a whitening traditional Chinese medicine composition as well as a preparation method and application thereof. The preparation method comprises the steps as follows: raw materials comprising safflower, notoginseng, sanguis draconis and persimmon leaf are weighed; the safflower is taken, crushed and then subjected to heating, reflux extraction is performed through an alcohol aqueous solution, and an extraction solution is filtered, and pressure-reduction concentration is performed to obtain a thick paste; the notoginseng is taken and crushed, heating reflux extraction is performed through petroleum ether, chloroform or acetidin, and an extraction solution is filtrated, and pressure-reduction concentration is performed to obtain another thick paste; the sanguis draconis is taken and crushed, pressure-reduction concentration is performed through a 95-percent alcohol aqueous solution, an extraction solution is filtrated, pressure-reduction concentration is performed through to remove alcohol, so that a concentrated solution is obtained, the concentrated solution is placed in water, uniformly agitated, filtrated, extracted by the petroleum ether and then extracted through acetidin to obtain a third thick paste; the persimmon leaf is taken, and crushed, heating reflux extraction is performed through the alcohol aqueous solution, an extraction solution is filtered, and pressure-reduction concentration is performed to obtain a fourth thick paste; all the thick pastes are uniformly mixed. Experiment results show that the whitening traditional Chinese medicine composition disclosed by the invention can resist the activity of tyrosinase, and enables the skin to keep healthy and white for a long time.
Owner:TIANJIN JIASHITANG SCI & TECH

Method for preparing acetophenone and its derivatives through selectively oxidizing ethylbenzene and its derivatives

The invention discloses a method for preparing acetophenone and its derivatives through selectively oxidizing ethylbenzene and its derivatives. The method comprises the following steps: putting ethylbenzene and its derivatives, a cobalt (II) salt catalyst, an oxidizing agent and a dispersant in an agate ball milling tank, sealing the ball milling tank, carrying out ball milling at room temperatureunder a rotating speed of 100-800 rpm for 3.0-24.0 h, stopping the ball milling one time every 1.0-3.0 h, and discharging a gas in the ball milling tank; and dissolving the obtained reaction mixturein anhydrous ethanol after the reaction is finished, performing stirring at room temperature, filtering the obtained solution, washing the obtained solid with anhydrous ethanol, mixing the obtained ethanol solutions, and making the volume reach a constant value. The method provided by the invention has the advantages of small catalyst dosage, no solvents, no heating, low reaction temperature, lessenergy consumption, convenience in operation, high acetophenone selectivity, no obvious peroxide residue, high safety factor, and realization of selective and safe oxidative conversion of ethylbenzene and its various derivatives.
Owner:ZHEJIANG UNIV OF TECH

Peanut shell activated carbon for removing toxins in peanut oil and preparation method thereof

The invention belongs to the technical field of activated carbon, and particularly relates to a peanut shell activated carbon for removing toxins in peanut oil and a preparation method thereof. The peanut shell activated carbon is prepared by carrying out pretreatment, extrusion molding, carbonization and activation on peanut shells. The preparation method comprises the following steps: pretreatment: carrying out hydrothermal treatment on the peanut shells, and pulverizing; extrusion molding: carrying out pressure molding with a granulator to obtain cylindrical granules of which the diameters are 4-8 mm and the lengths are 10-20 mm; heating, cooling in the absence of oxygen, crushing and screening to control the granule diameters at 1-3 mm; and introducing isothermal superheated vapor, storing in a sealed environment, and cooling to obtain the finished product. The activated carbon is prepared from the peanut shells which are accessible raw materials, thereby implementing utilization of waste peanut shells; and the obtained peanut shell activated carbon has the advantages of large specific area and small pore size, can simultaneously adsorb benzopyrene, aflatoxin and other harmful substances, and can prevent the peanut oil from oxidative rancidity.
Owner:山东沂蒙山花生油股份有限公司

Method for selectively oxidizing cumene compounds

The invention relates to a method for selectively oxidizing cumene compounds, and the method comprises the following steps: placing cumene compounds shown in a formula (I), an iron porphyrin catalyst,an oxidant and a dispersant into a ball milling tank, sealing the ball milling tank, performing ball milling for 3 to 24 hours at a rotating speed of 100 to 800 rpm at room temperature, stopping ballmilling once every 1 to 3 hours in the ball milling process, discharging gases in the ball milling tank, finishing the reaction, and performing post-treatment on a reaction mixture to obtain product2-phenyl-2-propanol compound shown in a formula (II); according to the invention, the oxidation conversion of the cumene and derivatives thereof is realized through solid-phase ball milling, the reaction mode is novel, the operation is convenient, and the energy consumption is low; the method needs no organic solvent, thus effectively avoiding the use of toxic and harmful organic solvents and being green and environment-friendly; has low peroxide content and high safety factor, and high 2-phenyl-2-propanol and derivative selectivity and meets the social requirements of the current green chemical process, environmental compatibility chemical process and biological compatibility chemical process.
Owner:ZHEJIANG UNIV OF TECH

Oil and fat composition

The invention relates to the field of oil and fat processing and provides an oil and fat composition by aiming at the problem that the single oil fat has single nutritional component. The oil and fatcomposition is prepared from the following components in parts by mass: 30 to 40 parts of soybean oil, 35 to 40 parts of olive oil, 15 to 20 parts of fish oil, 3 to 5 parts of lecithin, 1 to 3 parts of sucrose palmitate and 5 to 7 parts of edible alcohol. A preparation method of the fat and oil composition comprises the following steps: S1, mixing; S2, adding protease; and S3, deodorizing and performing centrifugal filtration. Another preparation method of the fat and oil composition comprises the following steps: S1, mixing; S2, adding protease and performing deacidification; S3, removing peroxide; S4, deodorizing; and S5, performing silica gel column chromatography and filtering a membrane. Through synergistic cooperation of the lecithin, the sucrose palmitate and the edible alcohol synergistically, and using the above method to prepare the oil and fat composition, the oil and fat composition prepared by the above method is favorable for synergistic cooperation of the soy oil, the olive oil and the fish oil, enables the nutrition in the oil and fat composition to be balanced and is favorable for improving the stability of the oil and fat composition.
Owner:广州隽沐生物科技股份有限公司
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