The invention discloses a
plutonium-containing feed liquid continuous
evaporation concentration and
oxalic acid destruction method and
system.The method comprises the steps that a
manganese solution and
nitric acid are added into the
plutonium-containing feed liquid for
seasoning, and
mixed feed liquid is obtained; continuously adding the mixed material liquid into an
evaporator, heating and maintaining a preset temperature, so that the mixed material liquid is evaporated and concentrated in the
evaporator, and
oxalic acid destruction is completed; when the concentration of the feed liquid in the
evaporator reaches the required multiple and the damage of
oxalic acid meets the requirement, the concentrated feed liquid starts to be continuously discharged to a concentrated liquid receiving tank,
continuous feeding and discharging are achieved, the discharging speed is equal to the feeding speed / the concentration multiple, the feeding speed of the
mixed feed liquid and the discharging speed of the concentrated liquid are adjusted, and the feeding speed of the
mixed feed liquid and the discharging speed of the concentrated liquid are adjusted; and the liquid level is constant at the preset liquid level value. The method has the advantages of large concentration multiple, high oxalic acid damage rate, large working flux, small equipment
fatigue damage, stable equipment,
continuous operation and simple operation, can meet the operation requirements of a post-treatment
plant, greatly reduces the treatment amount of a
plutonium purification cycle flow, and reduces the
wastewater amount.