A preparation method of a carbon-carbon
composite material with high
thermal conductivity comprises the following steps: parallelly arranging
mesophase asphalt-based
carbon fibers in a flat plate, uniformly spreading a layer of condensed polynuclear
aromatic hydrocarbon resin
powder on the
mesophase asphalt-based
carbon fibers, heating the resin
powder for fully melting so as to coat a resin film layer on the
fiber surface, naturally cooling to obtain a carbon
fiber preform; or dissolving the condensed polynuclear
aromatic hydrocarbon resin by an
organic solvent to prepare a solution, soaking the
mesophase asphalt-based
carbon fibers in the solution, completely volatilizing the
solvent to form a resin layer on the
fiber surface so as to obtain the carbon fiber preform;
cutting the carbon fiber preform into thin sheets according to a desired dimension, orderly stacking the sheet-like carbon fiber preform in a mold, performing pressurization to 20-70 MPa, heating to 110-145 DEG C, performing depressurization, maintaining for 0.5-2 hours, heating again to 200-300 DEG C, curing for 1-6 hours, after curing, naturally cooling to
room temperature for demolding, performing
carbonization at 900 DEG C of the obtained cured sample, soaking the sample with asphalt at a soaking temperature of 340-400 DEG C for soaking time of 1-8 hours, repeating the
carbonization-soaking
cyclic process to increase the sample density to 1.5-1.7 g / cm3, and performing graphitization to prepare the carbon-carbon
composite material with high
thermal conductivity. The invention has the advantages of low
energy consumption and high
thermal conductivity.