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Thick polycrystalline synthetic diamond wafers for heat spreading applications and microwave plasma chemical vapour depositon synthesis techniques

A method of fabricating a polycrystalline CVD synthetic diamond material having an average thermal conductivity at room temperature through a thickness of the polycrystalline CVD synthetic diamond material of at least 2000 Wm−1K−1, the method comprising: loading a refractory metal substrate into a CVD reactor; locating a refractory metal guard ring around a peripheral region of the refractory metal substrate, the refractory metal guard ring defining a gap between an edge of the refractory metal substrate and the refractory metal guard ring having a width 1.5 mm to 5.0 mm; introducing microwaves into the CVD reactor at a power such that the power density in terms of power per unit area of the refractory metal substrate is in a range 2.5 to 4.5 W mm−2; introducing process gas into the CVD reactor wherein the process gas within the CVD reactor comprises a nitrogen concentration in a range 600 ppb to 1500 ppb calculated as molecular nitrogen N2, a carbon containing gas concentration in a range 0.5% to 3.0% by volume, and a hydrogen concentration in a range 92% to 98.5% by volume; controlling an average temperature of the refractory metal substrate to lie in a range 750° C. to 950° C. and to maintain a temperature difference between an edge and a centre point on the refractory metal substrate of no more than 80° C. growing polycrystalline CVD synthetic diamond material to a thickness of at least 1.3 mm on the refractory metal substrate; and cooling the polycrystalline CVD synthetic diamond material to yield a polycrystalline CVD synthetic diamond material having a thickness of at least 1.3 mm, an average thermal conductivity at room temperature through the thickness of the polycrystalline CVD synthetic diamond material of at least 2000 Wm−1K−1 over at least a central area of the polycrystalline CVD synthetic diamond material, wherein the central area is at least 70% of a total area of the polycrystalline CVD synthetic diamond material, a single substitutional nitrogen concentration no more than 0.80 ppm over at least the central area of the polycrystalline CVD synthetic diamond material, and wherein the polycrystalline CVD synthetic diamond material is substantially crack free over at least the central area thereof such that the central area has no cracks which intersect both external major faces of the polycrystalline CVD synthetic diamond material and extend greater than 2 mm in length.
Owner:ELEMENT SIX TECH LTD

Pre-assembled plate consisting of armoured concrete

The invention relates to a pre-assembled plate consisting of armored concrete, especially for the use as a component of a solid roadway for high-speed means of transport. At least two steel rods extending in the longitudinal direction of the pre-assembled plate of armored concrete (10) and protruding over the concrete surface thereof on the front face (17) are provided. The pre-assembled plate (10) is provided with at least one, preferably several, predetermined breaking points (15) which extends crosswise in relation to the steel rods (19). The steel rod (19) is anchored in the area between the front face (17) of the pre-assembled plate (10) and the first predetermined breaking point (1) respectively and is mounted in the direction towards the respective front face (17) in the longitudinal direction thereof in an essentially freely moveable manner. According to a method for producing a plate composite structure of pre-assembled plates of armored concrete (10), the pre-assembled plate (10) is placed and exactly positioned. A casting compound (42) is underpoured under the exactly positioned pre-assembled plate. The pre-assembled plate (10) is connected to the adjacent pre-assembled plate (10) by casting the joint and connecting the steel rods (19) after the casting compound (42) has hardened.
Owner:MAX BOGL BAUUNTERNEHMUNG
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