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63results about How to "Reduce operating severity" patented technology

Method and apparatus for high-efficient crude oil desalination / dehydration

The invention belongs to the technical field of petrochemical industry, and particularly relates to a method and an apparatus for high-efficient crude oil desalination / dehydration by a combined filtration-electric field coalescence method. The apparatus for high-efficient crude oil desalination / dehydration of the invention comprises a raw material conveying system, a mixing device, a dehydration filtration device, and an electrical desalting device which are connected in order. The method for high-efficient crude oil desalination / dehydration of the invention is realized by using the apparatus for high-efficient crude oil desalination / dehydration of the invention and through the steps of raw material preheating, mixing, preliminary demulsification, and electrical desalination / dehydration. The invention adopts a combined filtration-electric field coalescence method for crude oil desalination / dehydration, which can overcome respective disadvantages of performing desalination / dehydration process by a filtration method or an electric field coalescence method, decrease running severity of both the two methods, not only improves the adaptability of the crude oil desalination process, the desalination / dehydration rate, and the stable running rate, but also reaches the purposes of energy saving and consumption reduction.
Owner:GUANGZHOU BOXENERGY TECH

Coal tar pretreatment method

The invention discloses a coal tar pretreatment method. The method comprises the following steps: 1, fully mixing a coal tar raw material with water, salt and a de-emulsifier A, and using an oil-water separation device to separate the coal tar raw material at 50-200 DEG C under 0.1-5.0 Mpa into oil above water, water and oil under water, wherein the addition amount of water is 5-50% of the weight of the coal tar raw material, the addition amount of the de-emulsifier A is 0.003-0.05% of the weight of the coal tar raw material, and the addition amount of the salt makes the density of the salt in water reach 1.001-1.015 g / cm<3>; 2, treating the oil above water obtained in step 1 to obtain refined coal tar I; 3, treating the oil under water obtained in the step 1 to obtain standing coal tar II; and 4, mixing the refined coal tar I obtained in step 2 with the standing coal tar II obtained in step 3 to obtain refined coal tar, adding the refined coal tar to a distillation system, separating to obtain a fraction with the boiling point being smaller than 150 DEG C and a fraction with the boiling point being greater than 150 DEG C, and mixing a part of the fraction with the boiling point being smaller than 150 DEG C with the fraction with the boiling point being greater than 150 DEG C to obtain pretreated coal tar.
Owner:特思锐能源科技(北京)有限责任公司

Process method for treating residual oil

ActiveCN106701192AImproved ability to remove/accommodate metalsDoes not limit the operating cycleTreatment with hydrotreatment processesFractionationSlurry
The invention discloses a process method for treating residual oil. A hydrogenation pretreatment unit, a coking device, a hydrogenation treatment unit and a catalytic cracking device are provided; the hydrogenation pretreatment unit comprises a hydrogenation pretreatment reaction area and a hydrogenation treatment reaction area; the process method comprises the following steps: performing a reaction on a residual oil raw material by using the hydrogenation pretreatment unit, and performing oil fractionation so as to obtain light fraction and heavy fraction, feeding the heavy fraction into the coking device for treatment so as to obtain coked gasoline, coked diesel oil and coked wax oil, mixing the light fraction with the coked wax oil and hydrogen, passing through the hydrogenation pretreatment reaction area and the hydrogenation treatment reaction area which are connected in series, performing gas-liquid separation on a reaction effluent of the hydrogenation treatment reaction area, circulating vapor phase back to the hydrogenation pretreatment reaction area and/or the hydrogenation treatment reaction area, directly feeding liquid phase into the catalytic cracking reaction area for a catalytic cracking reaction, and separating a catalytic cracking reaction effluent, thereby obtaining a dry gas, a liquefied gas, catalytic cracking gasoline fraction, catalytic cracking area diesel oil fraction, catalytic cracking area recirculation oil and catalytic cracking area oil slurry. Due to adoption of the process method disclosed by the invention, the stable operation period of a device can be prolonged.
Owner:CHINA PETROLEUM & CHEM CORP +1

Method for lightening residual oil

The invention discloses a method for lightening residual oil. According to the method, residual oil raw materials goes through a hydrotreatment device, and the obtained hydrogenated oil undergoes flash evaporation to obtain light components and heavy components; the heavy components enters a reduced pressure distillation device to separate out reduced pressure wax oil, and the reduced pressure wax oil which is mixed with the hydrogenated light components enters a catalytic cracking device and undergoes fractionation to obtain a gas, gasoline and diesel oil which are discharged form the catalytic cracking device and recycle oil and oil slurry which are returned to the hydrotreatment device; and reduced pressure residual oil obtained by the reduced pressure distillation device enters a delayed coking device and undergoes the fractionation to obtain a gas, gasoline and a diesel oil fraction which are discharged from the delayed coking device and coked wax oil and tail oil which are returned to the hydrotreatment device. The method which combines the residual oil hydrotreatment, the catalytic cracking, the reduced pressure distillation and above delayed coking technology allows charged material compositions of the residual hydrogenation, the catalytic cracking and the delayed coking to be optimized, and target product yields of the catalytic cracking and the delayed coking to be improved.
Owner:CHINA PETROLEUM & CHEM CORP +1

Technological method for transferring hydrogenation for sec-butyl acetate by secondary butyl alcohol and simultaneously producing methyl ethyl ketone

The invention relates to a technological method for transferring hydrogenation for sec-butyl acetate by sec-butyl alcohol and simultaneously producing methyl ethyl ketone. According to the method, the composition of sec-butyl alcohol and sec-butyl acetate is taken as a raw material, the transferring hydrogenation for sec-butyl acetate by sec-butyl alcohol is realized under the effect of a hydrogenation catalyst, and the sec-butyl alcohol is dehydrogenized, so that the methyl ethyl ketone is obtained, the sec-butyl acetate is subjected to transferring hydrogenation, so as to produce the sec-butyl alcohol and ethyl alcohol; the produced sec-butyl alcohol is dehydrogenized, so that the methyl ethyl ketone is obtained. A product is subjected to gas-liquid separation, high-purity hydrogen is obtained, and a liquid product is subjected to distillation separation firstly, so that the composition of ethyl alcohol and methyl ethyl ketone is obtained, and the sec-butyl alcohol or the composition of the sec-butyl alcohol and the sec-butyl acetate in a column reactor returns a transferring hydrogenation reactor, so as to be reacted continuously; the composition of ethyl alcohol and the methyl ethyl ketone is subjected to extractive distillation firstly, so that a high-purity methyl ethyl ketone product is obtained, an extraction agent containing ethyl alcohol in the column reactor is rectified again, a high-purity ethyl alcohol product is obtained, and the extraction agent in the column reactor returns an extractive distillation column to be recycled. The method solves the problems that the sec-butyl acetate and the sec-butyl alcohol are azeotropic and high-purity sec-butyl alcohol and methyl ethyl ketone cannot be obtained.
Owner:九江齐鑫化工有限公司 +2

Method for treating residual oil

ActiveCN106701187AImproved ability to remove/accommodate metalsDoes not limit the operating cycleTreatment with hydrotreatment processesFractionationSlurry
The invention discloses a method for treating residual oil. A coking device, a hydrogenation pretreatment reaction area, a hydrogenation treatment reaction area and a catalytic cracking reaction area are provided, the method comprises the following steps: performing fractionation on a residual oil raw material so as to obtain light fraction and heavy fraction, feeding the heavy fraction into the coking device for treatment so as to obtain coked gasoline, coked diesel oil and coked wax oil, mixing the light fraction with the coked wax oil and hydrogen, passing through the hydrogenation pretreatment reaction area and the hydrogenation treatment reaction area which are connected in series, performing gas-liquid separation on a reaction effluent of the hydrogenation treatment reaction area, circulating vapor phase back to the hydrogenation pretreatment reaction area and/or the hydrogenation treatment reaction area, directly feeding liquid phase into the catalytic cracking reaction area for a catalytic cracking reaction, and separating a catalytic cracking reaction effluent, thereby obtaining a dry gas, a liquefied gas, catalytic cracking gasoline fraction, catalytic cracking area diesel oil fraction, catalytic cracking area recirculation oil and catalytic cracking area oil slurry. By adopting the method disclosed by the invention, the stable operation period of a device can be prolonged.
Owner:CHINA PETROLEUM & CHEM CORP +1

Method for reducing viscosity of heavy oil

InactiveCN108587675AReduce tendency to polymerize and cokePromote coke formationCatalytic crackingCatalyst activation/preparationOil processingIsomerization
The invention discloses a method for reducing the viscosity of heavy oil and belongs to the technical field of petroleum processing. The method comprises the steps: contacting a heavy oil component with a catalyst with an alkaline carrier without silicon and aluminum elements in a viscosity reducing reactor, and carrying out cracking, isomerization, de-coagulation and viscosity reduction under thecondition of an oxygen-free and / or reducing atmosphere, wherein the process conditions are that the reaction temperature is 300-550 DEG C, the reaction pressure if 0.01-6.0Mpa, and the reaction timeis 0.1-5.0h. The viscosity of the heavy oil can be remarkably reduced, and a heavy oil fuel or heavy oil can provide a raw material for further processing and producing oil and gas products after theviscosity is reduced. A heavy oil viscosity reducing and cracking catalyst with the alkaline carrier without silicon and aluminum is adopted due to the polymerization coke generation promoting effectof an acidic catalyst and a polymerization coke generation inhibiting effect of an alkaline catalyst, viscosity reduction is carried out under the condition of the oxygen-free and / or reducing atmosphere, and therefore, on one hand, the polymerization coke generation tendency of a reaction product can be reduced under the condition of deep viscosity reduction, and on the other hand, the operation severity can be reduced when the relatively deep viscosity reducing effect is achieved.
Owner:HIGH TECH RES INST NANJING UNIV LIANYUNGANG

Heavy oil product treatment processing method

ActiveCN106701188AImproved ability to remove/accommodate metalsDoes not limit the operating cycleTreatment with hydrotreatment processesHydrocarbon oils treatment productsGas phaseSlurry
The invention discloses a heavy oil product treatment processing method. The method comprises a hydrogenation pretreatment device, a solvent deasphalting device, a hydrogenation treatment device and a catalytic cracking device, wherein the hydrogenation treatment device comprises a hydrogenation pretreatment reaction area and a hydrogenation treatment reaction area; the processing method comprises the following steps: residual oil raw material generated oil is subjected to fractional distillation after being reacted through a hydrogenation pretreatment unit to obtain light fraction and heavy fraction, wherein the heavy fraction is treated after entering the solvent deasphalting device so as to obtain deasphalted oil and deoiled asphalt, and the light fraction orderly passes through the hydrogenation pretreatment reaction area and the hydrogenation treatment reaction area which are in series connection after mixing with the deasphalted oil and hydrogen; gas-liquid separation is performed on reaction effluent of the hydrogenation treatment reaction area, and a gas phase is recycled back to the hydrogenation pretreatment reaction area and/or the hydrogenation treatment reaction area; a liquid phase directly enters a catalytic cracking reaction area to perform catalytic cracking reaction, and effluent of the catalytic cracking reaction is separated to obtain dry gas, liquefied gas, catalytic-cracked gasoline fraction, catalytic-cracked diesel fraction, catalytic-cracked heavy cycle oil and catalytic-cracked oil slurry. The stable operation period of the device can be prolonged by use of the method disclosed by the invention.
Owner:CHINA PETROLEUM & CHEM CORP +1

Process method for simultaneous production of methyl ethyl ketone by transfer hydrogenation of sec-butyl alcohol to sec-butyl acetate

The invention relates to a technological method for transferring hydrogenation for sec-butyl acetate by sec-butyl alcohol and simultaneously producing methyl ethyl ketone. According to the method, the composition of sec-butyl alcohol and sec-butyl acetate is taken as a raw material, the transferring hydrogenation for sec-butyl acetate by sec-butyl alcohol is realized under the effect of a hydrogenation catalyst, and the sec-butyl alcohol is dehydrogenized, so that the methyl ethyl ketone is obtained, the sec-butyl acetate is subjected to transferring hydrogenation, so as to produce the sec-butyl alcohol and ethyl alcohol; the produced sec-butyl alcohol is dehydrogenized, so that the methyl ethyl ketone is obtained. A product is subjected to gas-liquid separation, high-purity hydrogen is obtained, and a liquid product is subjected to distillation separation firstly, so that the composition of ethyl alcohol and methyl ethyl ketone is obtained, and the sec-butyl alcohol or the composition of the sec-butyl alcohol and the sec-butyl acetate in a column reactor returns a transferring hydrogenation reactor, so as to be reacted continuously; the composition of ethyl alcohol and the methyl ethyl ketone is subjected to extractive distillation firstly, so that a high-purity methyl ethyl ketone product is obtained, an extraction agent containing ethyl alcohol in the column reactor is rectified again, a high-purity ethyl alcohol product is obtained, and the extraction agent in the column reactor returns an extractive distillation column to be recycled. The method solves the problems that the sec-butyl acetate and the sec-butyl alcohol are azeotropic and high-purity sec-butyl alcohol and methyl ethyl ketone cannot be obtained.
Owner:九江齐鑫化工有限公司 +2

A method for treating residual oil

ActiveCN106701187BImproved ability to remove/accommodate metalsDoes not limit the operating cycleTreatment with hydrotreatment processesFractionationSlurry
The invention discloses a method for treating residual oil. A coking device, a hydrogenation pretreatment reaction area, a hydrogenation treatment reaction area and a catalytic cracking reaction area are provided, the method comprises the following steps: performing fractionation on a residual oil raw material so as to obtain light fraction and heavy fraction, feeding the heavy fraction into the coking device for treatment so as to obtain coked gasoline, coked diesel oil and coked wax oil, mixing the light fraction with the coked wax oil and hydrogen, passing through the hydrogenation pretreatment reaction area and the hydrogenation treatment reaction area which are connected in series, performing gas-liquid separation on a reaction effluent of the hydrogenation treatment reaction area, circulating vapor phase back to the hydrogenation pretreatment reaction area and / or the hydrogenation treatment reaction area, directly feeding liquid phase into the catalytic cracking reaction area for a catalytic cracking reaction, and separating a catalytic cracking reaction effluent, thereby obtaining a dry gas, a liquefied gas, catalytic cracking gasoline fraction, catalytic cracking area diesel oil fraction, catalytic cracking area recirculation oil and catalytic cracking area oil slurry. By adopting the method disclosed by the invention, the stable operation period of a device can be prolonged.
Owner:CHINA PETROLEUM & CHEM CORP +1

Method and apparatus for high-efficient crude oil desalination / dehydration

The invention belongs to the technical field of petrochemical industry, and particularly relates to a method and an apparatus for high-efficient crude oil desalination / dehydration by a combined filtration-electric field coalescence method. The apparatus for high-efficient crude oil desalination / dehydration of the invention comprises a raw material conveying system, a mixing device, a dehydration filtration device, and an electrical desalting device which are connected in order. The method for high-efficient crude oil desalination / dehydration of the invention is realized by using the apparatus for high-efficient crude oil desalination / dehydration of the invention and through the steps of raw material preheating, mixing, preliminary demulsification, and electrical desalination / dehydration. The invention adopts a combined filtration-electric field coalescence method for crude oil desalination / dehydration, which can overcome respective disadvantages of performing desalination / dehydration process by a filtration method or an electric field coalescence method, decrease running severity of both the two methods, not only improves the adaptability of the crude oil desalination process, the desalination / dehydration rate, and the stable running rate, but also reaches the purposes of energy saving and consumption reduction.
Owner:GUANGZHOU BOXENERGY TECH
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