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167results about "Phosphatic fertiliser granulation/pelletisation" patented technology

Method for producing fertilizer grade DAP having an increased nitrogen concentration from recycle

A process for the preparation of granular fertilizer grade DAP (a product composed of ammonium phosphates, principally diammonium phosphate, resulting from the ammoniation of phosphoric acid, as defined in Official Publication No. 52 of the Association of American Plant Food Officials, dated 1999) comprising partially preneutralizing orthophosphoric acid with ammonia, completing the ammoniation of the orthophosphoric acid with ammonia in a rotary ammoniator-granulator to provide granular DAP, sizing the granular DAP to provide the granular DAP product, reducing the particle size of the oversized granular DAP, and recycling the undersized granular DAP and the sized-reduced oversized granular DAP to the ammoniator-granulator. The ammoniacal nitrogen concentration of the granular DAP recycle, hence the granular DAP product, is enhanced by subjecting the finely-divided recycled granular DAP to anhydrous gaseous ammonia which is at a super atmospheric pressure and which is at a temperature sufficient to maintain said anhydrous ammonia in the gaseous state. The increase in the ammoniacal nitrogen concentration is a function of the absolute ammonia pressure, the initial moisture content of the granular DAP recycle, and the contact time of the ammonium with the granular DAP recycle.
Owner:THE MOSAIC COMPANY

Method and apparatus used for preparing ammonium phosphate fertilizer from phosphoric acid sediment

InactiveCN103435376ASimplify the process of filter press washingPhosphatesAlkali orthophosphate fertiliserO-Phosphoric AcidGaseous ammonia
The invention discloses a method and an apparatus used for preparing ammonium phosphate fertilizer from phosphoric acid sediment. The method comprises following steps: the phosphoric acid sediment with a P2O5 content of 30 to 35% is mixed with diluted phosphoric acid with a concentration of 18 to 20% so as to obtain intermediate mixture I with a phosphoric acid content of 20 to 25%; the intermediate mixture I and gaseous ammonia with a concentration of 99% are subjected to neutralization reaction at a N mole/P mole ratio of 1.3-1.35, and a certain amount of sulfuric acid is added so as to neutralize unreacted gaseous ammonia; the N mole/P mole ratio is increased to 1.4-1.45 so as to obtain intermediate mixture II; and the intermediate mixture II is subjected to condensation, granulation and screening treatment. Gaseous ammonia is used for neutralizing the intermediate mixture I with a phosphoric acid content of 21 to 25%, ammonium bicarbonate or liquid ammonia are not used, and reaction contact area and reaction speed of gaseous ammonia and the intermediate mixture I are enlarged and increased respectively, so that filter-pressing washing process of the phosphoric acid sediment is simplified, comprehensive utilization of the phosphoric acid sediment is realized, and the quality of the ammonium phosphate products is improved.
Owner:山东明瑞化工集团有限公司
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