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42results about How to "Shade stability" patented technology

Synthesis method of black active dyestuff compound

The invention relates to a synthesis method of a black active dyestuff compound and belongs to the field of dyestuff chemistry. The synthesis method comprises the following steps: preparing a raw material A shown as a formula 1 into a first coupling solution; preparing a raw material B shown as a formula 2 into second diazonium salt and preparing the second diazonium salt, a raw material C shown as a formula 3 and a raw material D shown as a formula 4 into a second coupling solution under the condition that baking soda is added; mixing the first coupling solution and the second coupling solution; carrying out third coupling reaction and drying to obtain the black active dyestuff compound. The synthesis method of the black active dyestuff compound, provided by the invention has comprehensive advantages in the aspects of equipment, manpower, reaction time, product quality and the like when being compared with a former technology; the reaction time is greatly shortened to 8h to 14h; a synthesized black dyestuff has stable quality and good reproducibility; the yield of a product is 2 percent to 3 percent higher than that of a former mixture technology; reaction steps are reduced so that the occupied rate of reaction equipment is low; meanwhile, post-treatment procedures and equipment are saved, so that the defects of more mixture reaction equipment and great blending working amount are overcome.
Owner:SHANGHAI WANDE CHEM

Method for enhancing alkali resistance and oxidation resistance of benzothiazole disperse dyes

The invention discloses a method for enhancing alkali resistance and oxidation resistance of benzothiazole disperse dyes, and belongs to the field of disperse dyes. According to the method, four diazocomponents and eight coupling components are adopted to design and synthesize 28-branch thiazole heterocyclic azo disperse dyes, so that the alkali resistance and the oxidation resistance of the disperse dyes are enhanced. The synthesized disperse dyes are subjected to structure confirmation, and the alkali resistance, the oxidation resistance and other dyeing properties of the disperse dyes aretested. According to the method for enhancing the alkali resistance and the oxidation resistance of the benzothiazole disperse dyes, the relationship between the dye structure and the alkali resistance and the oxidation resistance is clear, the disperse dyes with excellent alkali resistance and oxidation resistance are obtained, and the dyeing property is stable under the dyeing condition of 10g/Lsodium hydroxide or 5g/L hydrogen peroxide. The dyes can be applied to bleaching and dyeing one bath of polyester cotton and decrement dyeing one bath of polyester, short-process dyeing and finishingprocessing is achieved, and huge ecological benefits and economic benefits are generated.
Owner:QINGDAO UNIV +1
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