The invention discloses a continuous preparation and purification device for
graphene oxide, which includes a reactor, a concentrated
sulfuric acid solution storage
bottle and a water /
hydrogen peroxide storage
bottle connected to the reactor through a delivery
pipe, and a three-way valve is arranged on the delivery
pipe. Directly below and directly above are correspondingly equipped with an ultrasonic plate, a feeder, a stirring
paddle, and a first lifting platform connected to the reactor through a
discharge pipe, and the
discharge pipe is connected to the filter column through a second conveying pipe provided with a second
peristaltic pump. The filter column is connected to the
graphene oxide storage
bottle through the third conveying pipe provided with the third
peristaltic pump; the invention also discloses a preparation method of
graphene oxide: the strong acid and the oxidant are separately fed and oxidized with
graphite, and then stripped and purification to obtain graphene oxide. The device of the present invention is provided with a concentrated
sulfuric acid solution storage bottle, a feeder, a reactor and a filter, and realizes the continuous preparation and purification of graphene oxide; the method of the present invention improves the preparation and purification efficiency of graphene oxide, and realizes concentrated
sulfuric acid Solution
recovery and continuous utilization.