The invention discloses a preparation method of a purple sweet potato
pigment. The method comprises the following steps: performing cleaning, airing and
cutting. taking an
acetic acid aqueous solutionas an extracting agent, carrying out crude extraction according to a
solid-
liquid ratio of 1: 4, carrying out
freeze thawing treatment on the purple sweet potato strips twice, combining
pigment crudeextracts, and carrying out vacuum concentration to obtain a
pigment concentrated solution; treating the pigment concentrated solution with a
graphene oxide dispersion solution, carrying out primary purification, and carrying out
centrifugal separation to obtain supernatant; pre-treating and packing adsorption
macroporous resin SP70 into a column, and injecting a supernate pigment liquid into a resin layer, wherein the sample loading flow rate is 3.0-3.5 BV / h; washing the resin layer after adsorption saturation with 2BV clear water, wherein an eluent is prepared from 70%
ethanol and 0.5%
acetic acid, the
elution flow rate is 2.0-2.5 BV / h, and the
elution volume is 5BV; and collecting eluate, and performing vacuum concentrating and freeze-
drying to obtain a purple sweet potato
anthocyanin pigment dry product. According to the method, an
alcohol solvent is not used, the pigment extraction rate is increased through
freeze thawing treatment, impurities such as proteins are removed throughthe
adsorption effect of
graphene oxide in the purification process, the
anthocyanin complexing effect is avoided, the purification effect is improved, and the high-purity purple sweet potato
anthocyanin pigment is obtained.