The invention discloses a double-
tower purification process for
nitrous oxide, and relates to the technical field of
nitrous oxide purification. The process comprises the following steps: S1:
raw material preparation, wherein the
nitrous oxide raw material is passed through a filtering device to filter out
solid impurities, so as to obtain a
raw material liquid; S2: low-boiling separation, wherein the raw material liquid is transported from a feed
pipe to the inside of a first
distillation tower through a compressor, and impurities in the raw material liquid with a
boiling point lower than that of nitrous
oxide are separated to obtain a primary separation stock liquid; S3: high-boiling separation, wherein the primary separation stock liquid is transported from the first
distillation tower to the inside of a second
distillation tower, and impurities in the primary separation stock liquid with a
boiling point higher than that of nitrous
oxide are separated to obtain a nitrous
oxide liquid. The invention replaces an adsorption tower with a distillation tower, thereby not only reducing the replacement and maintenance costs of an adsorbent, but also greatly reducing the equipment complexity of a nitrous oxide purification
system, and also making both the nitrous oxide raw material and the final product liquid, which is convenient for storage and transportation.