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39results about How to "High resistance reduction rate" patented technology

Resistance reducing agent for fracture and preparation method thereof

ActiveCN104974308AChange spatial configurationHydration Swelling InhibitionDrilling compositionSolubilityDouble bond
The invention relates to a preparation method of a resistance reducing agent for fracture. The preparation method includes the steps of: (1) mixing an acrylamide-series monomer, a cationic monomer containing a double bond, an anionic polymer template, a chelating agent and a molecular weight regulating agent with water with pH value being regulated to obtain a water solution of which the pH value is 3-5; (2) contacting an organic solvent with an emulsification agent to obtain an oil solution; (3) contacting the water solution with the oil solution to obtain a water-in-oil emulsion; and (4) under an inert atmosphere, contacting the water-in-oil emulsion with an initiator in batches, performing a polymerization reaction to obtain a mixture, and contacting the mixture with a phase conversion agent. The emulsification agent is 4-6 in hydrophilic-lipophilic balance value, the molecular weight of the anionic polymer template is less than 800000, and the structure formula of the anionic polymer template is represented as the formula (I). The invention also relates to the resistance reducing agent for fracture prepared through the method. The resistance reducing agent for fracture is high in resistance reducing rate, is high in inhibition on clay expansion, is good in water solubility and is low in formation damage property.
Owner:CHINA PETROLEUM & CHEM CORP +1

Method for volume acid-fracturing reformation of seam net of carbonate reservoir

The invention provides a method for volume acid-fracturing reformation of a seam net of a carbonate reservoir. The method specifically comprises the following steps: (1) injecting low-viscose resistance-reducing sliding acid liquor, performing plunger injection for at least three times and performing volume fracturing reformation of the seam net; (2) injecting a water-based sand-carrying fracturing fluid and forming sand-filling cracks in length not less than 120 meters on the two sides of a well shaft; (3) injecting a displacement fluid, closing the well and then draining the liquid, wherein the low-viscose resistance-reducing sliding acid liquor is composed of 5-20% of acid, 1-3% of alkyl quaternary ammonium salt, 0.5-2% of sodium ascorbate, 0.1-0.5% of emulsion corrosion inhibitor, 0.5-1% of citric acid, 1-3% of discharge aiding agent and the balance of water; the emulsion corrosion inhibitor is selected from any one of polypropylene glycol emulsion, polyvinylpyrrolidone emulsion, acrylamide and 2-crylic acid-2-methallyl sulfonate copolymer emulsion; and the acid is selected from hydrochloric acid, formic acid, acetic acid or bionic acid. The method is simple in construction, the flow conductivity of the seam net is high and the yield-increasing effect is excellent.
Owner:RES INST OF SHAANXI YANCHANG PETROLEUM GRP

Resistance reducing agent for fracture and preparation method thereof

ActiveCN104974299AChange spatial configurationChange the spatial structureDrilling compositionSolubilityDouble bond
The invention relates to a preparation method of a resistance reducing agent for fracture. The preparation method includes the steps of: (1) mixing an acrylamide monomer, a nonionic-series monomer having a hydroxyl group and containing a double bond, a polyhydroxyl nonionic polymer template, a chelating agent and a molecular weight regulating agent with water to obtain a water solution; (2) contacting an organic solvent with an emulsification agent to obtain an oil solution; (3) contacting the water solution with the oil solution to obtain a water-in-oil emulsion; and (4) under an inert atmosphere, contacting the water-in-oil emulsion with an initiator in batches, performing a polymerization reaction to obtain a mixture, and contacting the mixture with a phase conversion agent. The emulsification agent is 4-6 in hydrophilic-lipophilic balance value, the molecular weight of the polyhydroxyl nonionic polymer template is less than 500000, and the structure formula of the polyhydroxyl nonionic polymer template is represented as the formula (I) or the formula (II). The invention also relates to the resistance reducing agent for fracture prepared through the method. The resistance reducing agent for fracture is high in resistance reducing rate, is high in inhibition on clay expansion, is good in water solubility and is low in formation damage property.
Owner:CHINA PETROLEUM & CHEM CORP +1

Crude oil composite demulsifier and preparation method thereof

The invention discloses a crude oil composite demulsifier and a preparation method thereof; the demulsifier comprises the following substances: 1000 parts of water, 40 to 50 parts of triethanolamine;350 to 450 parts of epoxypropane, 250 to 400 parts of ethylene oxide, 80 to 100 parts of acrylic acid, 50 to 60 parts of sulfonic acid perfluoroalkyl surfactant, 70 to 120 parts of alkyl alcohol polyoxyethylene ether sulfonate, 50 to 100 parts of citrate, 10 to 60 parts of inorganic base and 300 to 400 parts of organic solvent. The preparation method comprises the following steps: sequentially adding triethanolamine, propylene oxide and ethylene oxide for copolymerization to generate polyether, adding acrylic acid for reaction to obtain modified polyether, and dissolving the modified polyetherin an organic solution for later use; sequentially adding citrate, a sulfonic acid perfluoroalkyl surfactant and alkyl alcohol polyoxyethylene ether sulfonate into water; and adding the modified polyether solution into the mixed solution, adding inorganic base, and continuously stirring. The crude oil composite demulsifier provided by the invention not only has good demulsification performance oncrude oil, but also can provide good viscosity reduction performance and resistance reduction performance.
Owner:王达 +1

A kind of drag reducing agent for fracturing and preparation method thereof

ActiveCN104974308BChange spatial configurationHydration Swelling InhibitionDrilling compositionSolubilityPolymer science
The invention relates to a preparation method of a drag reducing agent for fracturing, comprising: mixing an acrylamide monomer, a cationic monomer containing a double bond, an anionic polymer template, a chelating agent, a molecular weight regulator and water and adjusting the pH value , to obtain an aqueous solution with a pH value of 3-5; the organic solvent is contacted with an emulsifier to obtain an oil solution; the aqueous solution is contacted with the oil solution to obtain a water-in-oil emulsion; under an inert atmosphere, the oil-in- The aqueous emulsion is contacted with the initiator in batches, and a polymerization reaction is carried out, and then the mixture obtained by the polymerization reaction is contacted with a phase inversion agent; wherein, the hydrophilic-lipophilic balance value of the emulsifier is 4-6, and the anionic polymer The molecular weight of the template is less than 800,000, and the structural formula of the anionic polymer template is shown in formula (I), and also relates to a drag reducing agent for fracturing prepared by the above method. The drag-reducing agent for fracturing prepared by the invention has high drag-reducing rate, high clay swelling inhibition, good water solubility and low stratum damage.
Owner:CHINA PETROLEUM & CHEM CORP +1

Multifunctional reversed-phase suspension resistance reducing agent system for shale gas factory-like sand fracturing fluid

PendingCN114686197AThe effect of reducing friction is goodHigh kinematic viscosityDrilling compositionHexamethylenetetramineActive agent
The invention relates to the technical field of resistance reducing agents, and discloses a multifunctional reversed-phase suspension resistance reducing agent system for shale gas factory-like sand fracturing fluid, which comprises an oil phase, a water-soluble monomer, a suspending agent, an initiator, a surfactant A, a surfactant B, a cleanup additive, an anti-swelling agent and clear water, the surfactant A is one or a composition of more of nonylphenol polyoxyethylene ether, span 80 and Tween; the surfactant B is one or a composition of more of alkylaryl polyoxyethylene ether and 12-hydroxystearic acid-polyoxyethylene ether; the surfactant B is one or a composition of more of alkylaryl polyoxyethylene ether and 12-hydroxystearic acid-polyoxyethylene ether; the discharge aiding agent is organic fluorocarbon; the anti-swelling agent is hexamethylenetetramine ammonium chloride. The scheme has the beneficial effects that the resistance reducing agent prepared by adopting a reversed-phase suspension polymerization method is quick in dispersion and dissolution time in water, high in viscosity and low in friction resistance, and can effectively reduce the friction resistance of fracturing construction, reduce the pumping pressure of construction and reduce the safety risk of construction at the same time; the system has discharge aiding and anti-swelling performance, and a discharge aiding agent and an anti-swelling agent do not need to be additionally pumped through a fracturing blender truck during construction.
Owner:四川川庆井下科技有限公司

A kind of drag reducing agent for fracturing and preparation method thereof

ActiveCN104974737BChange spatial configurationHydration Swelling InhibitionDrilling compositionSolubilityDouble bond
The invention relates to a preparation method of a resistance reducing agent for fracture. The preparation method includes the steps of: (1) mixing an acrylamide-series monomer, an anionic monomer containing a double bond, a cationic polymer template, a chelating agent and a molecular weight regulating agent with water with pH value being regulated to obtain a water solution of which the pH value is 6-9; (2) contacting an organic solvent with an emulsification agent to obtain an oil solution; (3) contacting the water solution with the oil solution to obtain a water-in-oil emulsion; and (4) under an inert atmosphere, contacting the water-in-oil emulsion with an initiator in batches, performing a polymerization reaction to obtain a mixture, and contacting the mixture with a phase conversion agent. The emulsification agent is 4-6 in hydrophilic-lipophilic balance value, the molecular weight of the anionic polymer template is less than 1000000, and the structure formula of the anionic polymer template is represented as the formula (I). The invention also relates to the resistance reducing agent for fracture prepared through the method. The resistance reducing agent for fracture is high in resistance reducing rate, is high in inhibition on clay expansion, is good in water solubility and is low in formation damage property.
Owner:CHINA PETROLEUM & CHEM CORP +1

A Method for Volumetric Acid Fracturing of Carbonate Reservoir Fracture Network

The invention provides a method for volume acid-fracturing reformation of a seam net of a carbonate reservoir. The method specifically comprises the following steps: (1) injecting low-viscose resistance-reducing sliding acid liquor, performing plunger injection for at least three times and performing volume fracturing reformation of the seam net; (2) injecting a water-based sand-carrying fracturing fluid and forming sand-filling cracks in length not less than 120 meters on the two sides of a well shaft; (3) injecting a displacement fluid, closing the well and then draining the liquid, wherein the low-viscose resistance-reducing sliding acid liquor is composed of 5-20% of acid, 1-3% of alkyl quaternary ammonium salt, 0.5-2% of sodium ascorbate, 0.1-0.5% of emulsion corrosion inhibitor, 0.5-1% of citric acid, 1-3% of discharge aiding agent and the balance of water; the emulsion corrosion inhibitor is selected from any one of polypropylene glycol emulsion, polyvinylpyrrolidone emulsion, acrylamide and 2-crylic acid-2-methallyl sulfonate copolymer emulsion; and the acid is selected from hydrochloric acid, formic acid, acetic acid or bionic acid. The method is simple in construction, the flow conductivity of the seam net is high and the yield-increasing effect is excellent.
Owner:RES INST OF SHAANXI YANCHANG PETROLEUM GRP

A drag reducing agent for fracturing and its preparation method

ActiveCN104974299BChange spatial configurationChange the spatial structureDrilling compositionSolubilityDouble bond
The invention relates to a preparation method of a resistance reducing agent for fracture. The preparation method includes the steps of: (1) mixing an acrylamide monomer, a nonionic-series monomer having a hydroxyl group and containing a double bond, a polyhydroxyl nonionic polymer template, a chelating agent and a molecular weight regulating agent with water to obtain a water solution; (2) contacting an organic solvent with an emulsification agent to obtain an oil solution; (3) contacting the water solution with the oil solution to obtain a water-in-oil emulsion; and (4) under an inert atmosphere, contacting the water-in-oil emulsion with an initiator in batches, performing a polymerization reaction to obtain a mixture, and contacting the mixture with a phase conversion agent. The emulsification agent is 4-6 in hydrophilic-lipophilic balance value, the molecular weight of the polyhydroxyl nonionic polymer template is less than 500000, and the structure formula of the polyhydroxyl nonionic polymer template is represented as the formula (I) or the formula (II). The invention also relates to the resistance reducing agent for fracture prepared through the method. The resistance reducing agent for fracture is high in resistance reducing rate, is high in inhibition on clay expansion, is good in water solubility and is low in formation damage property.
Owner:CHINA PETROLEUM & CHEM CORP +1
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