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93 results about "Calcium/Sodium" patented technology

Method for preparing probiotic microcapsules by using electrostatic spraying

The invention discloses a method for preparing probiotic microcapsules by using electrostatic spraying. Sodium alga acid and gelatin are taken as wall materials, probiotic suspension or microporous starch-adsorbed probiotics are taken as core materials, and calcium chloride is taken as solidifying solution. The method comprises the following steps of: a) mixing 1.5 percent solution of sodium alga acid and 1 percent gelatin in the same volume, and uniformly mixing with the probiotic suspension or microporous starch-adsorbed probiotics to form mixed solution; b) putting the mixed solution into a container, and injecting the mixed solution into 2 to 3 percent continuously stirred solution of calcium sodium chloride in the electrostatic spraying mode by using a microcapsule molding device to form microcapsules; c) standing and solidifying the encapsulated probiotic microcapsules for 20 minutes in the solution of calcium chloride, and filtering and cleaning the solution by using physiological saline; and d) saving the probiotic microcapsules in the physiological saline. The prepared microcapsules have the advantages of uniform grain diameter, good encapsulation performance, simple process, readily available wall materials, and low cost, and can be widely applied to the fields of food processing, biomedicines, chemical industry, and the like.
Owner:UNIV OF SHANGHAI FOR SCI & TECH

Multifunctional adsorption particles capable of treating industrial organic wastewater with imbalance of nitrogen and phosphorus and preparation method thereof

InactiveCN103611514AHas the function of slow-release nitrogen and phosphorusSimple preparation processOther chemical processesWater/sewage treatment by sorptionSorbentNitric acid
The invention discloses multifunctional adsorption particles capable of treating industrial organic wastewater with imbalance of nitrogen and phosphorus and a preparation method thereof. The preparation method comprises the steps of preparing a mixed solution F from a NH4HCO3 solution, a Ca(NO3)2 solution, a (NH4)2HPO4 solution, a NaOH solution, a nitric acid solution, a urea water solution and an ethylenediaminetetraacetic acid calcium sodium solution; preparing a mixed solution L from urea and a formaldehyde water solution; preparing a mixed solution M from a styrene chloroform solution, a divinyl benzene chloroform solution and an azobisisobutyronitrile chloroform solution; dropping the mixed solution L into the mixed solution M to obtain a mixed solution N; dropping the mixed solution F into the mixed solution N to obtain a mixed solution O; dropping the mixed solution O into a polyvinyl alcohol solution to obtain a mixed solution P; adding the polyvinyl alcohol solution into the mixed solution P, and performing centrifugal separation to obtain the multifunctional adsorption particles capable of treating the industrial organic wastewater with imbalance of nitrogen and phosphorus. The preparation process disclosed by the invention is simple, and a prepared multifunctional adsorbent has the function of nitrogen and phosphorus sustained release and the function of adsorbing pollutants in industrial organic wastewater.
Owner:BEIJING NORMAL UNIVERSITY

Method for preparing series titanium-iron alloy by smelting titanium raw material

A method to produce a series of ferrotitanium by smelting the titanium material in Panxi area. The technology steps are as following: the titanium material in Panxi area, calcareous metallurgy accessories and calcium-sodium treatment reagent will be delivered into the revolving burner, they will be warm-up fast, and then will be delivered into blendor by connecting barn to be uniformly mixed. And then aluminium, iron system material, auxiliary reducers and potassium chlorate will be orderly added in from the batch bin, when the material and the auxiliary material in the blendor have been uniformly mixed, they will drop into the smelting furnace, which has been warmed up, by the connecting barn, the igniter will be added in, and the inhibiting agent will be added when the reaction get over for about 2-3 minutes, they will be cooled for 20-40h, and at last the residue and the ferrotitanium will be separated. The ferrotitanium product will enter warehouse after being checked and paclaged. The material source of this patent is assured, and the production technology is on the safe side, the product quality of the ferrotitanium made by it is stable, and it fulfills the different needs of all kinds of steel industry, so it the myth that the Panxi vanadium-titinium magnetite can not produce high ferrotitanium because the impurity of it is high, and it fills up the blank in our country.
Owner:攀枝花市银江金勇工贸有限责任公司

Method for preparing lightweight calcium silicate board

The invention discloses a method for preparing a lightweight calcium silicate board. The method comprises the following steps: (1) treating raw materials: mixing calcium sodium silicate raw materials and a dilute alkali solution to obtain mixed slurry; carrying out alkaline hydrolysis on the mixed slurry; after the hydrolysis reaction, separating the solid from liquid to obtain solid calcium silicate slag, wherein the calcium sodium silicate raw materials include one or more of fly ash, red mud, coal gangue, diatomite and bentonite; (2) preparing a mixed material, adding water and mixing uniformly, wherein the mixed material includes calcium silicate slag and reinforced fibers, and the reinforced fibers are paper fibers or cotton fibers; (3) debonding the reinforced fibers, mixing with the mixed material uniformly, and then separating solid from liquid to obtain the filter cake; (4) pressing the filter cake into a board, after formation, demolding the product, so as to obtain wet blank. The calcium silicate board prepared by using the method provided by the invention is small in density, high in strength, not liable to deform, and excellent in fireproof and thermal insulating properties; the method can realize high-valued utilization of high silica raw materials, such as fly ash, is simple and environment-friendly, and adopts a non-pressure steaming process which is economic and easy to implement.
Owner:INST OF PROCESS ENG CHINESE ACAD OF SCI +1

Method for preparing full-plant corn silage by cellar pressing

The invention relates to a method for preparing full-plant corn silage by cellar pressing, which comprises the steps of cleaning a storage cellar, pressing the cellar, sealing the cellar and fermenting. The pressure storage of each silage layer adopts specific parameters, each ton of silage is added with 2-6 grams of a fermenting agent and 8-10 grams of a silage additive; after compaction, the thickness of each silage layer is 10cm-20cm, and the density is 700kg / m <3>;; The temperature of the silage cellar is selected to be in a normal temperature environment; the cellar-pressing silage is completed within 10 hours after the silage raw materials are harvested; wherein the water content of the silage raw material is ensured to be between 62% and 74% when harvesting; lactobacillus plantarumand pediococcus lactis are selected as the silage fermenting agent, and the dosage ratio of the lactobacillus plantarum and the pediococcus lactis is 2: 1; the silage additive is selected from cellulase, xylanase and calcium sodium silicate hydrate, and the dosage ratio of the cellulase to the xylanase to the calcium silicate hydrate is 5: 3: 2; according to the invention, the prepared silage hashigher water content, and the silage is fresh, tender and juicy; The content of soluble sugar and the consumption rate of crude protein in the silage are reduced to a lower degree, and nutrients in the silage are better retained; the pH value is lower, thereby being more beneficial to long-term stable storage of the silage.
Owner:呼和浩特市友邦草业有限公司

Method for preparing series titanium and iron alloy by smelting titanium raw charge

The invention discloses a method for smelting and preparing series ferrotitanium from high-phosphorus, sulfur and titanium raw materials in pan-xi region, which comprises the following steps: adding titanium raw materials in the pan-xi region and 20 to 40 percent of iron-containing materials into a revolving furnace, quickly heating the materials for 20 to 25 minutes until the temperature is between 700 and 850 DEG C, and sending the materials into a mixer through a connecting bin for full and uniform mixing; adding calcium metallurgical auxiliary materials, a calcium-sodium finishing agent, metal aluminum, an auxiliary reducer and potassium chlorate into a proportioning bin in turn, and uniformly mixing the raw materials and the auxiliary materials in the mixer; unloading the mixed materials into a smelting furnace which is preheated to a temperature of between 150 and 300 DEG C and an elevated stock bin through the connecting bin, and smelting the mixed materials according to lower ignition technology; adding refined materials and a retarder after the reaction is over, and cooling the mixed materials for 48 to 80 hours; and finally separating slag and the ferrotitanium, and checking, packaging and warehousing ferrotitanium products. The method has stable sources of raw materials and safe and reliable manufacturing technique, and the prepared ferrotitanium series products have stable quality, so that the method breaks through the myth that the ferrotitanium can not be produced due to high content of impurities in the titanium-containing raw materials in the pan-xi region and makes up for the blank in China.
Owner:PANZHIHUA JINTAISHAN IND & TRADE

Ti-Al series intermetallic compound alloy

The invention relates to a Ti-Al series intermetallic compound alloy which is smelted from a raw material containing titanium in the Panxi area. Per 100Kg of the raw material containing titanium of the Panxi area contains the following auxiliary materials: 75-115Kg of metallic aluminum, 15-25Kg of calcareous metallurgical auxiliary material, 18-28Kg of potassium chlorate and 1.5-3.5Kg of calcium-sodium series treating agent and can also contain any one or a combination of the following two auxiliary materials: 3-10Kg of vanadium series raw material, 12-45Kg of columbium series raw material, 4-6Kg of carbon raw material or 3-4Kg of silicon raw material. The invention has stable raw material source and safe and reliable production process, and a prepared Ti-Al series intermetallic compound alloy product has stable product quality and can meet the technology and quality requirements on Ti-Al series intermetallic compounds of the modern industry. Meanwhile, the invention also solves the technical problem of smelting the Ti-Al series intermetallic compound alloy product by using a vanadium-titanium raw material with a high impurity content of the Panxi area, thereby rewriting the history that the raw material containing titanium of the Panxi area cannot be used for producing titanium alloy because of the high impurity content and filling a domestic blank.
Owner:攀枝花市银江金勇工贸有限责任公司

Adsorption plate with efficient adsorption function on organic chemical industry wastewater and preparation method thereof

InactiveCN103623781AHas the function of slow release of phosphorusEfficient adsorption functionOther chemical processesWater/sewage treatment by sorptionNitric acidEthylenediamine tetraacetate
The invention discloses an adsorption plate with efficient adsorption function on organic chemical industry wastewater and a preparation method thereof. The preparation method comprises the following steps: preparing a NH4HCO3 solution, a Ca(NO3)2 solution, a (NH4)2HPO4 solution, a NaOH solution, a nitric acid solution, a urea water solution and a calcium sodium ethylenediamine tetraacetate solution into a mixed solution F; preparing a styrene chloroformic solution, a divinylbenzene chloroformic solution and an azodiisobutyronitrile chloroformic solution into a mixed solution M; dropwisely adding the mixed solution F into the mixed solution M to obtain a mixed solution O; injecting distilled water into a container filled with liquid nitrogen to prepare ice granules, screening, and compacting in a mold; and casting the mixed solution O into the mold to perform freeze molding, demolding and refrigerating to obtain the porous adsorption plate. The manufacturing technique is simple; and the prepared adsorption plate has the functions of slowing release of phosphorus and efficiently adsorbing pollutants in organic chemical industry wastewater.
Owner:BEIJING NORMAL UNIVERSITY

Colorful gradual-change silk-soft brightening eye shadow and preparation method thereof

The invention discloses a colorful gradual-change silk-soft brightening eye shadow and a preparation method thereof and belongs to the technical field of cosmetics. The eye shadow is prepared from thefollowing raw materials in percentage by mass: 5-10% of a polydimethyl siloxane cross-linking polymer, 5-15% of cyclic polydimethyl siloxane, 2-6% of trimethyl silane oxy silicate ester, 8-15% of mica, 5-15% of synthetic fluorophlogopite, 3-15% of silica, 3-5% of magnesium stearate, 2-10% of polymethyl methacrylate, 3-13% of polymethylsilsesquioxane, 1-10% of titanium dioxide, 3-15% of CI77491, 1-6% of CI77492, 1-5% of CI77499, 0.5-5% of tocopheryl acetate, 0.1-0.3% of caprylyl glycol, 0.1-0.5% of ethylhexylglycerin, 1-5% of ethylene glycol, 0.1-0.9% of phenoxyethanol, 0.01-0.1% of o-cymene-5-alcohol, 0.1-0.8% of calcium sodium borosilicate, 0.1-0.2% of tin oxide and 0.1-0.5% of sodium hyaluronate. The eye shadow prepared by using the preparation method disclosed by the invention has improved smoothness and softness, is beneficial to eye shadow skin adherence, and in addition, is free of powder flying and good in ductility. The eye shadow has good durability and coloring effects, hasmultiple functions with one powder, and is applicable to common consumer groups.
Owner:广州香枝化妆品有限公司

Adsorption plate with high-efficient adsorption and enhanced biodegradation of petroleum hydrocarbon pollutants and preparation method thereof

The invention discloses an adsorption plate with high-efficient adsorption and enhanced biodegradation of petroleum hydrocarbon pollutants and a preparation method thereof. The preparation method comprises the steps of preparing a mixed solution F from NH4HCO3, Ca(NO3)2, (NH4)2HPO4, a urea water solution and an ethylenediaminetetraacetic acid calcium sodium solution; preparing a mixed solution L from urea and a formaldehyde water solution; preparing a mixed solution M from a poly beta-hydroxybutyrate chloroform solution and a polyethylene glycol chloroform solution; dropping the mixed solution L into the mixed solution M to obtain a mixed solution N; dropping the mixed solution F into the mixed solution N to obtain a mixed solution O; spraying distilled water into a container containing liquid nitrogen to prepare ice ball particles, screening and then placing in a mold for compaction; pouring the mixed solution O into the mold for freezing and shaping, then demolding, and freezing to obtain the adsorption plate; culturing the adsorption plate in a petroleum hydrocarbon degrading bacterial culture solution for 24h and then taking out for air-drying. The preparation process disclosed by the invention is simple, and the prepared adsorption plate has high treatment efficiency against petroleum hydrocarbon pollutants and can prevent secondary pollution and destruction to an ecological environment of a water body.
Owner:BEIJING NORMAL UNIVERSITY

Non-linear optical crystal calcium sodium borate and preparation method and application thereof

The invention relates to non-linear optical crystal calcium sodium borate and a preparation method and application thereof. The optical crystal calcium sodium borate is a single crystal with a centimeter dimension and belongs to an orthorhombic system, wherein the molecular formula of the optical crystal calcium sodium borate is NaCa4B3O9, the molecular weight is 359.73, and the unit cell parameters are shown as follows: a is equal to 10.68004(11)A, b is equal to 11.28574(11)A and c is equal to 6.48521(6)A. In the preparation method, a target product is formed by taking calcium sodium borate polycrystal powder and the like as a raw material and by utilizing a flux growth method. In the non-linear optical crystal calcium sodium borate and the preparation method and the application thereof, the raw material has a broad source and is cheap and available. Moreover, the preparation process is simple and is easy to operate and has a short period; an obtained product has the centimeter dimension; inclusions are few; the non-linear optical effect of the non-linear optical crystal calcium sodium borate is approximately equal to 2/3 of the non-linear optical effect of potassium dihydrogen phosphate (KDP) to be tested under the same condition; the laser-induced damage threshold is larger; the mechanical property is good; the non-linear optical crystal calcium sodium borate is not easy to fracture and is not deliquescent; the physical and chemical properties are stable; the light transmission band is 220nm to 3000nm; and the non-linear optical crystal calcium sodium borate has a wider light transmission range in ultraviolet and deep ultraviolet areas, is easy to process and store and is suitable for widely being applied in non-linear optical devices, such as ultraviolet frequency doubling generators, upper or lower frequency converters or optical parameter oscillators and the like.
Owner:SUZHOU INST OF NANO TECH & NANO BIONICS CHINESE ACEDEMY OF SCI

Aqueous heat-insulation heat-preservation fireproof material and preparation method thereof

The invention discloses an aqueous heat-insulation heat-preservation fireproof material. The aqueous heat-insulation heat-preservation fireproof material is prepared from the following components in percentage by weight: 8 to 20 percent of nano silicon oxide composite material obtained by compounding structurally-controlled nano silicon oxide powder and a nano silicon oxide cake material with an ultrahigh specific surface area according to a proportion of 0.5:(1-5):1, 3 to 15 percent of glass micro-beads, 4 to 10 percent of nano titanium oxide, 1 to 8 percent of potassium titanate, 1 to 8 percent of titanium pyrophosphate, 1 to 3 percent of aluminum hydroxide, 1 to 3 percent of zinc borate, 1 to 3 percent of barium borate, 1 to 3 percent of calcium sodium metasilicate, 1 to 10 percent of aluminum silicate, 20 to 28 percent of acrylic hybrid emulsion, 1.5 to 3 percent of other assistants, and the balance of water. According to the aqueous heat-insulation heat-preservation fireproof material disclosed by the invention, the nano silicon oxide composite material obtained by compounding structurally-controlled nano silicon oxide powder and the nano silicon oxide cake material with the ultrahigh specific surface area as a core material, and by the components and corresponding optimized improvement of the proportions, the product has a good heat-flow stagnation function; and the heat conduction coefficient of the product is not more than 0.03W/(m.K), and the waterproof performance reaches A level.
Owner:上饶市安纳拓新材料有限公司

Copolymer adsorption ball with enhanced biodegradation function against various organic pollutants and preparation process thereof

The invention discloses a copolymer adsorption ball with an enhanced biodegradation function against various organic pollutants and a preparation process thereof. The preparation process comprises the steps of preparing a mixed solution F from NH4HCO3, Ca(NO3)2, (NH4)2HPO4, a urea water solution and an ethylenediaminetetraacetic acid calcium sodium solution; preparing a mixed solution L from urea and a formaldehyde water solution; preparing a mixed solution M from a poly beta-hydroxybutyrate chloroform solution and a polyethylene glycol chloroform solution; dropping the mixed solution L into the mixed solution M to obtain a mixed solution N; dropping the mixed solution F into the mixed solution N to obtain a mixed solution O; dropping the mixed solution O into a polyvinyl alcohol solution to obtain a mixed solution P; adding the polyvinyl alcohol solution into the mixed solution P and performing centrifugal separation to obtain the copolymer adsorption ball with a nitrogen and phosphorus sustained release function; culturing the copolymer adsorption ball in a petroleum hydrocarbon degrading bacterial culture solution for 24h and then taking out for air-drying. The preparation process disclosed by the invention is simple, and the prepared copolymer adsorption ball has the nitrogen and phosphorus sustained release function, the function of adsorbing various organic pollutants and the function of degrading petroleum hydrocarbons.
Owner:BEIJING NORMAL UNIVERSITY
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