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508results about How to "Effective immobilization" patented technology

Preparation and application of dopamine functional magnetic nano-carrier

The invention belongs to the field of immobilization of proteins, and relates to preparation and application of a dopamine functional magnetic nano-carrier. The preparation comprises the following steps: firstly, dissolving FeSO4.4H2O and FeCl3.6H2O into distilled water, high-speed stirring and under protection of nitrogen, adding ammonia water of 25% NH4OH, and adding oleic acid; secondly, repeatedly cleaning black precipitates obtained by a stirring reaction and then using a strong magnet to perform precipitation separation, and drying to obtain oleic acid magnetic nano-particles; and finally, adding the oleic acid magnetic nano-particles into a dopamine hydrochloric acid solution, after the reaction is over, using a magnet to separate, cleaning and drying obtained deep brown precipitates, and then the dopamine functional magnetic nano-carrier can be obtained. According to the preparation and application of the dopamine functional magnetic nano-carrier provided by the invention, dopamine hydrochloride is adopted for modifying magnetic oleic acid nano-particles, so that the surface of a magnetic nano-particle has a plentiful of quinonyls and amidogen functional groups, thus proteins can be effectively immobilized; besides, the surface of the carrier has a layer of soft poly dopamine oxide films, the surface area is larger, and the preparation method is simple.
Owner:JIANGSU UNIV

High-temperature-resistant heteromorphic nanocrystalline aerogel material and preparation method thereof

The invention relates to a high-temperature-resistant heteromorphic nanocrystalline aerogel material and a preparation method thereof. The method is as follows: preparing heteromorphic nanocrystal dispersion liquid; mixing the heteromorphic nanocrystal dispersion liquid and an assembly agent evenly by stirring and ultrasonic treatment to obtain a mixture phase first solution; then adding a catalyst solution, performing a gelation reaction process by stirring and ultrasonic treatment, and then performing a vacuum pumping process to obtain gelation reaction liquid; and performing an aging step and a drying step to obtain a heteromorphic nanocrystalline aerogel material; the heteromorphic nanocrystalline aerogel material is subjected to post-treatment in two or more different temperature stages to obtain the high temperature-resistant heteromorphic nanocrystalline aerogel material. The invention performs a staged heat treatment process on the aerogel material in the post-treatment process, thereby realizing the strengthening and toughening of themicrostructure of the aerogel material, so that the structural strength of the aerogel material is remarkably improved, the high temperature resistance performance and the large specific surface area after the heat treatment are realized, and the preparation of the high-temperature-resistant heteromorphic nanocrystalline aerogel material capable of high-efficient heat insulation is realized.
Owner:AEROSPACE INST OF ADVANCED MATERIALS & PROCESSING TECH

Carbon-carbon multi-component negative electrode material and preparation method thereof

The invention relates to a carbon-carbon multi-component negative electrode material. The carbon-carbon multi-component negative electrode material is mainly composed of flexible graphite, nanometer silicon and amorphous carbon which respectively account for 30-60%, 30-50% and 10-30% based on mass percent, the amorphous carbon is obtained through high-temperature pyrolyzation of an organic carbon source, and the flexible graphite is obtained by applying pressure to expanded graphite. A preparation method of the product comprises the steps of: firstly, preparing an expanded graphite/silicon-silicon dioxide/carbon composite negative electrode material through high-temperature pyrolyzation; secondly, pouring the expanded graphite/silicon-silicon dioxide/carbon composite negative electrode material into a mould and applying pressure to obtain a flexible graphite/silicon-silicon dioxide/carbon composite negative electrode material; thirdly, processing silicon dioxide to obtain a flexible graphite/silicon/carbon composite negative electrode material through etching by a corrosive liquid; and finally, using asphalt to permeate a gap inside the flexible graphite/silicon/carbon composite negative electrode material in a protective atmosphere, and obtaining the product after high-temperature heat treatment and repetition. The carbon-carbon multi-component negative electrode material has the advantages of high capacity, high coulombic efficiency, good cycle performance, structure stability, high reversible capacity and the like.
Owner:CENT SOUTH UNIV

Winding device for textile

The invention discloses a winding device for textile. The winding device comprises a base. A rotating base is fixedly connected with one side in the base and rotationally connected with a lead screw.The lead screw transversely penetrates through the base and extends out of the base. The outer surface wall of the lead screw is in threaded connection with a sliding base. The top end of the outer surface wall of the sliding base is fixedly connected with a connecting block. The position, corresponding to the connecting block, of the base is provided with a sliding groove sliding relative to theconnecting block. The upper surface, corresponding to the base, of the top end of the connecting block is fixedly connected with a supporting column. A first safety chuck is fixedly connected with thetop end of the supporting column. A fixed column is fixedly connected with the side, corresponding to the supporting column, of the upper surface of the base. A second safety chuck is fixedly connected with the top end of the fixed column. The winding device can be adjusted for use according to winding rollers with different sizes, efficiency is improved, the use range is expanded, it is avoidedthat spinning yarn or cloth is manually wound on winding rollers to be wound, the structure is simple, operations are convenient, and the work intensity of personnel is reduced.
Owner:安徽双盈纺织有限公司

Electrochemical biosensor for detecting hydrogen peroxide, preparation method and application thereof

The present invention relates to an electrochemical biosensor for detecting hydrogen peroxide, a preparation method and an application thereof. The preparation method comprises the steps of (1) synthesizing the silica-three-dimensional graphene composite material; (2) doping nitrogen and carbon into the synthesized silica-three-dimensional graphene composite material; (3) pretreating a glassy carbon electrode; (4) preparing the glassy carbon electrode modified by the nitrogen-carbon-doped silica-three-dimensional graphene composite material through the dispensing method; (5) putting the glassy carbon electrode into a chloroauric acid solution to prepare gold nanoparticle-nitrogen-carbon-doped silica-three-dimensional graphene glassy carbon electrode through chronoamperometry; (6) dipping the glassy carbon electrode into a double-sulfhydryl-modified GDNA solution and cultivating for 2-4 hours; (7) dipping the composite electrode into a hemin solution for 10-14 hours. The electrochemical biosensor is good in stability and reproducibility, high in specificity and sensitivity, fast and simple and convenient to operate. The electrochemical biosensor can be used for detecting the content of hydrogen peroxide in biological samples, cosmetics and the like.
Owner:广东省汕头市质量计量监督检测所

Test method and test device for simulating natural inhomogeneous rusting of reinforcing steel bar in concrete

The invention discloses a test method and a test device for simulating natural inhomogeneous rusting of a reinforcing steel bar in concrete. The method comprises the following steps: pre-burying stainless steel wires in concrete, and supplying constant-current power for electrolytic reaction to a concrete test piece. The test device comprises a mold unit, a stressing unit, a test piece to be tested and a power supply unit, wherein the mold unit comprises a mold for casting the test piece to be tested, a through hole bolt and a fastening bolt; the stressing unit comprises a bracket, a lower fulcrum, an upper fulcrum, a loading screw rod and a popping bolt; the test piece to be tested comprises a concrete base body, a reinforcing steel bar and a stainless steel wire electrode; the power supply unit adopts a voltage-stabilizing current-stabilizing direct-current power supply. The test method and the test device have the benefits that the test period is short, natural inhomogeneous rusting of the reinforcing steel bar can be effectively simulated, the position, the rusting range and the rusting degree of inhomogeneous rusting in the circumference direction, and inhomogeneous rusting in the length direction of the reinforcing steel bar can be effectively controlled, energy loss caused by concrete resistance can be reduced, and the prediction result precision is high.
Owner:ZHEJIANG UNIV OF TECH

Dust remover and bag cage of dust remover

The invention relates to a dust remover and a bag cage of the dust remover. The bag cage comprises inner longitudinal ribs assembled at the inner side of a filter bag, and outer longitudinal ribs assembled at the outer side of the filter bag, wherein the inner longitudinal ribs are positioned at the outer sides of the outer longitudinal ribs; the inner longitudinal ribs and the outer longitudinal ribs are distributed at intervals in a staggered manner and are used for enabling the cross section of the filter bag assembled between the inner longitudinal ribs and the outer longitudinal ribs to be in a polygonal star shape. During use of the dust remover, the cross section of the filter bag is replaced by the polygonal star shape from a traditional round shape, so that the filtering area is enlarged under the same distribution space; as the filtering area is enlarged, the air passing amount in the unit area of the filter bag is reduced under the same air passing amount condition, and furthermore the abrasion and the corrosion to the filter bag are reduced; the relatively effective supporting and fixing can be provided for the filer bag due to a double-layer structure formed by the inner longitudinal ribs and the outer longitudinal ribs, so that the deformation and the loosing of the filter bag can be avoided, the filtering effect is improved, and the service life of the filter bag is prolonged.
Owner:ZHEJIANG DEYAO ENERGY SAVING TECH CO LTD

Sintering fixture for micro channel semiconductor laser and sintering method thereof

The invention discloses a sintering fixture for a micro channel semiconductor laser and a sintering method thereof. The sintering fixture comprises a positioning base and an adjustable cover plate, wherein the adjustable cover plate is connected onto the positioning base; a concave surface is arranged on the positioning base; two sides of the concave surface are bosses; the adjustable cover plate comprises a main body, a pressing block and a pressing block adjustment mechanism, the main body is provided with a pressing block groove, and the pressing block is arranged inside the pressing block groove via the pressing block adjustment mechanism. The micro channel semiconductor laser sintering method by the above device comprises steps: a micro channel heat sink sintered with a semiconductor laser bar chip, an insulated sheet and the adjustable cover plate are sequentially connected onto the positioning base from bottom to top and fixed by using bolts, and the above well-fixed entire fixture is sealed in a protection cover shell with nitrogen and is placed on a heating table for sintering. According to the sintering fixture for the micro-channel semiconductor laser and the sintering method thereof, the structure is simple, the cost is low, the operation is simple, convenient and reliable, and through one-time sintering, quick and accurate fixed connection among the bar chip of the micro-channel semiconductor laser, the micro-channel heat sink, the insulated sheet and a negative electrode sheet can be realized.
Owner:Shandong Huaguang Optoelectronics Co. Ltd.

Novel membrane coupled anaerobic bioreactor and method of treating wastewater thereof

The invention relates to a novel membrane coupled anaerobic bioreactor, comprising an baffle plate anaerobic reactor and a tubular membrane ultrafiltration device; a water outlet of the baffle plate anaerobic reactor is communicated with a water inlet of the tubular membrane ultrafiltration device by pipelines, and a water return port of the tubular membrane ultrafiltration device is communicatedwith a water inlet of the baffle plate anaerobic reactor by pipelines; when treating wastewater, the wastewater flows in from the water inlet of the baffle plate anaerobic reactor and the water inletof the tubular membrane ultrafiltration device, then the wastewater after being treated flows out from a discharge port of the tubular membrane ultrafiltration device, and anaerobic activated sludge which is generated when the tubular membrane ultrafiltration device treats the wastewater reflows to the water inlet of the baffle plate anaerobic reactor. The reactor and the method can separate and fix microorganisms completely, ensure the microorganism concentration in a reaction chamber to be much more than the concentration in a normal anaerobic device, improve the anaerobic treating effect, quicken the anaerobic reaction speed greatly, shorten the residence time of the wastewater effectively and prolong the residence time of the sludge greatly.
Owner:杨春辉

Preparation method of chalcogenide glass tapered fibers

ActiveCN104609723AEasy to solveSolve the core diameterGlass making apparatusTemperature controlFiber
The invention discloses a preparation method of chalcogenide glass tapered fibers. Chalcogenide glass fibers are tapered by the aid of accurate temperature control of a specific electric-heating coil and traction of a precision stepping motor, important parameters such as taper zone lengths, taper zone outer diameters and the like of the tapered fibers are controlled through control on the heating temperature and the tapering traction speed, and the chalcogenide glass tapered fibers with different taper zone lengths and taper zone outer diameters are drawn accurately. The method is simple in technology, high in operability, good in repeatability and high in accuracy and can effectively solve problems that the chalcogenide glass fibers are broken easily during tapering, fiber core diameters and taper zone lengths are difficult to control accurately and the like, the fiber core diameters of the prepared chalcogenide glass tapered fibers with nanoscale or submicron diameters range from 700 mu m to 1,000 mu m, the taper zone lengths range from 3 cm to 7 cm, the production cycle is short, the success rate is high, the chalcogenide glass tapered fibers can be applied to new technical fields of coupling of micro-waveguides, generation of super-continuum spectrum and the like, and research and application fields of the chalcogenide glass tapered fibers are greatly extended.
Owner:NINGBO UNIV

Flat tube type solid oxide fuel cell pack

The invention discloses a flat tube type solid oxide fuel cell pack, which comprises more than two flat tube type fuel cell units that are connected by plate alloy connecting components. The substrate of the plate alloy connecting components is a Cr-containing Fe based or Ni based alloy, the surface of which is coated with a conductive coating inhibiting alloy high temperature oxidation and Cr pollution. The plate alloy connecting components are provided with arc-shaped grooves or bent surfaces matching with arc surfaces on both sides of the flat tube type cell units. During formation of the cell pack, the arc-shaped grooves or bent surfaces cooperate with the fuel cell units to form independent gas flow channels and make the solid fuel cell units fixed. Over two fuel cell units and the plate alloy connecting components are alternately arranged to form the cell pack with a rectangular cross section. The flat tube type solid oxide fuel cell pack can introduce a reaction gas into the narrow space between the flat tube type fuel cell units, and a fuel cell stack with a compact structure is easy to form by close piling. The flat tube type solid oxide fuel cell pack has the advantages of good power generation performance, compact structure and high stability, etc.
Owner:DALIAN INST OF CHEM PHYSICS CHINESE ACAD OF SCI

Multi-temperature-regulation massaging device for hemodialysis

The invention discloses a multi-temperature-regulation massaging device for hemodialysis. The multi-temperature-regulation massaging device for hemodialysis has powerful functions and can be used for effectively heating and keeping heat of a punctured blood vessel of a hemodialysis patient and promoting hemangiectasis, and the puncturing success rate is improved; the punctured blood vessel of the patient can be massaged through simple operation, edema liquid of a punctured part is eliminated and the blood vessel is exposed, so that the puncturing success rate is improved and pains of the patient are alleviated. The hematoma of the punctured part of the patient can also be subjected to cooling treatment and blood capillaries are retracted through cold application, so that partial hyperemia and bleeding are alleviated and the limitation of edema is facilitated. The device is used for carrying out hot application and massaging on the punctured parts including internal fistula and the like of the patient in combination with corresponding medicines, and partial blood circulation can be facilitated; the permeability of tissue cells is improved and the medicines can be easily absorbed; the elimination of the hematoma is accelerated and the absorption of the hematoma is promoted; damaged tissues are stimulated to regenerate and scars are softened; an vascular access of the patient is effectively protected and the living quality of the patient is improved.
Owner:皖南医学院第一附属医院

Nano-crystalline cellulose based 3D printing lactobacillus embedding material as well as preparation method and application thereof

The invention discloses a nano-crystalline cellulose based 3D printing lactobacillus embedding material as well as a preparation method and application thereof. The method comprises the following steps of adding sodium alginate in a nano-crystalline cellulose solution, uand performing uniform mixing and centrifuging to obtain a mixed solution; adding chitosan in water, performing uniform mixing, and adding glacial acetic acid to obtain a chitosan solution; adding lactobacillus powder in the chitosan solution, and performing uniform mixing to obtain a chitosan-lactobacillus bacterial suspension; taking the mixed solution as an outer material, and the chitosan-lactobacillus bacterial suspension as an inner material, and performing 3D printing to obtain a printing product; and spraying the surface of the printing product with a calcium chloride solution, and performing curing and cold drying to obtain the nano-crystalline cellulose based 3D printing lactobacillus embedding material. For the nano-crystalline cellulose based 3D printing lactobacillus embedding material, the lactobacillus is immobilized by taking the nano-crystalline cellulose and the chitosan as carriers, so that efficient continuous cyclic fermentation of yogurt can be realized, and the problems of difficulty in preservation of lactobacillus, low utilization rate and high cost can be solved.
Owner:SOUTH CHINA UNIV OF TECH

Horizontal positioning device for prefabricated stand column and method for positioning and installing prefabricated stand column through horizontal positioning device

The invention provides a horizontal positioning device for a prefabricated stand column. The horizontal positioning device comprises a positioning frame (1), wherein the positioning frame (1) is defined by side walls on the periphery, and the center of the positioning frame (1) is of a hollow frame-shaped structure. The lower portion of the positioning frame (1) is connected to a horizontal position, where the prefabricated stand column needs to be positioned, of a bearing platform in a positioned mode. The shape of the inner edge of the positioning frame (1) is identical or approximately identical to the shape of the cross section of the prefabricated stand column. The area defined by the inner edge is identical or slightly larger than the cross sectional area of the prefabricated stand column. According to a steel bar jig frame manufactured through the horizontal positioning device, and precise positioning and positioning correction of the prefabricated stand column in the horizontal direction can be effectively achieved, so that when the prefabricated stand column and the bottom bearing platform are spliced, the positioning precision of the horizontal position of the prefabricated stand column is high, and control operation is easy and convenient. The invention further relates to a positioning and installing method of the horizontal position of the prefabricated stand column through the horizontal positioning device for the prefabricated stand column.
Owner:SHANGHAI HIGHWAY INVESTMENT CONSTR DEV CO LTD +1
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