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44 results about "Spin filtering" patented technology

Preparation method of 33 dtex/144f fine denier polyester fiber

The invention relates to a preparation method of 33 dtex/144f fine denier polyester fiber. Conventional polyester melt serves as main melt, hydrophilic polyester melt and the main melt are mixed through a front-of-pump injecting system and then subjected to before-spinning filtering, enter a spinning assembly to be subjected to melting and spinning, and are subjected to annular air blowing cooling, oiling, stretching and rolling to obtain superfine denier POY fiber; superfine denier POY fiber serves as the raw material, the superfine denier POY fiber on a DTY elasticizer passes through a pretangle jet, a first roller, a deformation hot box, a cooling plate, a false twister, a second roller, a main network nozzle, an auxiliary second roller, a sizing hot box, a third roller and an oiling wheel to be subjected to rolling and forming to prepare fine denier polyester filaments. Due to the excellent filament number, the small fiber diameter and the large surface specific area of the fine denier polyester filament, the fiber has the advantages that the fiber has excellent softness and hand feeling of natural fiber and overcomes the defect that natural fiber is poor in mechanical performance and poor in wear resistance, and the additional value and competitiveness of a product are improved.
Owner:福建百宏聚纤科技实业有限公司

Spinning technology suitable for novel spinning machine with externally-arranged winding device

The invention relates to a spinning technology suitable for a novel spinning machine with an externally-arranged winding device. The spinning technology includes the working procedures of mucilage glue metering and feeding, before-spinning filtering, strand molding, spinning and winding, wherein heating drying processing is carried out on strands before winding is carried out. The spinning technology is used for the specific novel spinning machine with the externally-arranged winding device, under the mutual effects of the working procedures and technological parameter control, the strands can be wound in the externally-arranged winding device to form hygrometric-state cake packaged yarns and/or hygrometric-state drum packaged yarns and/or hygrometric-state twisted packages yarns capable of being directly used for yarn twisting. According to the spinning technology, the product quality can be guaranteed while it is guaranteed that the spinning machine runs at the high spinning speed, particularly, the strands can not be polluted by dropping of washing acid removal liquid and oil agents in the final winding molding working procedure, the follow-up dyeing technology is guaranteed, a worker can easily and conveniently carry out operation, equipment can be easily maintained, and energy consumption is reduced, so that the production efficiency is effectively improved, and meanwhile the product cost is greatly reduced.
Owner:YIBIN GRACE GROUP CO LTD +1

Chiral recognition material and preparation method thereof

The invention relates to the technical field of chiral recognition materials and particularly relates to a chiral recognition material and a preparation method thereof. The material comprises a long-afterglow luminescent material loaded with metal nanoparticles on the surface, and chiral cysteine which is self-assembled on the surfaces of the metal nanoparticles to form a chiral molecular layer. The heterojunction between the long-afterglow material and a chiral recognition material is utilized, long-life electrons are transferred from the long-afterglow material to the surface of the chiral recognition material, and a large number of long-life electrons are injected into the surface of the chiral recognition material, the current density on an electrode is effectively enhanced, and an electrochemical recognition signal is amplified. Meanwhile, the spin filtering effect of chiral molecules on electrons is utilized, the electrons are spin-polarized when flowing through the chiral molecular layer assembled on the surfaces of the metal nanoparticles, so an electromagnetic field on the surface of the electrode is changed, the acting force difference between L and D amino acid enantiomers in an electrolyte is amplified, and the detection sensitivity is improved.
Owner:JINLING INST OF TECH

A kind of preparation method of α-abortion-3,5-cracking-androst-5-one-3,17-dioic acid

The invention provides a preparation method of A-nor-3, 5-cracking-androstane-5 -keto-3, 17-diacid. The preparation method comprises the following steps: (1), 3-carbonyl-4-androstene-17beta carboxylic acid is dissolved in alkaline water, and the temperature of the solution is controlled to be 20-40 DEG C; (2), an oxidizing agent which is an aqueous solution including sodium periodate and potassium permanganate is added, and reaction is performed continuously for 1-3 h after addition; (3), after sufficient reaction, cooling is performed by ice brine until the temperature is 0-5 DGE C, spin-filtering is performed, and a filter cake is washed by ice alkaline water at the temperature of 0-5 DEG C and spin-dried; and (4), a filtrate obtained from spin-filtering is acidized and spin-filtered, and a filter cake is washed until an eluate is neutral. According to the provided method, an organic solvent is not used, accordingly, the method is economic and environment-friendly, and aftertreatment is simple; reaction is performed under homogeneous phase condition, the reaction temperature and iodate separation temperature are lower, the product quality is good, the yield is high, the iodate recovery rate is high, and the cost is low. Therefore, a product with higher purity can be obtained at high yield and low cost with the method.
Owner:HUNAN KEREY BIOTECH

A kind of preparation method of the polyester fine denier yarn of 33dtex/144f

The invention relates to a preparation method of 33 dtex / 144f fine denier polyester fiber. Conventional polyester melt serves as main melt, hydrophilic polyester melt and the main melt are mixed through a front-of-pump injecting system and then subjected to before-spinning filtering, enter a spinning assembly to be subjected to melting and spinning, and are subjected to annular air blowing cooling, oiling, stretching and rolling to obtain superfine denier POY fiber; superfine denier POY fiber serves as the raw material, the superfine denier POY fiber on a DTY elasticizer passes through a pretangle jet, a first roller, a deformation hot box, a cooling plate, a false twister, a second roller, a main network nozzle, an auxiliary second roller, a sizing hot box, a third roller and an oiling wheel to be subjected to rolling and forming to prepare fine denier polyester filaments. Due to the excellent filament number, the small fiber diameter and the large surface specific area of the fine denier polyester filament, the fiber has the advantages that the fiber has excellent softness and hand feeling of natural fiber and overcomes the defect that natural fiber is poor in mechanical performance and poor in wear resistance, and the additional value and competitiveness of a product are improved.
Owner:福建百宏聚纤科技实业有限公司

A spinning process suitable for spinning machine with external winding device

The invention relates to a spinning technology suitable for a novel spinning machine with an externally-arranged winding device. The spinning technology includes the working procedures of mucilage glue metering and feeding, before-spinning filtering, strand molding, spinning and winding, wherein heating drying processing is carried out on strands before winding is carried out. The spinning technology is used for the specific novel spinning machine with the externally-arranged winding device, under the mutual effects of the working procedures and technological parameter control, the strands can be wound in the externally-arranged winding device to form hygrometric-state cake packaged yarns and / or hygrometric-state drum packaged yarns and / or hygrometric-state twisted packages yarns capable of being directly used for yarn twisting. According to the spinning technology, the product quality can be guaranteed while it is guaranteed that the spinning machine runs at the high spinning speed, particularly, the strands can not be polluted by dropping of washing acid removal liquid and oil agents in the final winding molding working procedure, the follow-up dyeing technology is guaranteed, a worker can easily and conveniently carry out operation, equipment can be easily maintained, and energy consumption is reduced, so that the production efficiency is effectively improved, and meanwhile the product cost is greatly reduced.
Owner:YIBIN GRACE GROUP CO LTD +1

Synthesis method of cinnamyl piperazine

The invention discloses a synthesis method of cinnamyl piperazine. The method includes the steps of: a) adding a solvent into a reaction kettle and adding piperazine to uniformly dissolve the piperazine, dropwisely adding hydrochloric acid at 20-25 DEG C until the pH of the reaction solution is 2, which is the terminal, and after the reaction is performed for 1 h, cooling the reaction solution to 20 DEG C, and centrifugally spin-filtering the reaction solution to obtain piperazine dihydrochloride; b) adding the solvent into the reaction kettle, adding the piperazine dihydrochloride and the piperazine with stirring at the same time, and performing a reaction at 68-85 DEG C for 0.5-3 h; c) reducing the temperature to 45-55 DEG C, dropwisely adding cinnamyl chloride, and then increasing the temperature to 60-75 DEG C to perform a temperature maintained reaction for 1-4 h, and reducing the temperature to 10-35 DEG C, performing centrifugal separation, sucking a mother liquid into a distillation reaction kettle, heating the distillation mother liquid to recycle the solvent, adding pure water, and dropwisely adding an alkali liquid to regulate the pH to 9-12, and adding chloroform to perform extraction, drying the mixture, and evaporate-drying the chloroform to obtain the cinnamyl piperazine. The synthesis method reduces production steps and pollutant emission, and is more suitable for modern industrial production.
Owner:郑州瑞康制药有限公司
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