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31results about How to "With rigid structure" patented technology

A kind of submicron organic spirocyclic aluminum phosphate flame retardant and preparation method thereof

The invention relates to a submicron organic spirocyclic aluminum phosphate flame retardant and a preparation method thereof, belonging to the field of flame retardants. A submicron organic spirocyclic aluminum phosphate flame retardant, the structural formula is as follows: the preparation method is: firstly, the pentaerythritol diphosphate (DPP) is hydrolyzed in the alcohol aqueous solution under the action of alkali to obtain its sodium salt or potassium salt II solution, and then react the prepared pentaerythritol diphosphate sodium or potassium salt under heating and vigorous stirring conditions to prepare an organic spirocyclic aluminum phosphate flame retardant. The particle size of the prepared organic spirocyclic aluminum phosphate is less than 0.7 μm, and the particle size distribution range is narrow, reaching the submicron level, which can effectively reduce the consumption amount of the flame retardant in the polymer. The preparation method designs phosphorus-based flame retardants and aluminum salts with excellent flame-retardant properties in one molecule, which fundamentally solves the problem of the compounding of flame retardants in the process of material flame-retardant and the uneven distribution of components in the flame-retardant system. Equality issues.
Owner:BEIJING INSTITUTE OF TECHNOLOGYGY

High-temperature-resistant heat-insulating protective clothing and preparation process thereof

The invention discloses a high-temperature-resistant heat-insulating protective garment and a preparation process thereof, and relates to the field of protective garments, and the high-temperature-resistant heat-insulating protective garment is prepared by selecting a polysulfonamide fabric, performing flame-retardant finishing by using an after-finishing flame retardant, soaking the polysulfonamide fabric in an anti-static liquid, dipping, drying, and coating the surface of the fabric with a polytetrafluoroethylene coating, thereby obtaining the high-temperature-resistant heat-insulating protective garment. The anti-static breathable layer, the heat insulation layer and the flame-retardant layer are sequentially compounded, and the problems that an existing protective garment is poor in heat insulation performance, cannot well block heat energy outside the protective garment and is not ideal in flame-retardant effect are solved; the compounding of organic and inorganic materials can realize complementary advantages, and gives consideration to the mechanical property, weaving property, heat insulation and open fire resistance of polysulfonamide, so that the heat insulation property of the fabric is improved, the flame-retardant layer can prevent combustion products from escaping and inhibit thermal decomposition of materials under the layer, the flame-retardant, low-smoke and low-toxicity effects are achieved, a cracked carbon layer is formed on the surface of the polysulfonamide, and the flame-retardant, flame-retardant and flame-retardant effects are achieved. And the oxidation resistance of the cracked carbon layer is improved, so that the flame-retardant purpose is achieved.
Owner:安徽上造智能设备科技有限公司

Submicron organic spiro aluminum phosphate flame retardant and preparation method thereof

The invention relates to a submicron organic spiro aluminum phosphate flame retardant and a preparation method thereof, which belong to the field of fire retardants. The structural formula of the submicron organic spiro aluminum phosphate flame retardant is as follows (see the description). The preparation method comprises the steps of firstly, hydrolyzing pentaerythritol phosphate (DPP) in an alcohol-water solution under the action of alkali, so as to prepare a solution of sodium salt or sylvite II, and then reacting the prepared pentaerythritol phosphate sodium or sylvite in heating and violent mixing conditions, so as to prepare the organic spiro aluminum phosphate flame retardant. The particle size of prepared organic spiro aluminum phosphate is less than 0.7 mum, the particle size distribution range is narrow and achieves the submicron level, and the consumption of the flame retardant in polymers can be effectively reduced. According to the preparation method, the phosphorus based flame retardant and aluminum salt with good flame retardation are designed in a molecule, so that the problems of formulation of the flame retardant in the flame retardant process of materials and unevenness of distribution of respective components of a flame retardant system are basically solved.
Owner:BEIJING INSTITUTE OF TECHNOLOGYGY
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