The invention discloses a preparation method for a
low oxygen content and high alloying
nickel-based mother
alloy and
powder and belongs to the field of
powder metallurgy. The technological process of the preparation method includes the steps that firstly, a pure mother
alloy ingot is prepared by means of duplex processes of vacuum
smelting and electroslag remelting. In the process of vacuum
smelting, a
calcium oxide crucible is adopted, raw materials are pre-treated, carbon blocks are added in a refining stage for
deoxidization, elements prone to the burning loss are supplemented at the end stage of
smelting, and the mother
alloy ingot in designed components is obtained. In the process of the electroslag smelting, by adjusting the shape, the depth, the
viscosity and other parameters of a
slag pond, the float-up condition of the nonmetallic inclusion is created, and the mother alloy is further purified. After the mother alloy
ingot subjected to electroslag remelting is subjected to scaling, the mother alloy ingot is subjected to high-speed disk
grinding breakage under the protective
atmosphere, and the ultra-thin mother alloy
powder is obtained. The particle size of the K418 mother alloy powder prepared through the method is smaller than 20 microns, the
oxygen content is lower than 200 ppm, the
sulfur content is lower than 20 ppm, after the alloy podwer is mixed with carbonyl
nickel powder,
sintering compacting at low temperature can be achieved, and the production cost and the process
energy consumption of a high temperature alloy of the powder are greatly reduced.