The invention relates to the technical field of
textile dyeing and finishing, in particular to a method for recovering hydrolyzed
reactive dye and
dyeing wool fabric with little water, which comprises the following steps: preparing an aminated magnetic almond shell adsorbent, and extracting the hydrolyzed
reactive dye; the method comprises the following steps of:
dyeing 0.5 g of
wool fabric, 3% (o.m.f) of hydrolytic
reactive dye, a bath ratio of 1: 50 and 60 DEG C in a less-water
system of water and a deep-eutectic
solvent LaBet in a ratio of 3: 7, heating to 80 DEG C, carrying out shock dyeing for 1 hour, washing with water after dyeing, soaping, and
drying. Wherein LaBet is a eutectic
solvent prepared by mixing
anhydrous lactic acid and
betaine according to a
molar ratio of 19: 1, heating to a certain temperature, magnetically stirring for 2 hours until a faint yellow transparent liquid is formed, and cooling to normal temperature. According to the present invention, the waste by-product during nut
processing is researched to prepare the adsorbent, the
hydrolysis reactive dye is extracted and recovered, and the dyeing process of the three-
primary color hydrolysis reactive dye in the DES
chromosome system on the
wool fabric is optimized by using the
single factor method so as to achieve the
recovery of the waste resource;