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45 results about "Lead extraction" patented technology

A lead extraction is the removal of one or more leads from inside the heart. Leads that are placed outside the heart during open heart surgery cannot be removed during this procedure.

Comprehensive recycling method for non-ferrous metal metallurgy acidic wastewater and zinc-containing residues

Disclosed is a comprehensive recycling method for non-ferrous metal metallurgy acidic wastewater and zinc-containing residues. The zinc-containing residues generated in the zinc smelting production process serve as an acidic wastewater neutralizer. Liquid obtained after neutralization is subjected to fluorine and chlorine removal and concentrated to meet the requirements for a zinc sulfate solution of a zinc system, and then directly enters the electrolytic zinc system. Valuable metal such as arsenic, cadmium and copper in the acidic wastewater is recycled through an impurity purification procedure of the zinc system. The zinc-containing residues are subjected to a neutralization step to be recycled and fed into a lead extraction procedure after being enriched with lead, silver and other metal. The filter residues with fluorine and chlorine removed are regenerated with a sodium hydroxide solution, the residues obtained after regeneration can be used for the fluorine and chlorine removal procedure repeatedly, and sodium fluoride, sodium chloride and sodium hydroxide in the liquid obtained after regeneration are separated and recycled through efficient evaporative crystallization. The comprehensive recycling method for non-ferrous metal metallurgy acidic wastewater and zinc-containing residues is based on an existing zinc hydrometallurgy system, the balance of original materials in the system is maintained, and an additional heavy metal impurity purification procedure is not added. The comprehensive recycling method for non-ferrous metal metallurgy acidic wastewater and zinc-containing residues is short in process, low in cost, high in valuable metal recycling rate, free of discharging of secondary waste residues and waste water and good in comprehensive economical benefit.
Owner:湖南麓云达环境科技有限公司

Process for extracting tea saponin from tea seed cakes or meal

The invention relates to a process for extracting tea saponin from tea seed cakes or meal after oil frying by applying an industrial production device. The process comprises the following steps: crushing the tea seed cakes or the meal (leading the particle size to be 1-3mm), then sending into a steaming and stir-frying cauldron, drying (preventing the water content from exceeding 7%), then leading the material to enter into a material storage cylinder, using a screw conveyor to send the material into a rotocel extractor, and adding a solvent for extraction; carrying out residue-liquid separation (the meal residue can be used as a feed or a fertilizer) after double extraction, leading extraction solution to enter into a long pipe evaporator, removing part of water by double evaporation, and recycling the solvent (which can be recycled); and concentrating the extraction solution via a vacuum concentration tank, then crystallizing and drying, and obtaining a fine saponin finished product for packaging and leaving a factory. A product produced by the process contains 81.5% of active matters, and the pH value is 5.9. Compared with other methods, the process has the advantages of high product purity, light color, high production rate (14%), energy conservation, low consumption, no pollution and environmental protection, and is easy for operation and the like.
Owner:ANHUI YINGSHANHONG BIOLOGICAL TECH

Multi-metal comprehensive recovery process for arsenic-containing smoke dust

ActiveCN103981369AEliminate pollutionEliminate the effects of pollutionProcess efficiency improvementElectrolysisHydrometallurgy
The invention provides a multi-metal comprehensive recovery process for arsenic-containing smoke dust. According to the process, leachate containing zinc and copper and leaching slag containing arsenic and lead are obtained through selective leaching, the leachate is extracted by respectively using a copper extraction agent and a zinc extraction agent, and then reverse extraction and electrodeposition are carried out so as to obtain copper and zinc; the leaching slag is leached with a mixed arsenic removing agent consisting of H2O2 and Na2S2O3 so as to obtain arsenic-containing leachate and lead-containing arsenic-removed leaching slag, the arsenic-containing leachate is concentrated and crystallized so as to obtain sodium arsenate, and the lead-containing arsenic-removed leaching slag is subjected to pyrogenic process lead extraction and electrolytic refining so as to obtain lead. According to the invention, the multi-metal comprehensive recovery process uses combined hydrometallurgy and pyrometallurgy, comprehensive recovery process and a main smelting system are effectively combined together, seamless butt joint of a part of technology and main process technology is realized, process steps are environment-friendly, metallic copper, zinc and lead are effectively recovered, and resourceful treatment of arsenic is realized.
Owner:甘肃高能中色环保科技有限公司

Waste lead-acid battery diachylon hydrothermal reduction dual conversion method

The invention discloses a waste lead-acid battery diachylon hydrothermal reduction dual conversion method. Waste diachylon and alkali solution are firstly converted under normal pressure to remove most sulfate radicals; normal-pressure conversion liquid is fed to recover sodium sulfate; normal-pressure conversion slag and the alkali solution are pulped to feed into a reducing agent to add in a high-pressure reaction kettle for reaction under requested temperature and nitrogen partial pressure, so that residual lead sulfate in the normal-pressure conversion slag is reacted with alkali to deeply remove the sulfate radicals; meanwhile, lead dioxide is reduced as lead monoxide; after the reaction time is reached, the solid-liquid separation is performed; hydrothermal conversion liquid is returned into the normal-pressure conversion process; and lead is further extracted from the hydrothermal conversion slag. The essence of the method is to realize dual purposes of deep conversion desulfurization and reduction conversion of the waste diachylon by using a water heat and reduction combined mode; the desulfurization rate and the lead dioxide reduction rate both reach above 99.0%; and advantageous conditions are created for subsequent lead extraction from conversion slag.
Owner:CENT SOUTH UNIV

Method for producing silica white and lead sulfide with waste lead glass tubes as raw material

InactiveCN103172075AOvercoming Process ComplexityOvercoming Process Energy ConsumptionSilicaLead sulfidesDecompositionHigh energy
The invention discloses a method for producing silica white and lead sulfide with waste with lead glass tubes as a raw material, and aims at solving the problems of complicated technology, high energy consumption and easy generation of secondary pollution in the existing lead glass tube lead-extraction technologies. According to the method, firstly waste lead glass tubes are coarsely broken and fine ground to obtain fine ground waste lead glass, and then are added with a potassium hydroxide solution to react for 60-210 minutes under 80-200 DEG C, and leaching residues and lead-silicone contained leaching solution are obtained by filtration; the lead ion concentration in the lead-silicone contained leaching solution is measured, sodium sulfide is added inside based on the mol ratio of Pb/S=1 to react for 30-120 minutes under 60-80 DEG C, and lead sulfide and filtrate are obtained by filtration; the pH value of the filtrate is adjusted to 7-9 by carbon dioxide decomposition or adding acid liquid, so that gel is obtained and then is aged for 60-180 minutes and filtered, and silica white is obtained by drying the filter cake. The method has the advantages of modest reaction conditions, simple process flow, large waste consumption and the like, and is easily suitable for large-scale industrial production.
Owner:HANGZHOU DIANZI UNIV

Method for rapidly recovering rhenium, copper and lead from copper smelting waste acid and device for implementing method

The invention discloses a method for rapidly recovering rhenium, copper and lead from copper smelting waste acid and a device for implementing the method. According to the method, the copper smelting waste acid is subjected to lead removing through filtering, lead residues with the lead content higher than 55% are obtained and taken as lead extraction raw materials, the lead extraction raw materials are subjected to targeted rhenium precipitation, rhenium-rich residues are obtained and are subjected to hot-pressing oxidizing leaching, a rhenium-rich leaching agent is obtained, the rhenium-rich leaching agent after evaporation and concentration is subjected to KCl rhenium precipitation and recrystallization, potassium perrhenate is prepared, and a liquid obtained after rhenium precipitation is vulcanized for copper deposition. The device comprises a rhenium and copper precipitant storage tank, a precipitation tank, a flocculating agent storage tank, a flocculation reaction tank, a reaction kettle, an evaporation-crystallization device, a centrifugal separator, a waste acid anti-gravity-osmosis filter, a rhenium-rich copper residue anti-gravity-osmosis filter, a filter press, a rhenium and copper precipitation tank steam heating system, a copper precipitation tank steam heating system and a slurry pump. The method and the device have the characteristics of low investment, rapid and short procedures, simple and efficient operation, and high recovery rate, and are clean and environment-friendly.
Owner:ZIJIN MINING GROUP

Process for extracting tea saponin from tea seed cakes or meal

The invention relates to a process for extracting tea saponin from tea seed cakes or meal after oil frying by applying an industrial production device. The process comprises the following steps: crushing the tea seed cakes or the meal (leading the particle size to be 1-3mm), then sending into a steaming and stir-frying cauldron, drying (preventing the water content from exceeding 7%), then leading the material to enter into a material storage cylinder, using a screw conveyor to send the material into a rotocel extractor, and adding a solvent for extraction; carrying out residue-liquid separation (the meal residue can be used as a feed or a fertilizer) after double extraction, leading extraction solution to enter into a long pipe evaporator, removing part of water by double evaporation, and recycling the solvent (which can be recycled); and concentrating the extraction solution via a vacuum concentration tank, then crystallizing and drying, and obtaining a fine saponin finished productfor packaging and leaving a factory. A product produced by the process contains 81.5% of active matters, and the pH value is 5.9. Compared with other methods, the process has the advantages of high product purity, light color, high production rate (14%), energy conservation, low consumption, no pollution and environmental protection, and is easy for operation and the like.
Owner:ANHUI YINGSHANHONG BIOLOGICAL TECH
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