The application relates to a preparation method of a high-
porosity high-flux asymmetric membrane, and belongs to the field of membrane
separation technology. The preparation method of the high-
porosity high-flux asymmetric membrane comprises the following steps: uniformly dissolving a
polymer and a hydrophilic additive in an
organic solvent to prepare a homogeneous
casting solution; preparing a nascent membrane from the
casting solution; then, performing atomization pretreatment on the nascent membrane; rapidly cooling the nascent membrane after the pretreatment; then, immersing the nascent membrane in a gel bath to form an asymmetric membrane; and performing multiple flushing and soaking on the asymmetric membrane in normal-temperature deionized water to obtain the high-
porosity high-flux asymmetric membrane. The asymmetric membrane adopts a non-
solvent atomization technology combined with cooling-induced
crystallization, the non-
solvent atomization is introduced into the surface of the nascent membrane, the solution is rapidly saturated by accurate
temperature control, the
crystal formation is triggered, the macroporous pores are formed, and the
membrane porosity and flux are improved. The obtained asymmetric membrane has a macroporous
network on the
surface layer and a finger-shaped pore on the support layer, the porosity is 75% to 85%, the pure water flux is greatly improved, and the high-efficiency separation requirement is met.