According to the preparation method of the
metal interconnection structure provided by the invention, the
titanium nitride layer is formed twice, the first
titanium nitride layer formed before the
metal silicide layer is formed through high-temperature annealing for the first time and before the
metal layer is deposited for the second time can well isolate the lower
titanium layer, so that the titanium layer is prevented from being oxidized by contacting with
oxygen; although the first
titanium nitride layer may crack in the high-temperature annealing process, the second
titanium nitride layer continues to be formed on the surface of the first
titanium nitride layer after the high-temperature annealing and before the metal layer
deposition process, and the second titanium
nitride layer can effectively fill cracks formed in the first titanium nitride layer, so that in the metal layer
deposition process, the first titanium nitride layer is not prone to
cracking. According to the invention, the contact between deposition source gas for depositing the metal layer and the titanium layer below the titanium nitride layer can be effectively avoided, so that the generation of volcanic defects is reduced or even avoided, the
electrical performance of a subsequently formed metal
interconnection structure is effectively improved, and the product yield is ensured; in addition, the preparation method does not need to introduce additional
process equipment, and is easy to implement.