The invention discloses a method of preparing
nickel cobaltite /
carbon nanotube composite materials. The invention further relates to a method of preparing a
carbon nanotube loaded with nano-particles
nickel cobaltite. The method comprises the following steps of dissolving Ni(NO3)2.6H2O and Co(NO3)2.6H2O in diglycol to prepare a
mixed metal solution A containing Ni2+ / Co2+ with a mol ratio being 1:2; dissolving NaOH and a
carbon nanotube in the diglycol and performing
ultrasonic dispersion to form a solution B; making the solution B added in the solution A drop by drop to acquire a
mixed solution; fully and uniformly stirring the
mixed solution in a condition with a temperature of 80 DEG C, moving the solution to a reaction vessel and further replacing CO2, and after the replacement, adjusting the pressure intensity of the CO2 to be 10MPa; putting the reaction vessel in an
oil bath pan, setting the stirring rate to be 400r / min, the temperature to be 140-220 DEG C, and the reaction time to be 4-10h; cleaning the acquired product by
ethanol and
distilled water to be neutral and further performing
centrifugation and 80 DEC C
drying to acquire
nickel cobaltite / carbon
nanotube composite materials. The method which hardly damages the structure of the carbon
nanotube has the characteristics of simple operation and environment friendliness. By means of the method, products can be directly acquired in the solution without calcining. The acquired nickel cobaltite / carbon
nanotube composite materials have relatively high specific
capacitance and good
electrochemistry performance stability when applied to super
capacitor electrodes.