The invention relates to a preparation method of a
manganese-doped two-dimensional lead
halide perovskite material with the high
photoluminescence quantum yield. The preparation method mainly comprises the following steps that (1) haloid acid is added into organic amine according to a 1:1
molar ratio, and ice-bath stirring is conducted for 15 minutes; (2) the solution is placed in a 80 DEG C
drying oven overnight, till crystals are completely dissolved out; (3) the crystals are placed into the 80 DEG C
drying oven to be dried after being washed clearly with absolute ethyl
alcohol; and (4) organic halate, lead
halide and
manganese halide with certain proportion are added into a
mortar and uniformly ground, and an end product is obtained. The general formula of the prepared
manganese-doped lead halide
perovskite meets (C<n>H<2n+1>NH3)2Pb<1-x>Mn<x>X4, wherein the value of x is between 0.001 and 0.95, the lead halide
perovskite material has an excellent
optical property, the
luminescence center
wavelength is between 595 and 630 nm, and the
quantum yield emitted by Mn<2+> reaches 90%. By adjusting the
chain length and the structure of organic amine salt and sorts of halide ions, controlling of the
wavelength emitted by Mn<2+> is achieved, and the preparation method of manganese-doped two-dimensional lead halide perovskite is simple and rapid.