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55results about How to "Improve driving rate" patented technology

Phosphoric acid production tail gas recovery method

InactiveCN102258929AIncrease flow rateThe beneficial effect of increasing the first-level scrubber is: 1) reduce the flow rateDispersed particle separationPhosphoric acidRecovery methodPhosphoric acid
The invention relates to a method for recovering tail gas from phosphoric acid production. The process flow is as follows: the fluorine-containing gas enters the Venturi scrubber through the tail gas duct, and performs first-stage downstream spray washing with the washing liquid from the first washing pump, and the washed gas enters the first washing tower and the first washing tower. The washing liquid sent by the washing pump is subjected to the first-stage countercurrent two-layer spray washing again, and the gas after washing enters the second washing tower and the washing liquid sent by the second washing pump is subjected to the second-stage countercurrent two-layer spray washing. After being pumped by the tail gas fan, it enters the defoaming tower for defoaming, and finally discharges into the atmosphere through the chimney; the process water for washing first enters the second washing tower and is preheated and sprayed by the second washing pump, and then overflows from the second washing tower into The first washing tower is sent to the Venturi scrubber and the spraying device of the first washing tower by the first washing pump for spray washing and absorption. The beneficial effects of the present invention are: 1) reduce the gas flow rate, increase the washing and absorption efficiency; 2) preheat the washing liquid through the second washing tower, accelerate the formation of H2SiF6, and further strengthen the washing and absorption effect; 3) reduce the adhesion of the fan impeller, Reduce fan failures and corrosion of related equipment; 4) Strengthen the stability of operating indicators and increase the operating rate.
Owner:WUHAN ZHONGDONG PHOSPHATE TECH

Dehydration method during production process of toluene diisocynate

The invention belongs to the field of toluene diisocynate production technology and relates to a dehydration method during the production process of toluene diisocynate. Toluenediamine and phosgene have cold light gasification reaction to obtain a mixture flow of carbamyl chloride, amidogen hydrochloride and hydrogen chloride; the mixture flow flows into a phosgenation reaction tower; carbamyl chloride and amidogen hydrochloride react to produce toluene diisocynate and the by-product hydrogen chloride; at the bottom of a hydrogen chloride rectifying tower, the mixture flow of amidogen and hydrogen chloride is divided into two parts, most of the mixture flow returns to the top of the phosgenation reaction tower and serves as the backflow, and the rest of the mixture flow enters into a drain sump containing activated carbon as the catalyst; water and phosgene in the mixture flow react to produce hydrogen chloride and carbon dioxide to remove water in the mixture flow under the function of the activated carbon catalyst; the dehydrated mixture flow enters into the bottom of the phosgenation reaction tower for further rectification and is discharged from the bottom of the phosgenation reaction tower for next step. The dehydration technology is simple and environmentally friendly, the cost is low, and the dehydration effect is excellent.
Owner:QINGDAO UNIV OF SCI & TECH +1

Ammonium phosphate slurry pipeline compound dredging method

The invention discloses an ammonium phosphate slurry pipeline compound dredge method which includes a first step of installing a dredging device, wherein a flange mounting seat is arranged on an opening of the tail end of a pipeline for producing ammonium phosphate slurries, a flange plate is fixed on the flange mounting seat, and the dredging device is supported on the flange plate, a second step of spraying cleaning media, wherein a portion, located inside the pipeline, of the dredging device can carry out spraying of the cleaning media on the inner wall of the pipeline, and the cleaning media soaked with the dissolving slurries can dissolve scale layers on the inner wall of the pipeline, and a third step of carrying out dredging, pushing a dredging rod in the process of spraying the cleaning media, and enabling a cleaning disc to move to clean the inner wall of the pipeline. Through the method, the pipeline does not need to be dismantled, and workers can carry out on-line dredging on the clogged pipeline, so the ammonium phosphate slurry pipeline compound dredge method can greatly reduce labor intensity of the maintenance workers, improves working efficiency, reduces safety risks in the operation process of the maintenance workers, shortens down time, and improves on-stream rate.
Owner:中化重庆涪陵化工有限公司

Method for recycling waste product and by-product in sulfuric acid method titanium dioxide production

The invention relates to a method for recycling the waste product and by-product in sulfuric acid method titanium dioxide production which adopts a forced circulation system which contains a sulfuric acid circulating pump, a cooler and recycle acid pipelines to cool and mix sulfuric acid, and combines the processes of refrigeration, purification and preparation of concentrated sulfuric acid in the sulfuric acid method titanium dioxide production to only one process through filtration, thus greatly simplifying the production process and reducing the production cost and investment. Because the invention adopts big flow forced circulation technology, the temperature of circulating sulfuric acid and the temperature difference are lower so that the demand to the material of the sulfuric acid circulating pump is reduced and the service life is prolonged; besides, the flow velocity on the sulfuric acid side of the cooler in the forced circulation technology is higher so that the scaling forming speed on the sulfuric acid side of the cooler is slower and the operation rate is higher. The invention solves the problems of the sulfuric acid method titanium dioxide production that the flows of refrigeration, purification and preparation of concentrated sulfuric acid are long, the investment is large, the operation rate is low, the production cost and the maintenance cost are high and the like, and the obtained economic benefit is remarkable.
Owner:XIANGYANG LOMON TITANIUM IND CO LTD

Direct-current low-voltage 24V safe and energy-saving anti-dropping device for parking equipment

The invention discloses a direct-current low-voltage 24V safe and energy-saving anti-dropping device for parking equipment. The device mainly consists of a device loading and fixing structure, a power supply and signal feedback circuit, an electric energy and mechanical energy conversion structure, and an operation state LED (light-emitting diode) display lamp. In a using process of the device, a safety grab (in a power-off state) extends out, so that a car carrying board can be firmly grabbed during sudden failure to achieve safety protection effect; the device adopts a direct-current low-voltage 24V safety power supply to supply power, so that damages, during electric leakage, to a human body, equipment and the like can be avoided; the operation state LED display lamp is additionally arranged to display a device operation state in real time, so that a failure position can be conveniently found and maintenance is convenient. The direct-current low-voltage 24V safe and energy-saving anti-dropping device has the advantages of being energy-saving, environmentally-friendly, safe and reliable, compact in structure, simple to mount, and the like, is suitable for various forms of lifting and transverse-moving mechanical type stereo garages, and is used as a safety protection device of other mechanisms which possibly have dropping faults.
Owner:储华群 +3

High-yield hydrated crystalline phase reconstruction wet-process phosphoric acid production technology

The invention discloses a high-yield hydrated crystalline phase reconstruction wet-process phosphoric acid production technology. The technology comprises a semi-hydrated reaction filtration process and a dihydrate reaction filtration process, and the semi-hydrated reaction filtration process comprises the steps of premixing, dissolving, crystallizing, curing and semi-hydrated filtration; and the dihydrate reaction filtration process comprises a conversion step and a dihydrate filtering step. According to the invention, through gradient control of the relationship between the sulfate ion concentration and the CaO concentration in different stages of the semi-hydrated reaction, the crystal size is increased, the crystal is kept stable, and the semi-hydrated gypsum crystal with uniform particle size is obtained; by changing the circulation path of the slurry, the reaction retention time is prolonged, and the growth of semi-hydrated gypsum crystals in a relatively stable environment is ensured; coarse, uniform and stable dihydrate gypsum crystals are obtained by controlling the degree of supersaturation of a dihydrate reaction, the filtering performance is good, the content of water-soluble phosphorus in the dihydrate gypsum is reduced, and the filtering yield is improved; and by reasonably utilizing the filtrate and the flushing water, the wastewater discharge is reduced, and the total yield of P2O5 is increased.
Owner:WUHUAN ENG

Method of raising decomposition yield of cumyl hydroperoxide

The invention relates to a method for raising the decomposition yield of cumyl hydroperoxide of a phenol-acetone unit.The method includes the steps that 1, first-level decomposition liquid is recycled to a decomposer through a special distributor after being cooled; 2, a concentrated sulfuric acid catalyst is added into a decomposition liquid recycling system from two different points; 3, the concentration of sulfuric acid in the decomposer is lowered; 4, standing time of decomposition liquid in the decomposer is increased, and the reaction temperature of the decomposer is lowered; 5, standing time of the decomposition liquid in a second-level composer is increased; 6, the reaction temperature of second-level decomposition is increased; 7, flash evaporation is conducted on materials discharged through second-level decomposition to recycle energy, total or part of flash evaporation condensate liquid is recycled to the decomposer, and the remaining part is sent to a crude acetone tower on the downstream of the phenol-acetone unit; 8, part of decomposer steam condensate liquid is sent to a fine acetone tower on the downstream of the phenol-acetone unit or fed into a feeding tank.The method mainly solves the problems that by means of an existing phenol acetone production technology, the decomposition yield is low, a great number of tar by-products are generated, and a distilled fed material is high in salt content.
Owner:张殿豪

Rapid heating extraction method of extraction tank

ActiveCN103496684AReduce manufacturing costFast heating and thickening timePhosphorus compoundsFiltrationPhosphoric acid
The invention discloses a rapid heating extraction method of an extraction tank. The method comprises the steps: (1) after the extraction tank is cleared, complementing dilute phosphoric acid to a 1.5m position in the extraction tank; (2) starting stirring fans and tail gas fans in all regions, and keeping the extraction tank at micro-negative pressure; (3) respectively adding sulfuric acid and phosphoric ore pulp into the extraction tank at the speeds of 3m<3> / h and 5m<3> / h, heating and thickening, wherein the dilute phosphoric acid or sewage is complemented again into the heating process so that the liquid level of the extraction tank and the proportion of the extracted phosphoric acid are controlled; (4) when the extraction temperature is up to 60 DEG C, adjusting the negative pressure value of each tail gas fan, gradually increasing the adding amounts of the sulfuric acid and the phosphoric ore pulp, and shortening the heating and thickening times of the extraction tank; and (5) when the liquid level and all indexes of the extraction tank meet a filtrations condition, filtering and washing, collecting solids into a gypsum stockpile, collecting liquid into a phosphoric acid tank, and exhausting tail gas after the tail gas is washed and emptied by using a washing tower. The rapid heating extraction method has the advantages that the heating and thickening times are saved, reducing the production costs of enterprises is reduced, extraction reaction effect is good and the like.
Owner:山东聊城鲁西化工第五化肥有限公司

Dehydration method during production process of toluene diisocynate

The invention belongs to the field of toluene diisocynate production technology and relates to a dehydration method during the production process of toluene diisocynate. Toluenediamine and phosgene have cold light gasification reaction to obtain a mixture flow of carbamyl chloride, amidogen hydrochloride and hydrogen chloride; the mixture flow flows into a phosgenation reaction tower; carbamyl chloride and amidogen hydrochloride react to produce toluene diisocynate and the by-product hydrogen chloride; at the bottom of a hydrogen chloride rectifying tower, the mixture flow of amidogen and hydrogen chloride is divided into two parts, most of the mixture flow returns to the top of the phosgenation reaction tower and serves as the backflow, and the rest of the mixture flow enters into a drain sump containing activated carbon as the catalyst; water and phosgene in the mixture flow react to produce hydrogen chloride and carbon dioxide to remove water in the mixture flow under the function of the activated carbon catalyst; the dehydrated mixture flow enters into the bottom of the phosgenation reaction tower for further rectification and is discharged from the bottom of the phosgenation reaction tower for next step. The dehydration technology is simple and environmentally friendly, the cost is low, and the dehydration effect is excellent.
Owner:QINGDAO UNIV OF SCI & TECH +1

A method for manufacturing a high-temperature and corrosion-resistant graphitic acid distributor

The invention discloses a high-temperature-resistant corrosion-resistant graphitic acid distributor and a manufacturing method thereof. The graphitic acid distributor comprises an acid disc, wherein overflow pipes are uniformly distributed inside the acid disc; both the acid disc and the overflow pipes are made of graphite material. The acid distributor is made of the graphite material, the graphite has high-temperature resistance and corrosion resistance, the influence of temperature on the graphite material is slight, the deformation amount is small, the distribution uniformity of materials in tower equipment in chemical production is guaranteed, and bias of the materials in the tower equipment is reduced. Compared with the conventional acid distributor made of a polytetrafluoroethene material, the graphitic acid distributor manufactured by adopting the manufacturing method has the advantages that the temperature resistance and corrosion resistance are improved by 30 percent, the strength is improved by 5-10 times, the bias is reduced, the production consumption is lowered, the service life is prolonged by two times, the problem that the high-temperature highly corrosive materials are easily biased in the tower equipment is solved, and great contribution is made to the development of fluorine chemical industry and other petrochemical industries.
Owner:龚孝祥
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