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53results about How to "Control contact time" patented technology

Disk-type assembled bagged catalytic distillation filler

The invention relates to a disk-type assembled bagged catalytic distillation filler, which structurally comprises an assembly A and an assembly B, wherein the assembly A is a rectangular catalyst bag formed through seaming and is filled with catalyst particles; the assembly B is a regular filler sheet; and the regular filler sheet of the assembly B and the catalyst bag of the assembly A are tightly stacked in parallel and are curled into a disk-type spiral structure and then fixed by using a banding sheet to form the catalytic distillation filler. The catalyst bag is adjustable in seaming size, the loading density of the catalyst is adjustable, the content of the catalyst is adjusted and the utilization rate of the catalyst is improved. The assembly A and the assembly B are alternately arranged, so that flowing of a liquid is improved by the regular filler sheet, uniform distribution of gas and liquid phases is ensured, a reactant and a product are continuously separated to the tower top and the tower bottom, the mass transfer process is promoted and the reaction rate is improved. The catalytic distillation filler is of the disk-type spiral structure and the catalyst bag and the regular filler sheet are arranged at an interval, so that uniform distribution of gas and liquid phases is improved, and meanwhile, the pressure drop can be reduced.
Owner:TIANJIN UNIV +1

Liquid-phase hydrogenation reactor and hydrogenation process

The invention relates to a liquid-phase hydrogenation reactor and a hydrogenation process, the liquid-phase hydrogenation reactor comprises an inner cylinder and a reactor shell, the inner cylinder is conical, the top and the bottom of the inner cylinder are open, the edge of the bottom of the inner cylinder is hermetically connected with the inner wall of the reactor, and a plurality of small holes are formed in the wall of the inner cylinder; a ceramic membrane tube bundle is vertically arranged in the axial direction of the reactor and is communicated with external hydrogen; the inner cylinder is filled with a hydrogenation catalyst I, the annular cavity is filled with a hydrogenation catalyst II, and the activity of the hydrogenation catalyst I is higher than that of the hydrogenation catalyst II; the reactor raw material inlet communicates with the top of the inner cylinder; the materials flow in the inner cylinder from top to bottom; the materials flow in the annular cavity from top to bottom. According to the method, the contact time of the material and the catalyst in the whole hydrogenation reaction process can be effectively controlled, so that the temperature rise of a catalyst bed layer is more uniform, the problems of severe heat release and reaction conversion rate inhibition in the reaction process are solved, and higher hydrogenation reaction rate and conversion rate in the whole liquid-phase hydrogenation reaction process are achieved.
Owner:CHINA PETROLEUM & CHEM CORP +1

Heavy oil hydrogenation reactor and hydrogenation method

The invention discloses a heavy oil hydrogenation reactor and a hydrogenation method. The reactor comprises a reactor outer cylinder, an inner cylinder I and an inner cylinder II, the inner cylinder I and the inner cylinder II are arranged in the axial direction of the reactor, the cross sectional area of the inner cylinder I is gradually reduced from top to bottom, and the cross sectional area of the inner cylinder II is gradually increased from top to bottom; an annular space is formed among the inner cylinder I, the inner cylinder II and the reactor outer cylinder body; wherein the inner cylinder I is filled with a hydrogenation catalyst I, the annular space is filled with a hydrogenation catalyst II, and the activity of the hydrogenation catalyst I is higher than that of the hydrogenation catalyst II. The viscosity of the material is reduced through the viscosity reduction assembly arranged in the inner cylinder II, and then the material sequentially passes through the inner cylinder I and the annular space to generate hydrogenation reaction, so that the mass transfer process driving force and reaction rate of heavy oil liquid phase hydrogenation reaction are improved, the contact time of the reaction material and different active catalysts is controlled, and catalyst surface coking is slowed down; the deep cracking reaction of the light oil is reduced, and the liquid yield and the heavy impurity removal conversion rate in the heavy oil liquid phase hydrogenation reaction process are improved.
Owner:CHINA PETROLEUM & CHEM CORP +1

Hydrogenation reactor and hydrogenation method thereof

The invention discloses a hydrogenation reactor and a hydrogenation method thereof. The hydrogenation reactor comprises an inner cylinder and a reactor shell, the inner cylinder is conical, and an annular space is formed between the inner cylinder and the reactor shell; the edge of the bottom of the inner cylinder is connected with the inner wall of the reactor in a sealed manner; the inner cylinder is filled with a hydrogenation catalyst I, the annular space is filled with a hydrogenation catalyst II, and the activity of the hydrogenation catalyst I is higher than that of the hydrogenation catalyst II; a hydrogen supplementing assembly is horizontally arranged in the reactor; a reactor raw material inlet is communicated with the bottom of the inner cylinder; a reactor product outlet is communicated with the lower part of the annular space; the material flows in the inner cylinder from bottom to top; and the material flows in the annular space from top to bottom. The method can effectively control the contact time of the material and different active catalysts in different temperature sections in the hydrogenation reaction, realizes the purposes of rapid reaction in low and medium temperature sections and inhibition of side reaction in high temperature sections, and improves the hydrogenation reaction rate and reaction depth.
Owner:CHINA PETROLEUM & CHEM CORP +1

Method for treating low-concentration VOCs (Volatile Organic Compounds) and achieving deodorizing through electrocatalytic oxidation

The invention belongs to the field of waste gas VOCs treatment, and particularly relates to a method for treating low-concentration VOCs and achieving deodorizing through electrocatalytic oxidation, and the method specifically comprises the following steps: adding an electrolyte into water to prepare an ionic electrolyte with a certain concentration; conducting spraying in a mist form according to a certain direction; and enabling VOCs gas to reversely enter a special spray tower according to a certain flow rate, making the VOCs gas full contact with the electrolyte, keeping the spraying direction of the VOCs opposite to the direction of sprayed ionic liquid, and introducing direct current voltage into a mixed liquid tank where the VOCs gas is in contact with the ionic liquid. Therefore, the method for treating the low-concentration VOCs and deodorizing is obtained. According to the invention, by controlling the proportion of current to voltage, the intensity of an electric field is controlled, and the VOCs gas is electrically catalyzed; and the VOCs gas is effectively treated by controlling the contact time of the gas and the conductive liquid by adopting small-opening gas entering and large-opening gas flowing out.
Owner:江门市绿一茵环保科技有限公司

A green synthesis device for 4-chloroacetoacetates

The invention discloses a green synthesis device for 4-chloroacetoacetate, which comprises a sealed heat-insulating shell, a conductive cylinder is arranged inside the heat-insulating shell, and the upper and lower ends of the conductive cylinder are connected with the inner cavity of the heat-insulating shell. The upper and lower sides are sealed and fixedly connected. An electrostatic generator is installed outside the insulation shell. The output end of the electrostatic generator is connected to the side of the conductive cylinder through a cable, and the cable runs through the insulation shell. The upper part of the inner cavity of the conductive cylinder is equipped with an electrostatic Sprayer, a precooler is installed on the outside of the conductive cylinder; this green synthesis device of 4-chloroacetoacetates electrostatically atomizes the diketene solution to increase the contact area between the diketene solution droplets and chlorine gas, and double The downward movement distance of the diketene solution droplet determines the reaction time of the diketene solution droplet and chlorine gas, the reaction time of diketene solution and chlorine gas is easy to control, reduces the generation of by-products, and avoids the loss of raw materials.
Owner:山东昌邑灶户盐化有限公司

Equipment for preparing catalytic cracking catalyst

The invention relates to equipment for preparing a catalytic cracking catalyst, which comprises a tubular reactor, a gas-solid separator, an absorption column, a beating machine and a nodulizer, wherein the tubular reactor comprises a first feeding hole, a discharging hole and a tube body, and the first feeding hole and the discharging hole are respectively positioned at two end parts of the tubebody; the tubular reactor is communicated with the gas-solid separator through the discharging opening, the upper part and the lower part of the gas-solid separator are respectively communicated withthe absorption column and the beating machine, the position where the gas-solid separator is connected with the discharging hole is lower than that where the gas-solid separator is connected with theabsorption column, and the nodulizer is used for receiving materials from the beating machine. The equipment for preparing the catalytic cracking catalyst, provided by the invention, can realize continuous operation of the contact reaction of the molecular sieve and SiCl4, and can control the contact time of the molecular sieve and the SiCl4 through controlling the length of the tubular reactor and the flow speed of the carrier gas, thereby being capable of enabling the contact reaction of the molecular sieve with the SiCl4 to be fully carried out in the tubular reactor.
Owner:CHINA PETROLEUM & CHEM CORP +1

Green synthesis device of 4-chloroacetoacetate

The invention discloses a green synthesis device of 4-chloroacetoacetate. The synthesis device comprises a sealed thermal insulation shell; an electro-conductive barrel is arranged in the thermal insulation shell; the upper end and lower end of the electro-conductive barrel are hermetically and fixedly connected with the upper side and lower side of the inner cavity of the thermal insulation shellrespectively; an electrostatic generator is arranged outside the thermal insulation shell, the output end of the electrostatic generator is connected with the side face of the electro-conductive barrel through a cable, the cable penetrates through the thermal insulation shell, an electrostatic sprayer is arranged in the upper portion of the inner cavity of the electro-conductive barrel, and a pre-cooler is installed outside the electro-conductive barrel. The green synthesis device atomizes a diketene solution through static electricity, the contact area between liquid drops of the diketene solution and chlorine is increased, the time of reactions between the liquid drops of the diketene solution and chlorine is determined by the downward moving distance of the liquid drops of the diketenesolution, the time of reactions between the diketene solution and chlorine is convenient to control, byproducts are reduced, and raw material loss is avoided.
Owner:山东昌邑灶户盐化有限公司

A liquid phase hydrogenation reactor and hydrogenation process

The invention discloses a liquid-phase hydrogenation reactor and a hydrogenation process, comprising an inner cylinder and a reactor shell, the inner cylinder is conical, the top and bottom of the inner cylinder are open, the bottom edge is tightly connected with the inner wall of the reactor, and the inner cylinder is open. A number of small holes are opened on the cylinder wall; a ceramic membrane tube bundle is vertically arranged on the axial direction of the reactor, and the ceramic membrane tube bundle communicates with external hydrogen; the inner cylinder is filled with hydrogenation catalyst I, the annular cavity is filled with hydrogenation catalyst II, and hydrogenation catalyst I The activity of the catalyst is higher than that of the hydrogenation catalyst II; the inlet of the raw material of the reactor is connected to the top of the inner cylinder; the flow mode of the material in the inner cylinder is from top to bottom; the flow mode of the material in the annular cavity is from top to bottom. The invention can effectively control the contact time between the material and the catalyst in the whole process of the hydrogenation reaction, make the temperature rise of the catalyst bed more uniform, solve the problems of severe exotherm and inhibit the reaction conversion rate in the reaction process, and realize the whole liquid phase hydrogenation reaction process Both achieve higher hydrogenation reaction rate and conversion.
Owner:CHINA PETROLEUM & CHEM CORP +1
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