This invention belongs to the field of
flame retardant technology, and provides a reactive
phosphorus-containing
flame retardant, a resin composition, its preparation method, and its application. The preparation method includes: (1) dissolving DOPO-Cl and DPO-Cl in a first reaction
solvent to obtain a premix; (2) sequentially transferring 2-butynedi-1,4-
diol, a base-binding acid, and a second reaction
solvent to a
constant pressure dropping funnel to obtain a
mixed solution, adding the
mixed solution dropwise into the premix and reacting to obtain a reaction solution; (3) adding a
quenching agent to the reaction solution and extracting, washing the
organic layer,
drying, filtering, concentrating, and separating the crude product to obtain the final product. This
flame retardant has high and long-lasting flame retardant efficiency, and also possesses excellent
dielectric properties, compatibility, and
heat resistance. The preparation method has mild synthesis conditions, low cost, and is easy to implement. The resin composition prepared from this flame retardant has the application prospect of preparing
copper-clad laminates.