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57results about How to "Improve mechanical bonding" patented technology

Preparation method of flexible self-supporting silicon/graphene cathode material of lithium ion battery

The invention discloses a preparation method of a flexible self-supporting silicon/graphene cathode material of a lithium ion battery. The method comprises the following steps: I, dispersing nano silicon particles in a mixed solution to be heated and cleaned and centrifugalized; II, dispersing the centrifugalized precipitate in a polydiene dimethyl ammonium chloride solution to obtain the nano silicon particles with positive charges; III, dropwise adding the nano silicon particles into a graphene oxide solution and carrying out suction filtration to obtain a silicon/graphene oxide composite film; and IV, thermally treating the silicon/graphene oxide composite film at a high temperature to obtain the flexible self-supporting silicon/graphene cathode material. The nano silicon particles withpositive charges and the graphene oxide with negative charges are self-assembled statically to botain the flexible self-supporting silicon/graphene cathode material which is excellent in mechanical flexibility. An electrode of the lithium ion battery can be directly prepared without adding a binder and conducting carbon black, so that the problem that the electrochemical property is reduced by adding the binder is solved, and the service life of the lithium ion battery is prolonged while the high capacity of the lithium ion battery is ensured.
Owner:XIAN UNIV OF SCI & TECH

Magnesium alloy implant composite material and preparation method and application thereof

The invention discloses a magnesium alloy implant composite material and a preparation method and application thereof. The magnesium alloy implant composite material is prepared by the following steps of: by taking a model manufactured from magnesium alloy powder through 3D printing as a magnesium alloy implant substrate, forming a micro-arc oxidation layer on the surface of the magnesium alloy implant substrate through a micro-arc oxidation method; then forming a hydroxyapatite layer or a hydroxyfluorapatite layer on the surface of the micro-arc oxidation layer by means of an electrochemical deposition method; and finally, immersing the surface of the hydroxyapatite layer or the hydroxyfluorapatite layer to form a polylactic acid layer. According to the material provided by the invention, individual development of the magnesium alloy implant material is realized from data acquisition of an original damaged bone structure to preparation of a final multi-coating composite material, so that the high quality magnesium alloy implant composite material is obtained. A polarizing test shows that the anti-corrosive property of the material can be enhanced by four orders of magnitudes, and osteoblast cultivation shows that the magnesium alloy composite material has a better osteocyte promoting ability.
Owner:ZHEJIANG UNIV OF TECH

Preparation method of titanium surface multilevel porous structure

In order to solve the problems that existing titanium and titanium alloys have low bioactivity and low bonding strength with bone tissues, the invention relates to a preparation method of a titanium surface multilevel porous structure. The method comprises: 1. polishing a titanium material by 240-mesh, 600-mesh and 1000-mesh metallographical sandpaper hierarchically, then performing ultrasonic cleaning with acetone and alcohol in order at room temperature, and conducting drying so as to obtain a treated titanium material; 2. carrying out sand blasting treatment with aluminum oxide particles; 3. soaking the titanium material subjected to the sand blasting treatment in a sulfuric acid solution; 4. taking the acid-etched titanium material as the anode, and taking platinum as the cathode, placing them in an NH4F aqueous solution, and conducting anodic oxidation treatment, thus obtaining the anode oxidized titanium material; and 5. cleaning the anode oxidized titanium material with an NaOH solution, deionized water and anhydrous ethanol, and performing drying, thus obtaining the titanium surface multilevel porous structure with high bioactivity and high bonding strength with bone tissues. The method provided in the invention is applied in the biomedical field.
Owner:HARBIN INST OF TECH

Titanium alloy implant composite material and preparation and application thereof

The invention discloses a titanium alloy implant composite material and preparation and an application thereof. The titanium alloy implant composite material is prepared by the following steps of: by taking a model manufactured from titanium alloy powder through 3D printing as a titanium alloy implant substrate, forming a micro-arc oxidation layer on the surface of the titanium alloy implant substrate through a micro-arc oxidation method; then forming a hydroxyapatite layer or a hydroxyfluorapatite layer on the surface of the micro-arc oxidation layer by means of an electrochemical deposition method; and finally, immersing the surface of the hydroxyapatite layer or the hydroxyfluorapatite layer to form a polylactic acid layer. According to the material provided by the invention, individual development of the titanium alloy implant material is realized from data acquisition of an original damaged bone structure to preparation of a final multi-coating composite material, so that the high quality titanium alloy implant composite material is obtained. A polarizing test shows that the anti-corrosive property of the material can be enhanced by 2-3 orders of magnitudes, and osteoblast cultivation shows that the titanium alloy composite material has a better osteocyte promoting ability.
Owner:ZHEJIANG UNIV OF TECH

Coating method capable of improving wear resistance of polyester harness cord

The invention relates to a coating method capable of improving wear resistance of a polyester harness cord. The method comprises the following steps: waterborne polyurethane size is taken as coating size, the pretreated polyester harness cord is impregnated in the coating size for padding, then drying and heat setting are performed, and the coated polyester harness cord is obtained; or the waterborne polyurethane size is taken as pre-applied primer size, another size is taken as the coating size, the pretreated polyester harness cord is impregnated in the pre-applied primer size for padding, and drying is performed; then the polyester harness cord is impregnated in the coating size for padding, drying and heat setting are performed, and the coated polyester harness cord is obtained. Selected waterborne polyurethane is safe, non-toxic and good in film forming property, the solubility parameter of waterborne polyurethane is close to that of polyester, and waterborne polyurethane has excellent adhesion and can effectively improve the adhesion effect between other coatings and polyester fibers; permeability of the polyester harness cord is good, coated property is good, and a uniform coating which is smooth, soft, not prone to yellowing and is resistant to wear, heat and light can be formed on the surface of the polyester harness cord.
Owner:DONGHUA UNIV

Preparation method for silicon carbide fiber bundle enhanced aluminum matrix composite

The invention discloses a preparation method for a silicon carbide fiber bundle enhanced aluminum matrix composite. Quartz fiber bundles are adopted to be woven into fiber cloths, the fiber cloths and graphite powder are pressed in a layered mode to form silicon carbide fiber cloths, aluminum or an aluminum alloy foil and the silicon carbide fiber cloths are subjected to layered alternate overlapping, a prefab before composite pressing and sintering is obtained, the prefab is subjected to pressing, sintering and cooling, and a filament silicon carbide fiber bundle net-shaped enhanced aluminum matrix composite is obtained. The volume fraction of silicon carbide fiber in the prepared silicon carbide fiber bundle net-shaped enhanced aluminum matrix composite is 50-60%. The compactness of the composite is 95.5-98.7%, the density is 2.80-2.90 g/cm<3>, the anti-bending elasticity modulus is 109-136 Gpa, the heat conductivity of the composite is high and not less than 170 W/(m.K), and the coefficient of thermal expansion is (8.5-12.5)x10<-6> / K and adjustable. Compared with a current used aluminum silicon carbide composite, the heat conductivity is high, the volume fraction of an enhancesome SiC is large, and the cost of the silicon carbide fiber bundle enhanced aluminum matrix composite is lower than the cost of an aluminum diamond composite.
Owner:武汉强英新材料有限公司

Thermoplastic composite pipe with sealing and buckling joint, and manufacturing method

The invention discloses a thermoplastic composite pipe with a sealing and buckling joint, and a manufacturing method. The thermoplastic composite pipe comprises a buckling joint comprising a core pipe, and the outer diameter of the right side of the core pipe is smaller than the outer diameter of the left side of the core pipe; the right outer wall of the core pipe is sheathed with a casing, and the inner wall of the sleeve is provided with a sawtooth groove; the outer wall of the core pipe is provided with a sawtooth groove, and an assembly cavity is formed between the inner wall of the casing and the outer wall of the core pipe, and fit to the wall size of the composite pipe on the right side of the buckling joint; and the outer wall of the sawtooth groove in the outer wall of the core pipe and the inner wall of the sawtooth groove in the inner wall of the casing are both provided with shape memory alloy rings of which the outer walls are fit to the composite pipe, so that the mechanical binding force between the metal core pipe or the casing and the composite pipe is improved effectively, and the purpose of improving the sealing performance of the buckling joint is achieved. Themethod is simple and effective, and high in manufacturing efficiency, and additional energy consumption is not required.
Owner:TUBULAR GOODS RES INST OF CNPC +1

Conductive composite material and preparation method thereof, and preparation method for conductive line

The invention discloses a conductive composite material and a preparation method thereof, and a preparation method for a conductive line. The conductive material comprises a substrate, and metal particles uniformly dispersed in the substrate, the diameter of the metal particles is from 100 nm to 10 <mu>m, the substrate is polymer resin, and the metal particles are metal particles with three-dimensional fractal layered structures. The conductive material is used for laser etching, the micro-nano metal particles with the three-dimensional fractal layered structures are employed as the conductive filling material, the unique geometric shapes of the metal particles are employed so that ablation occurs more easily under the effect of laser compared with conventional filling material particles, and finer wiring effect can be realized under low laser power; the same conductivity is reached by adopting less metal particles than the conventional filling material particles so that the required laser etching energy is less; and the content of the metal particles is less so that the bonding force in conductive slurry and the bonding force between the conductive slurry and a matched insulation substrate can be both greatly increased.
Owner:SHENZHEN GRADUATE SCHOOL TSINGHUA UNIV

Composite fiber based on luminescent metal organic frame material and preparation method thereof, and application to multi-parameter distributed fiber fluorescence sensing system

The invention discloses a composite fiber based on a luminescent metal organic frame material and a preparation method thereof, and an application to a multi-parameter distributed fiber fluorescence sensing system. The system includes an excitation light source, a fiber coupler, a delay fiber, sensing units, a long pass filter, a fluorescence spectrometer and a signal processing unit, wherein thesensing unit is a luminescent MOFs composite fiber prepared through a casing method, and the multi-parameter distributed fiber fluorescence sensing network can be formed by cascading and paralleling the multiple sensing units containing different luminescent MOFs. The system is advantaged in that composition of the luminescent MOFs and the fibers is realized, the method is simple, cost is low, thesensing units for detecting different analytes can be prepared according to actual needs and are combined with other optical instrument components to form a sensing system, further real-time in-situremote online fluorescence detection and sensing are realized simultaneously at multiple points, and the sensing application of the illuminating MOFs is greatly improved.
Owner:SOUTH CHINA UNIV OF TECH

Multifunctional surface enhanced Raman substrate material, and preparation method and application thereof

The invention discloses a multifunctional surface enhanced Raman substrate material, and a preparation method and an application thereof. The material is formed by combining a nylon filter membrane and nano-silver embedded into micropores of the nylon filter membrane. The preparation method comprises the following steps: (1) preparing AgNPs suspension liquid; (2) pretreating the nylon filter membrane: firstly carrying out pretreatment by using oxygen, and then carrying out cleaning by using plasmas; (3) preparing a multifunctional surface enhanced Raman substrate: carrying out solid-liquid separation on the AgNPs suspension liquid prepared in the step (1) in a vacuum suction filtration mode through the nylon filter membrane obtained in the step (2), then taking out the nylon filter membrane embedded with AgNPs, and carrying out air drying. The vacuum suction filtration method is adopted; the packaging performance is good, the stability is improved; the substrate distribution is uniform; the sensitivity is high; the signal consistency is good; the nylon filter membrane is adopted as a carrying material; the anti-friction performance is achieved; the material can be repeatedly used;the cost is low; and the preparation process is simple. Meanwhile, the multi-appearance and multi-function design is also suitable for practical application in the POCT field.
Owner:FOOD INSPECTION CENT OF CIQ SHENZHEN +1

Metal foil current collector for battery

ActiveCN107681159AExcellent intrinsic conductivity and mechanical self-dispersion propertiesAvoid microcoalescingElectrode carriers/collectorsCvd grapheneMetal foil
The invention discloses a metal foil current collector for a battery and belongs to the technical field of electrochemistry. The metal foil current collector is technically characterized in that a nano carbon coating is arranged on the surface of the metal foil current collector; and the coating contains a graphene carbon nanotube hybrid prepared through a high-temperature chemical vapor deposition method. Graphene and a carbon nanotube in the graphene carbon nanotube hybrid are connected through a form of a covalent bond, so that the metal foil current collector has excellent intrinsic conductivity and mechanical self-dispersion characteristics, and micro coalescence of a carbon nanostructure is avoided. In assembly and operation processes of the battery, direct mechanical bonding and conductive interconnection of the current collector and positive active material particles can be effectively improved and the wetting characteristics of an electrolyte can be strengthened through the nano carbon coating on the surface of the metal foil current collector; and the metal foil current collector has important value to reduction of the impedance characteristic of the battery and improvement of the high current charge-discharge capability and the cycling stability of the battery.
Owner:TSINGHUA UNIV

Abrasion-resistant and ultraviolet-aging-resistant epoxy composite material and preparation method thereof

The invention provides an abrasion-resistant and ultraviolet-aging-resistant epoxy composite material and a preparation method thereof. The abrasion-resistant and ultraviolet-aging-resistant epoxy composite material is prepared from the materials of an epoxy resin matrix material and a TiO2 / Ti3C2 nano-composite material uniformly dispersed in the epoxy resin matrix material, wherein the TiO2 / Ti3C2nano-composite material accounts for 0.1-3 wt% of the epoxy resin matrix material, and the epoxy composite material is obtained by curing the TiO2 / Ti3C2 nano-composite material and epoxy resin in thepresence of a quaternary ammonium salt. The preparation method of the epoxy composite material is simple, and raw materials are easily available. The abrasion-resistant and ultraviolet-aging-resistant epoxy composite material prepared by the preparation method has a lower abrasion rate than ordinary epoxy materials, and meanwhile the ultraviolet-aging resistance is excellent, the tensile strengthis further improved to a certain extent, and the abrasion-resistant and ultraviolet-aging-resistant epoxy composite material is particularly suitable for being used in abrasion-resistant devices, such as the manufacture of abrasion-resistant automotive parts and abrasion-resistant sports equipment.
Owner:JIAXING UNIV

Preparation method of phenyl-polysilsesquioxane modified meta-aramid insulating paper

The invention relates to a preparation method of phenyl-polysilsesquioxane modified meta-aramid insulating paper, and belongs to the technical field of insulating materials. According to the method, phenyl-polysilsesquioxane (PPSQ) and meta-aramid fibers are modified, a conventional paper sheet forming method is adopted, and a modified insulating paper handsheet is obtained through the processes of dispersion in deionized water, fiber dissociation, mixing and stirring, filtering, papermaking, paper forming, drying, hot pressing and the like. Due to the addition of the PPSQ, a larger structuralspace is locally provided for the meta-aramid fibers, the free volume of the whole system is increased, the intermolecular structure of the meta-aramid fibers is improved, the tightness between molecular chains of the meta-aramid fibers is enhanced, the structure between paper becomes more compact, the interpermeability between the chains of the aramid fibers is further enhanced, the stress can be better transferred, the performance loss such as interphase layering is effectively prevented, and the bonding capacity between macromolecules of the aramid fibers is firmer. And meanwhile, the insulating paper prepared by the method has relatively high thermal aging resistance, and the thermal stability and the like are also improved.
Owner:SOUTHWEST UNIVERSITY

A kind of preparation method of silicon carbide fiber bundle reinforced aluminum matrix composite material

The invention discloses a preparation method for a silicon carbide fiber bundle enhanced aluminum matrix composite. Quartz fiber bundles are adopted to be woven into fiber cloths, the fiber cloths and graphite powder are pressed in a layered mode to form silicon carbide fiber cloths, aluminum or an aluminum alloy foil and the silicon carbide fiber cloths are subjected to layered alternate overlapping, a prefab before composite pressing and sintering is obtained, the prefab is subjected to pressing, sintering and cooling, and a filament silicon carbide fiber bundle net-shaped enhanced aluminum matrix composite is obtained. The volume fraction of silicon carbide fiber in the prepared silicon carbide fiber bundle net-shaped enhanced aluminum matrix composite is 50-60%. The compactness of the composite is 95.5-98.7%, the density is 2.80-2.90 g / cm<3>, the anti-bending elasticity modulus is 109-136 Gpa, the heat conductivity of the composite is high and not less than 170 W / (m.K), and the coefficient of thermal expansion is (8.5-12.5)x10<-6> / K and adjustable. Compared with a current used aluminum silicon carbide composite, the heat conductivity is high, the volume fraction of an enhancesome SiC is large, and the cost of the silicon carbide fiber bundle enhanced aluminum matrix composite is lower than the cost of an aluminum diamond composite.
Owner:武汉强英新材料有限公司

Forming method of composite material tie rod and composite material tie rod

The invention relates to the technical field of tie rod forming. The forming method of the composite pull rod comprises step A, preparation of winding forming mold and positioning of metal joints; design and preparation of winding forming mold, and engraved lines are designed on the outer surface of the winding forming mold in the circumferential direction; step B, winding of dry fiber yarn; Fiber winding equipment is used to wind according to the winding law; step C, resin infusion molding of the tie rod; after the tie rod is wound and formed with dry fiber yarn, it is placed in the resin infusion mold together with the winding molding mold, and then the resin material is poured, and the resin infusion mold is placed Heating and curing in an oven, curing and demoulding to obtain a semi-finished product; step D, processing the tie rod; processing the length of the tie rod and internal thread along the position of the metal joint of the tie rod. The composite pull rod includes metal joints, dry fiber yarns, and a cured integrally formed structure of resin materials; it solves the problems of existing tie rods that are prone to failure connection at the joint position and insufficient structural strength.
Owner:NORTH CHINA INST OF AEROSPACE ENG
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