The invention discloses a method for preparing a SiC-based multiphase
ceramic solidified body, which is characterized in that the steps are: using ZnO, CaO, Al 2 o 3 , SiO 2 As a
raw material, ZCAS glass is obtained by ball milling,
drying, calcining, ball milling, and
drying; SiC-ZCAS composite
powder is obtained by ball milling,
drying, and calcining using
silicon powder,
graphite, and ZCAS glass as raw materials; Adding
polyvinyl alcohol sol, mixing, granulating, and pressing to shape; heat-treating the shaped
green body and
sintering it in a vacuum hot-pressing
sintering furnace to obtain a SiC-based multiphase
ceramic solidified body. The invention adopts safe and cheap raw materials, simple and practical vacuum
hot pressing sintering technology, and prepares a SiC-based multiphase
ceramic solidified body with excellent
radiation resistance stability,
chemical stability,
mechanical stability and
thermal stability at a relatively low temperature. The SiC-based multiphase ceramic solidified body prepared by the invention is suitable for safe treatment of high-radioactive
graphite waste produced by decommissioning of nuclear reactors.