34results about How to "Strong resistance to hydration" patented technology

The invention discloses a magnesium aluminate spinel enhanced magnesia-based foamed ceramic filter with capability of realizing sintering at low temperature, excellent chemical stability and excellentthermal shock resistant performance, and a preparation method thereof. The preparation method comprises the following steps that (1) 10 to 20 percent of nanometer alumina sol, 0.8 to 1.5 percent of rheological agents and the balance of magnesium oxide ceramic powder containing a nanometer aluminum oxide sintering aid are proportioned; deionized water is added; ball milling and uniform mixing areperformed; then, through vacuum exhaust, ceramic slurry with the solid content being 60 to 70 percent is prepared; (2) a polyurethane foamed plastic template is soaked into the ceramic slurry; the polyurethane foamed plastic template is extruded through a roller press for removing the redundant leaching hanging slurry; then, biscuit is prepared; then, the biscuit is heated to 80 to 120 DEG C for drying; (3) the dried biscuit is put into a sintering furnace; the temperature is raised to 1400 to 1600 DEG C; high-temperature sintering is performed; cooling is performed along with the furnace to room temperature; the magnesia-based foamed ceramic filter is obtained.

The invention provides a nano-matrix-combined high-performance fused magnesium calcium brick and a manufacturing method thereof. The fused magnesium calcium brick is prepared from 8-5mm high-calcium fused magnesium calcium sand, 5-2mm high-calcium fused magnesium calcium sand, 2-0mm high-calcium fused magnesium calcium sand, <=0.074mm high-calcium fused magnesium calcium sand, 8-5mm fused magnesite, 5-2mm fused magnesite, 2-0mm fused magnesite, <=0.074mm fused magnesite fine powder, nano sea water magnesia fine powder and a binder paraffin. The manufacturing method comprises the following steps: fine powder premixing, integral compounding, molding, drying, firing and the like. The product has the advantages of compact microstructure, fewer low-melting-point minerals, higher erosion resistance, higher scour resistance, higher stripping resistance and higher hydration resistance. The furnace life is prolonged by 30% above on average. Thus, the product satisfies the requirements of high efficiency, long service life and high cleanness for stainless steel and special steel smelting, and lowers the cost for the steel enterprises.

The invention relates to the field of preparation of refractory materials, particularly a method for preparing high-quality calcium magnesia by superhigh-temperature calcination, which is characterized by comprising the following steps: preparing dolomite and magnesite into a raw material in which the CaO content is 15-20 wt% and the MgO content is 80-85%; adding the raw material into a ball milling tank, grinding and mixing, and meanwhile, adding water to carry out slaking and slurrying; and drying the slurry, adding calcium lignosulphonate, evenly mixing, pressing into green bricks, and calcining. The calcination process comprises the following steps: heating to 1100 DEG C, keeping the temperature for 3-5 hours, heating to the final calcination temperature of 2000-2200 DEG C, keeping the temperature for 5-7 hours, vacuumizing, cooling with water to 1000 DEG C, introducing protective hydrogen, and continuing cooling with water to room temperature. Compared with the prior art, the calcium magnesia has the advantages of high hydration resistance and high corrosion resistance, thereby basically solving the problem of high hydration tendency in the magnesium-calcium refractory material, and facilitating the storage, transportation, building and the like in future.

The invention relates to a preparation process of a high-voltage anode foil for a contracted ox horn type aluminum electrolytic capacitor. The preparation process comprises the following steps: (1) first-stage feeding; (2) high-temperature water boiling of an aluminum foil sheet; (3) first-stage formation; (4) second-stage formation; (5) second-stage feeding; (6) third-stage formation; (7) fourth-stage formation; (8) third-level feeding; (9) five-stage formation; (10) six-stage formation; (11) first phosphoric acid treatment; (12) first rear end repairing; (13) second phosphoric acid treatment; (14) second rear end repairing; (15) sheet firing; (16) third rear end repairing; (17) post-treatment; and (18) drying treatment. According to the preparation process of the high-voltage anode foilfor the contracted ox horn type aluminum electrolytic capacitor, the aluminum foil with high capacity, high strength, low electric leakage and high hydration resistance can be prepared.

The invention, which belongs to the technical field of the electrolyte, particularly relates to an electrolyte for a low-corrosivity electrolytic condenser and a method for making the same. The electrolyte is mainly composed of ethylene glycol, ammonium adipate, ammonium formate, additives and ultrapure water. The additives consist of ethylene glycol, diammonium hydrogen phosphate, phosphoric acid, p-nitrobenzoic acid, ammonium 4-nitrobenzoate dihydrate, a complexing agent, an interfacial agent and a corrosion inhibitor. The electrolyte which is suitable for a low-voltage electrolytic condenser has advantages of high frequency, low impedance, low electric leakage, and low corrosivity. According to the electrolyte, the service life of the electrolytic condenser is prolonged effectively by suppressing a hydration degradation reaction of an electrode aluminum foil and re rising of leak currents; and with the electrolyte, bottom heaving of the electrolytic condenser is avoided and thus the safety of the electrolytic condenser is enhanced substantially.

The invention belongs to the technical field of electrolytes, and particularly relates to a low-resistivity electrolytic capacitor-used electrolyte and a preparation method thereof. The low-resistivity electrolytic capacitor-used electrolyte provided by the invention is mainly composed of ethylene glycol, ammonium adipate, ammonium formate, additives and ultrapure water, wherein the additives comprises ethylene glycol, ammonium dihydrogen phosphate, phosphorous acid, silicon dioxide, a complexing agent, a surfactant and a hydrogen removing agent. The low-resistivity electrolytic capacitor-used electrolyte is applicable to a low-voltage electrolytic capacitor, and has the advantages of high frequency, low impedance, low electric leakage and low corrosivity; the electrolyte can restrain a hydration deterioration reaction of an electrode aluminum foil and rebound of leakage current, can also prevent an electrolytic capacitor floor heave phenomenon and can effectively prolong the service life of the electrolytic capacitor.

The invention relates to a high-quality dolomite-periclase-calcium zirconate composite fireproof material suitable for smelting stainless steel, special steel AOD furnace and refining ladles. The adopted raw materials mainly comprise, by weight, 8-10% of magnesium calcium sand with a particle size of 5-8 mm, 9-18% of magnesium calcium sand with a particle size of 3-5 mm, 10-22% of magnesium calcium sand with a particle size of 1-3 mm, 5-10% of calcium zirconate with a particle size of 0.5-1 mm, 5-10% of magnesia with a particle size of 0.5-1 mm, 3-10% of 600 mesh electric melting calcium zirconate, 15-24% of magnesia with a particle size of less than or equal to 0.5 mm, 3-10% of 400 mesh 98 large crystal magnesia, 1-3% of a binding agent, and 1-2% of a sintering agent, wherein the raw materials are subjected to mixing, molding, sintering, finished product inspection, package and other steps to prepare the material.

The invention belongs to the technical field of refractories for steel smelting furnaces, and in particular relates to a zirconium composite high-performance electrofused magnesium-calcium zirconium brick and a manufacturing method thereof; the zirconium composite high-performance electrofused magnesium-calcium zirconium brick comprises 5-10% of electrofused magnesium-calcium zirconium sand with a partical size of 5-8mm, 20-35% of electrofused magnesium-calcium zirconium sand with a partical size of 2-5mm, 20-30% of electrofused magnesium-calcium zirconium sand with a partical size of 2-0.074mm, 10-15% of electrofused magnesium-calcium zirconium sand fine powder with a partical size of 0.074mm or less, 1-5% of electrofused magnesium sand with a partical size of 5-8mm, 1-10% of electrofused magnesium sand with a partical size of 2-5mm, 1-5% of electrofused magnesium sand with a partical size of 2-0.074mm, 5-10% of electrofused magnesium sand fine powder with a partical size of 0.074mm or less, 5-10% of electrofused magnesium sand super-fine powder with a partical size of 0.037mm or less, 0.5-1.2% of calcium stabilized zirconia with a partical size of 0.5mm or less, 0.5-2% of metal calcium powder with a partical size of 0.088mm or less, 0.1-0.5% of silica fume with a partical size of 0.003mm or less and 2-5% of a binder. The method can obviously improve the physical and chemical performance indexes of the magnesium-calcium zirconium brick, anti-penetration, anti-erosion, anti-erosion and anti-spalling and other use performances of the magnesium-calcium zirconium brick can be improved, and most importantly, the magnesium-calcium zirconium brick can meet the requirements of current smelting conditions.

The invention discloses a preparation method of a zirconium dioxide short fiber and basic magnesium sulfate whisker composite enhanced magnesia-based crucible which can be sintered at the low temperature and has excellent chemical stability and thermal shock resistance. The method comprises steps as follows: (1) 15%-25% of nano aluminum sol, 0.8%-1.5% of a rheological agent and the balance of fused magnesia ceramic powder containing nano lanthanum oxide, zirconium dioxide short fiber and basic magnesium sulfate whisker are prepared in percentage by mass, deionized water is added, the mixture is subjected to ball milling and mixed uniformly, then, vacuum exhausting is performed, and ceramic slurry with the solid content of 70%-80% is prepared; (2) a crucible biscuit is prepared; (3) the dried biscuit is put in a sintering furnace to be sintered at the high temperature and then cooled with the furnace, and a magnesia-based crucible blank is obtained; (4) the magnesia-based crucible blankis subjected to vacuum impregnation treatment in aluminum sol, then, surface polishing treatment is performed, high-temperature secondary sintering is performed after drying, a product is cooled withthe furnace to the room temperature, and the magnesia-based crucible is obtained.