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123results about How to "Highly uniform dispersion" patented technology

Catalyst for producing low-carbon olefin by using synthesis gas and preparation method of catalyst

The invention relates to a catalyst for producing low-carbon olefin by using synthesis gas and a preparation method of the catalyst, and is mainly used for solving the problem of low CO conversion rate and low low-carbon olefin selectivity in reaction for preparing the low-carbon olefin by using the synthesis gas in the prior art. The catalyst consists of a composite carrier and active components, wherein the composite carrier consists of alpha-aluminium oxide and a ZSM-5 molecular sieve; the silicon-aluminium ratio of the ZSM-5 molecular sieve is 40-200; the active components are loaded on the composite carrier and comprise the following compounds with chemical formulas by atomic ratio: Fe100AaBbCcOx, A is at least one of transition metals of Cu and Mn, B is at least one of lanthanide La and Ce, and C is at least one of alkaline metals of K and Cs; the weight of the composite carrier is 20%-80% of the weight of catalyst; by weight percent of the composite carrier, the weight of alpha-aluminium oxide is 20%-99% of the weight of the composite carrier. With the adoption of the technical scheme, the problem is well solved; the catalyst can be used for industrial production of the low-carbon olefin produced by using the synthesis gas.
Owner:CHINA PETROLEUM & CHEM CORP +1

Preparation method of nano zero-valent iron loaded hydrophilic porous biochar composite material

The invention discloses a preparation method of a nano zero-valent iron loaded hydrophilic porous biochar composite material, relates to preparation methods of hydrophilic porous biochar composite materials, and aims to solve the problems that an existing matrix loading metal particles is high cost, and nano zero-valent iron is unstable and prone to agglomeration and is low in performance when being applied to heavy metal adsorption. The method includes the steps of firstly, subjecting biomass to pyrolysis and molten salt activation; secondly, preparing a hydrophilic porous biochar material; thirdly, loading the nano zero-valent iron to obtain the nano zero-valent iron loaded hydrophilic porous biochar composite material. The specific surface area of the prepared nano zero-valent iron loaded hydrophilic porous biochar composite material can reach 603.4m<2>*g<-1>. Due to the fact that corn straw is agricultural waste which is low in cost and wide in source, the cost of the preparation method is lowered by using the pyrolysis product of the corn straw as the matrix material. The prepared nano zero-valent iron loaded hydrophilic porous biochar composite material is applicable to the field of environmental pollution remediation.
Owner:NORTHEAST AGRICULTURAL UNIVERSITY

Magnesium aluminate spinel enhanced magnesia-based foamed ceramic filter and preparation method thereof

The invention discloses a magnesium aluminate spinel enhanced magnesia-based foamed ceramic filter with capability of realizing sintering at low temperature, excellent chemical stability and excellentthermal shock resistant performance, and a preparation method thereof. The preparation method comprises the following steps that (1) 10 to 20 percent of nanometer alumina sol, 0.8 to 1.5 percent of rheological agents and the balance of magnesium oxide ceramic powder containing a nanometer aluminum oxide sintering aid are proportioned; deionized water is added; ball milling and uniform mixing areperformed; then, through vacuum exhaust, ceramic slurry with the solid content being 60 to 70 percent is prepared; (2) a polyurethane foamed plastic template is soaked into the ceramic slurry; the polyurethane foamed plastic template is extruded through a roller press for removing the redundant leaching hanging slurry; then, biscuit is prepared; then, the biscuit is heated to 80 to 120 DEG C for drying; (3) the dried biscuit is put into a sintering furnace; the temperature is raised to 1400 to 1600 DEG C; high-temperature sintering is performed; cooling is performed along with the furnace to room temperature; the magnesia-based foamed ceramic filter is obtained.
Owner:NANJING UNIV OF AERONAUTICS & ASTRONAUTICS

Alkaline high-dispersion loaded Pt-based nano-catalyst and preparation and application thereof

The invention provides an alkaline high-dispersion loaded Pt-based nano-catalyst and preparation and application thereof. The catalyst is represented as Pt / MO-CN, wherein MO is one of CeO2, ZrO2, ZnOand NiO, and the mass percent of Pt is 1% to 5%; the particle size of Pt is 2nm to 4nm; and the mass ratio of CN to MO is 0.2 to 1.2. The method comprises the steps of introducing melamine into metalnitrate, which serves as a raw material, and NaBH4 which serves as a precipitant so as to obtain a metal oxide / melamine precursor, carrying out roasting treatment so as to obtain an alkaline-bit-enriched MO-CN carrier with high specific surface area, highly uniformly dispersing noble metal Pt in the surface of the MO-CN carrier through a liquid-phase reduction method by using NaBH4, , thereby obtaining the Pt / MO-CN. According to the catalyst, under the conditions of no additional alkali liquor introduction, relatively low O2 pressure and relatively low reaction temperature, 2,5-furan diformicacid can be prepared through rapid, efficient and selective catalyzed oxidation of 5-hydroxymethyl furfural, the conversion ratio and selectivity separately reach up to 92% to 98% and 89% to 99%, andthe catalyst has a relatively high application value and prospect.
Owner:BEIJING UNIV OF CHEM TECH

High-dispersion graphene heat-conduction water-based paint and preparation method thereof

The invention relates to high-dispersion graphene heat-conduction water-based paint. The high-dispersion graphene heat-conduction water-based paint is prepared from water-based paint and modifier cellulose nanocrystal/flaky graphene suspension, wherein a mass ratio of the cellulose nanocrystal/flaky grpahene suspension to the water-based paint is (1 to 7): 100, and a mass ratio of the flaky graphene in the cellulose nano crystal/flaky graphene suspension to cellulose nano crystal suspension is (0 to 2.5): 100. The preparation method comprises the following steps: (1) preparing cellulose nano crystal/flaky graphen suspension; (2) mixing the suspension and the water-based paint; (3) smearing the modified water-based paint; and (4) drying, curing, and forming a film. The high-dispersion graphene heat-conduction water-based paint has the advantages that: (1) hydroxyl on the surface of the cellulose nanocrystal sufficiently reacts with the surface active group of a graphene flake layer, sothat the graphene is highly uniformly dispersed; (2) the synergistic effect of the cellulose nanocrystal and the graphene can apparently improve the heat conductivity, impact resistance, hardness andadhesion of a coating; and (3) the high-dispersion graphene heat-conduction water-based paint is low in cost, wide in source, controllable in process and good in applicability.
Owner:NANJING FORESTRY UNIV +1

Method for preparing needle-shaped Fe-Mn-S ternary nano-material supported porous charcoal compound material

The invention provides a method for preparing a needle-shaped Fe-Mn-S ternary nano-material supported porous charcoal compound material, relates to a method for preparing porous charcoal compound materials to solve the problems that an existing Fe-Mn binary nano-material is easily agglomerated and has low adsorption capacity to heavy metals. The method comprises the following steps: 1, performingpyrolytic carbonization on a biomass material; 2, performing hydrophilic treatment on the pyrolytically carbonized porous charcoal material; 3, stirring the hydrophilic porous charcoal material in a ferric salt aqueous solution, dropwise adding a manganate solution and sulfide solution for stirring, adding a weak alkaline solution for stirring, performing hydrothermal reaction, and drying to obtain the ternary nano-material supported porous charcoal compound material. According to the method, the interaction among molecules of a ternary nano-material is reduced by supporting the Fe-Mn-S ternary nano-material to the surface of the charcoal material, nano-particle agglomeration is reduced, and the dispersibility of ternary nano-particles is improved. The method is applied to the field of charcoal compound materials.
Owner:NORTHEAST AGRICULTURAL UNIVERSITY

High-limestone-flour-adulterate-amount composite enhanced grinding aid for cement and preparation method of high-limestone flour-adulterate amount composite enhanced grinding aid

The invention relates to a high-limestone-flour-adulterate-amount composite enhanced grinding aid for cement and a preparation method of the high-limestone-flour-adulterate-amount composite enhanced grinding aid. The preparation method comprises the following steps that 1, materials including 18%-25% of triethanolamine, 8%-15% of triisopropanolamine, 20%-28% of ethanediol, 8%-12% of molasses, 4%-8% of polycarboxylate superplasticizer, 6%-10% of sodium sulfate, 5%-8% of glacial acetic acid and 2%-24% of water are taken; 2, the water is poured into an agitator kettle, and sodium sulfate is added to be stirred till sodium sulfate is completely dissolved; 3, glacial acetic acid is added to be completely dissolved, triethanolamine, triisopropanolamine, ethanediol, molasses and polycarboxylate superplasticizer are sequentially added after glacial acetic acid is dissolved, stirring continues to be carried out for 20-30 minutes, and the high-limestone flour-adulterate amount composite enhanced grinding aid is obtained. The high-limestone-flour-adulterate-amount composite enhanced grinding aid has the advantages that cement particles are prevented from clustering, and the cement particles are kept in a high homodisperse state; the strength of an interfacial transition zone is increased, and the strength of the cement is further increased; the grinding aiding efficiency of the grinding aid is improved.
Owner:WUHAN UNIV OF TECH

Functional polyester production method and production system and functional polyester fiber

The invention belongs to the technical field of polymer material synthesis, and particularly relates to a functional polyester production system. The functional polyester production system comprises apolyester main production system, and further comprises a functional powder slurry concentrate preparation system, the polyester main production system comprises an esterification system, a pre-polycondensation system and a final polycondensation system which are connected in sequence, the functional powder slurry concentrate preparation system comprises an online adding device which is connectedwith the esterification system or a part between the esterification system and the pre-polycondensation system. The functional powder slurry concentrate preparation system is introduced in the polyester main production system, and can continuously prepare a functional powder slurry concentrate with low hydroxyl value and low pressure filtration value, and the prepared functional powder slurry concentrate and a polyester oligomer are uniformly mixed for polycondensation reaction to obtain functional polyester with uniformly dispersed functional powder. The invention further relates to a functional polyester production method.
Owner:CHINESE TEXTILE ACAD +1

Carbon resistance superfine nano wolfram carbide material as well as preparation method and application thereof

The invention discloses a carbon resistance superfine nano wolfram carbide (WC) material as well as a preparation method and application thereof. The preparation method of the carbon resistance superfine nano WC material comprises the following steps: (1) adding a deionized water solution of a wolfram source in a solution prepared from ethanol, stronger ammonia water and a surfactant, wherein the wolfram source is ammonium metatungstate, sodium tungstate or tungsten chloride, the surfactant is sodium dodecyl benzene sulfonate, hexadecyl trimethyl ammonium bromide or P123, stirring the solution uniformly, adding resorcinol to the solution, stirring uniformly and then adding formaldehyde, and stirring for 8-28 hours at the room temperature to obtain the mixed solution; (2) performing a hydrothermal reaction on the mixed solution, and drying the solution to obtain a mixed polymer; (3) performing high-temperature carbonization on the mixed polymer in a CO atmosphere to obtain the carbon resistance superfine nano WC material. The WC material can enable the WC particles to keep stable in the high temperature process without secondary agglomeration; the WC material can be taken as an electrocatalyst to be applied to an electrocatalysis nitroreduction reaction, or can also be taken as a carrier to prepare a platinum-carried catalyst, and the prepared platinum-carried catalyst can be applied to anode catalysis of a methanol fuel cell.
Owner:ZHEJIANG UNIV OF TECH +1

Method for continuously producing polyester functional master batch and polyester functional master batch

The invention belongs to the technical field of polymer material synthesis, and relates to a method for continuously producing a polyester functional master batch and the polyester functional master batch, the method comprises the following steps: using aromatic binary acid, aliphatic dihydric alcohol and a catalyst to prepare an aromatic binary acid aliphatic dihydric alcohol ester oligomer; mixing functional powder and aliphatic dihydric alcohol to obtain functional slurry; and adding the functional slurry into the aromatic binary acid aliphatic dihydric alcohol ester oligomer on line, uniformly mixing, carrying out melt polycondensation reaction, and carrying out pelletizing forming, crystallizing and solid-phase polycondensation reaction to obtain polyester functional master batch slices. According to the invention, the functional slurry online addition procedure, the melt polycondensation reaction procedure, the pelletizing forming and crystallizing procedures and the solid-phasepolycondensation reaction procedure are introduced, the continuous production of the polyester functional master batch and the accurate addition and height dispersion of the functional powder are realized, and the structure uniformity of the polyester functional master batch is improved.
Owner:CHINESE TEXTILE ACAD +1

Method for preparing desulfurizing agent by carrying out thermal activation on red mud and active carbon

InactiveCN106881019AEasy to get from a wide range of sourcesThe source is easy to getGas treatmentDispersed particle separationMass ratioRed mud
The invention discloses a method for preparing a desulfurizing agent by carrying out thermal activation on red mud and active carbon and belongs to the field of coal desulfurization. The method comprises the specific steps: step a: sieving the red mud and the active carbon with a 300-mesh sieve respectively; drying at 105 DEG C until the weight is constant; step b: mixing the red mud and the active carbon according to the mass ratio ranging from (1 to 10) to (1 to 30); step c: activating a mixture in the step b in a muffle furnace at 700 DEG C to 1100 DEG C for 10min to 30min; after finishing the thermal activation, naturally cooling to room temperature under a sealed condition. The method disclosed by the invention has the advantages that the waste dreg red mud produced in a production process of aluminum oxide is prepared into the desulfurizing agent; a preparation process is simple and the activation time is short; the wet-method desulfurizing efficiency can reach 90 percent; the desulfurizing rate can be maintained to be 87 percent when the desulfurizing agent is continuously used under a low pH (Potential of Hydrogen) condition; the dosage of the desulfurizing agent is reduced so that the desulfurizing agent is economical and feasible.
Owner:CHINA UNIV OF MINING & TECH

Titanium dioxide/graphene composite nanometer photocatalyst, method for preparing same and application of titanium dioxide/graphene composite nanometer photocatalyst

The invention discloses a titanium dioxide/graphene composite nanometer photocatalyst, a method for preparing the same and application of the titanium dioxide/graphene composite nanometer photocatalyst. The titanium dioxide/graphene composite nanometer photocatalyst, the method and the application have the advantages that solvothermal processes are adopted, alcohol is used as a solvent, hexamethylene tetramine is decomposed under solvothermal conditions to generate alkaline and reduction species, accordingly, the titanium dioxide/graphene composite nanometer photocatalyst can be prepared at one step, and the problems of secondary stacking of graphene lamellar structures and aggregation of TiO2 nanometer particles in procedures for preparing titanium dioxide and graphene composite materials by the aid of fractional-step methods can be solved; the titanium dioxide/graphene composite nanometer photocatalyst is high in dispersion, has a large specific surface area and is extremely high in photocatalytic degradation capacity for nitrogen-containing organic dyestuff in printing and dyeing wastewater, and accordingly the titanium dioxide/graphene composite nanometer photocatalyst and the method have broad application prospects.
Owner:北京清淞泉生物科技有限公司
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