The invention discloses a method for preparing high-melting-point
metal powder through multistage depth reduction, and belongs to the technical field of
powder preparing. The method comprises the steps that dried high-melting-point metallic
oxide powder and
magnesium powder are mixed and then subject to the self-propagating reaction, and high-melting-point
metal Me is one or several of W, Mo, Ta, Nb, V, Zr, Hf or Re; intermediate products are placed in a seal reaction kettle,
hydrochloric acid serves as a leaching agent to carry out leaching, and low-valence
oxide MexO precursor of low-valence high-melting-point
metal is obtained; the precursor is evenly mixed with
calcium powder to be pressed, a mixture is placed in a vacuum reduction furnace, heating is carried out to enable the temperature to rise to 700 DEG C to 1200 DEG C, deep reduction is carried out for 1 h to 6 h,
hydrochloric acid serves as the leaching agent to carry out leaching on a deep reduction product, and through treatment, high-melting-point
metal powder is obtained. The method is low in
raw material cost, easy to operate, and low in requirement for process and instrument equipment, the foundation is laid for industrial production, and the high-melting-point
metal powder has the beneficial effects of being high in purity, controllable in
granularity distribution, high in powder activity and the like.