The application belongs to the technical field of
fuel cells, and specifically discloses a high-temperature PEMFC ordered catalytic layer structure
electrode and a preparation method, which comprises the following steps: S1, preparation of a
gas diffusion layer, to obtain a
gas diffusion layer with a hydrophobic agent
mass fraction of 15-25%; S2, preparation of an ordered catalytic layer: placing the
gas diffusion layer obtained in S1 and a reaction solution in a reaction container to perform a
hydrothermal reaction, performing cleaning,
drying and
calcination treatment after the reaction is completed, to obtain a catalyst carrier array, loading Pt on the catalyst carrier array by using a
formic acid reduction method, and then
coating a conductive substance, to obtain an ordered catalytic layer structure
electrode. The high-temperature PEMFC ordered catalytic layer structure
electrode and the preparation method have the advantages of mild preparation conditions, a simple process, low cost, a more stable structure and excellent durability of the electrode under high-temperature and
phosphoric acid conditions, and significant improvement of battery performance and service life.