The invention discloses a separation tower resin interface intelligent monitoring system and a high-tower method resin analysis method. The system comprises a separation tower, an upper window, a middle window, a lower window, an anion resin exit door, a cation resin exit door, an upper window camera, a middle window camera, a lower window camera, an optical fiber cable, an industrial switch, a monitoring computer, a human-computer interface, a bus converter, a signal converter, a PLC/DCS controller, an electrical switching controller and a resin analysis algorithm program. According to the separation tower resin interface intelligent monitoring system and the high-tower method resin analysis method, an intelligent visual technology is adopted, accurate control over output of anion resin and cation resin in the resin separation tower in a condensate polishing treatment regeneration system of an nuclear power conventional island and a thermal power generating unit water island is achieved by means of a computer image identification algorithm, and correct quantitative analysis is conducted on loss, generated in the running and transfer conveying processes, of the cation and resin and the anion resin and needed supplement dosage.