The invention provides a novel method for preparing an A-type
molecular sieve membrane, which adopts preparation of the
molecular sieve membrane in a flow
system. The method comprises the following steps: a
silicon source, an aluminum source, an alkali source and deionized water are prepared into precursor
sol of A-type
molecular sieve according to certain proportion first; a vector membrane tube which is precoated with A-type molecular
sieve crystal seeds is fixed inside a synthesis reactor; the molecular
sieve precursor
sol which is heated to a given temperature is conveyed into the synthesis reactor through a
slurry pump, and the precursor
sol is driven to flow and circulate on the surface of an outer membrane of the vector membrane tube; and the A-type molecular
sieve membrane can be obtained after flowing, circulating and
crystallization for a
definite time at the given temperature. The preparation method provided by the invention has the advantages that the preparation method can basically solve the problem of
concentration gradient during the synthetic process of he molecular sieve, is favorable to the preparation of the uniform, continuous and compact molecular sieve membrane with superior separation performance, and is particularly suitable for preparing the molecular sieve membrane for industrial application.