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63results about How to "Increase the effective surface" patented technology

Improved liquid distributor

The invention discloses an improved liquid distributor. The liquid distributor comprises a distribution plate and a liquid inlet header pipe; the middle of the distribution plate is uniformly provided with shunting holes, and the upper part of the distribution plate is uniformly provided with multiple partitions; each adjacent partitions are connected through a separation plate, and liquid accumulation grooves are formed among the partitions and the separation plates; the liquid inlet header pipe is placed above the liquid accumulation grooves, the bottom of the liquid inlet header pipe is communicated through the liquid accumulation grooves, the middle of the liquid inlet header pipe is provided with a round hole, and two ends of the liquid inlet header pipe are each provided with a liquid inlet hole. Uniform initial distribution or redistribution of a liquid is carried out at a certain height, so that the effective surface for mass transfer and heat transfer is increased, the interphase contact is improved, and thus the efficiency of a tower is improved; the liquid accumulation grooves are formed among the partitions and the separation plates, space in each grooves is large, and the fluidity is good; and then the liquid is shunted out through the shunting holes, and the distribution is uniform.
Owner:MINGSHENG CHEM MACHINERY NANTONG

Method for preparing dihydromyrcenol through reaction distillation continuity

The invention relates to a method for preparing dihydromyrcenol through reaction distillation continuity. Corrugated gauze filling materials and solid acid catalysts are filled in a reaction distillation tower, raw materials of dihydromyrcene, water and solvents are respectively preheated to 80 to 120 DEG C, 85 to 95 DEG C and 70 to 90 DEG C to be respectively fed from the upper part, the middle part and the lower part of a reaction section of the reaction distillation tower according to the flow rate ratio of (1-3): (1-3). The tower kettle temperature is controlled to be 105 to 120 DEG C, and the tower top condensing temperature is controlled to be 50 to 70 DEG C. An oil phase and a water phase are separated out from condensed liquid, partial oil phase reaches the tower top to flow back, and the water phase and the rest oil phase respectively return a raw material tank to be cyclically utilized. According to the method, the reaction and the distillation are simultaneously carried out, heat released by the reaction can be effectively utilized for heating materials, and a heat load of a tower kettle is reduced. The corrugated gauze filling materials in the reaction distillation tower and a tubular liquid distributor are favorable for improving the effective surfaces for mass transfer and heat transfer and improving the inter phase contact, dihydromyrcenol products with the purity being 95 percent are obtained from the tower bottom, and the reaction efficiency and the dihydromyrcenol conversion rate are higher.
Owner:淮安市产品质量监督检验所
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