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Method for removing water from an aqueous fluid mixture

A method permits concentration of a water-miscible organic liquid in a mixture of such liquid and water, with recovery of a desired concentrate of the water-miscible organic liquid and water, and a relatively clean water containing only a very low contest of the water-miscible organic liquid which enables disposal of the water in sewage systems, the method thus enhancing the ability to satisfy environmental concerns; the method has particular application to the recovery of a reusable glycol / water mixture from diluted spent aircraft deicer fluid (ADF). The diluted spent ADF is heated in a plate heat exchanger with steam to form a hot frothing mass of liquid and steam which is delivered to a cyclone concentrator, the hot frothing mass in the plate heat exchanger and the cyclone concentrator are maintained at a first pressure and a steam phase including steam bubbles in the hot frothing mass is efficiently separated from and withdrawn from a hot liquid phase which represents a more concentrated glycol / water mixture. The steam withdrawn from the hot frothing mass is compressed to a second pressure higher than the first pressure and cycled back to provide the steam input of the plate heat exchanger. After start-up the operation proceeds, with maintenance of the pressure differential, exploiting the heat of the compressed steam with no requirement for external heating. The method may be applied to other aqueous fluid mixtures.
Owner:INLAND TECH HLDG INC

Method and device to fill receiving containers

A receiving container is filled with a predetermined target mass mz of a free-flowing substance from a reservoir with the help of a dosage-dispensing device that dispenses measured doses of the substance. The device has a valve for variably setting the mass flow {dot over (m)} from the reservoir into the receiving container. The device is also able to determine the time t that has elapsed since the beginning of the fill cycle, the mass m of the substance present in the receiving container, and a unit for controlling the valve. The controller unit includes estimating and correction modules. At least once during the fill cycle, the estimating module performs an estimate of the mass {tilde over (m)}(t, t2) that is expected to be present in the receiving container at the end of the fill cycle at the time t2. This estimate is based on the assumptions that from the time t onward the valve is being closed according to a predefined closing-down profile and the fill cycle is completed at the time t2. The correction module compares the mass {tilde over (m)}(t, t2) estimated at the time t to the target mass mz. If the estimated mass {tilde over (m)}(t, t2) is smaller than the target mass mz, the valve is controlled so that the aperture associated with the mass flow {dot over (m)} that exists at the time t will be maintained longer by a differential time segment Δt, and / or the mass flow {dot over (m)} at the time t is increased.
Owner:METTLER TOLEDO GMBH
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