The invention relates to the field of the
chemical industry, in particular to a method for preparing N-methylol group-D,L-
calcium methionine microelement chelates. The method is
environmentally friendly and low in cost. According to the method,
saponification liquid produced in the production process of D,L-
methionine serves as production raw materials and reacts with
trace metal element
calcium salt to obtain D,L-
methionine microelement chelates, the obtained D,L-methionine microelement chelates react with
formaldehyde in a water medium, filtering, washing in cold water,
drying and crushing are carried out after the reaction, and the powdered N-methylol group-D,L-
calcium methionine microelement chelates are obtained. According to the method, high-purity D,L-methionine is needless, the N-methylol group-D,L-calcium methionine microelement chelates are directly prepared through the
saponification liquid, and production cost is reduced. According to the method, the high-purity N-methylol group-D,L-calcium methionine microelement chelates are prepared, stability is high, animals can easily digest and absorb the N-methylol group-D,L-calcium methionine microelement chelates, the N-methylol group-D,L-calcium methionine microelement chelates can serve as feed additions, obtained filter liquor can be recycled, and the method is
environmentally friendly.