The invention relates to a preparation method of a 3D hierarchical-structure flexible carbon fabric-loaded MOF-LDH 
hybrid array 
supercapacitor electrode material, in particular to a novel method for preparing the 3D hierarchical-structure flexible carbon fabric-loaded MOF-LDH 
hybrid array 
supercapacitor electrode material according to the steps of carbonizing 
cotton cloth to prepare a carbon fabric, performing 
hydrothermal reaction on 
cobalt nitrate and 
urea aqueous solution to prepare a 
nanowire array, preparing an MOF array by taking the 
nanowire array as a sacrifice template, performing ionexchange on the obtained product and performing 
etching. The method comprises the following steps of firstly, carbonizing the 
cotton cloth to prepare the carbon fabric, activating the carbon fabric,and carbonizing the 
cotton cloth to the carbon fabric at 700-900 DEG C; secondly, placing the obtained carbon fabric in a 
mixed solution of 
cobalt nitrate, 
urea and deionized water, performing 
hydrothermal reaction for 4-12 hours at 90-100 DEG C, taking out and cleaning the product, and 
drying the product; thirdly, placing the obtained product in the previous step in an 
aqueous solution of 2-methylimidazole for reaction for 1 hour at a normal temperature, and performing cleaning and 
drying; and finally, placing the obtained product in an 
ethanol solution of 
nickel nitrate for reaction for 1 hour, and performing cleaning and 
drying.