The invention relates to a method and a device for concentrating and enriching stable isotopes 2H, 18O and 13C. The method comprises the steps of: by taking compounds respectively containing stable isotopes 2H, 18O and 13C as materials, carrying out purification treatment, adding to a
heavy isotope concentration
tower group formed by a plurality stages of gas-liquid
mass transfer towers connected in series; continuously and partially vaporizing and partially condensing in the gas-liquid
mass transfer towers connected in series by weak
vapor pressure difference between light and heavy
isotopes of hydrogen,
oxygen, and carbon elements, and gradually concentrating and purifying corresponding
heavy isotope. Each
tower disclosed by the invention adopts different operation pressures and
coupling utilization of heat between the towers; over 30-40% of
energy consumption can be saved; a
composite structure mass transfer component composed of a liquid collecting distributer, a Dixon
mass transfer component, a corrugated
mass transfer component and the like is adopted inside the
tower; the device is easy to amplify; the device of producing heavy 2H, 18O or 13C
isotope at a large scale just needs to be connected with 2-8 gas-liquid
mass transfer towers in series; over 50% of investment is saved in comparison with the same scale of device, and the towers adopt a single tandem
cascade technology; and the method is simple in flow and easy to control and operate.