The invention discloses a method for preparing a
quantum dot of a transitional
metal chalcogenide compound and belongs to the field of preparing functional
nanomaterials by colloidal chemical methods. The method disclosed by the invention comprises the following steps: mixing a
metal carbonyl compound and
trioctylphosphine oxide, heating and dissolving the mixture as a
metal source precusor, by taking
octadecene as a reaction
solvent, heating the mixture under
inert gas protection to
reaction temperature, and preparing a metal source
reaction system; by taking
organic phosphorus as a coorinating
solvent, preparing non-metal source
sulfur powder,
selenium powder or
tellurium powder into a precusor solution; injecting the non-metal source solution into the metal source
reaction system under
inert gas protection and maintaining the
reaction temperature and carrying out a heating reaction; and carrying out high speed
centrifugal separation, and adding a
mixed solution of n-
butylamine / n-
hexane into the obtained
solid product to obtain a
quantum dot material of the transitional metal
chalcogenide compound in a collide dispersing state. The preparation method for the
quantum dot material of the transitional metal
chalcogenide compound disclosed by the invention is good in universality, fast in
reaction speed, high in reaction yield, simple to operate, mild in reaction condition and easy for large-scaled production.