The invention discloses a
Phosphor / TiO2 photocatalyst which has high
thermal stability and the corresponding preparation method. The photocatalyst can be prepared though a method comprising the following steps: 1) a solution which contains the precursor of inorganic
titanium salt and phosphorated compound is prepared, then a precipitant is added into the solution which contains the precursor of inorganic
titanium salt and phosphorated compound until the pH value reaches to 4-8, and a
solid is obtained by aging and filtering; 2) the
solid obtained form the step 1) is dried and calcined to get the
phosphor / TiO2 photocatalyst; the precursor of inorganic
titanium salt is the
random combination of one or more of TiCl4, TiCl 3, TiOCl 2, Ti(SO4)2 and TiOSO4; the phosphorated compound is phosphorated oxy acid and / or phosphorated oxysalt. The photocatalyst of the invention has no polymorphic transformation after being calcined under high temperature, maintains high photocatalitic activity under
ultraviolet and visible light, and can be used in the degeneration of the
pollutant in
industrial effluent and the reparation of wall paint or wall
brick paint film which have antibiotic and air purifying effects.