The application discloses an acid
pickling corrosion inhibitor prepared based on bamboo pulp
papermaking black liquor, and a preparation method and application thereof, and relates to the technical field of acid
pickling corrosion inhibitors. The method comprises the following steps: (1) adding concentrated
sulfuric acid into the bamboo pulp
papermaking black liquor, adjusting the pH value of the solution to 1-3, and then fully reacting, standing and
settling, and separating to obtain a precipitate A and a filtrate A; the precipitate A is washed and dried to obtain
lignin; (2) the filtrate A is concentrated through multi-effect vacuum reduced pressure
evaporation to obtain a precipitate B; (3) the precipitate B is extracted through
sewage ethanol extraction, suction
filtration and washing to obtain an
ethanol extraction liquid and a precipitate C; the
ethanol extraction liquid is distilled through reduced pressure
distillation to obtain an ethanol extraction liquid; the precipitate C is recrystallized, and after removing
solid inorganic salts, the precipitate C is distilled through reduced pressure
distillation to obtain a
distillation liquid; the ethanol extraction liquid and the distillation liquid are mixed, and then evaporated through reduced pressure
evaporation and dried to obtain the acid
pickling corrosion inhibitor.