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High temperature high pressure acoustic emission electrochemistry simulation experiment apparatus capable of loading stress

The invention provides a high temperature high pressure acoustic emission electrochemistry simulation experiment apparatus capable of loading stress. The apparatus comprises: a pressure kettle, wherein the pressure kettle is provided with an inner cavity, and a specimen is arranged inside the inner cavity; stretching test systems installed on both ends of the specimen, wherein the tension test system stretches the specimen, tests and obtains tension and a strain signal of the specimen; a solution circulation inflation system connected with the inner cavity of the pressure kettle and provided for providing a solution required by an experiment for the pressure kettle; acoustic emission probes arranged on both ends of the specimen and provided for testing an acoustic signal of the specimen; an electrochemistry test system connected with the specimen and the pressure kettle, and provided for applying polarization current on the specimen to carry out polarization, testing and obtaining an electrochemistry signal; and a data collector for collecting the simultaneously measured strain signal, the electrochemistry signal and the acoustic emission signal. With the present invention, controllable pressurizing, controllable heating and controllable inflation can be performed, and an actual working condition of the on-site material is well simulated.
Owner:BC P INC CHINA NAT PETROLEUM CORP +1

Simulation and evaluation method and system for under-salt dolomite water-rock reaction

The invention provides a simulation and evaluation method and system for an under-salt dolomite water-rock reaction. The method comprises analyzing stratum water of a research area; stratum water classification is carried out by using a Sulin method; formulating experimental fluids, preparation of dolomite core sample, dolomite water rock reaction test is performed; the dolomite water-rock reaction is judged to reach chemical equilibrium; the method comprises the following steps: determining the fluid flow rate of the dolomite water rock reaction, carrying out the under-salt dolomite water rock reaction by using the prepared experimental fluid and a dolomite rock core sample, analyzing and calculating the changes of mineral components, corrosion and precipitation, and quantitatively evaluating the influence of the under-salt dolomite formation water on the corrosion and precipitation of the dolomite. According to the method, the quantitative evaluation of the reaction between the dolomite and the corresponding formation water under the geological background of the subsalt dolomite reservoir can be realized; the specific influence of stratum water attributes in the dolomite water-rock reaction process can be analyzed, control factors beneficial to formation and storage of under-salt dolomite pores are defined, and an analysis basis is provided for large-scale and efficient under-salt dolomite reservoir distribution and prediction.
Owner:PETROCHINA CO LTD

Content determination method for scutellarin and scutellarein in sculellaria barbata medicinal material and formula granule of sculellaria barbata medicinal material

The invention relates to a content determination method for scutellarin and scutellarein in sculellaria barbata medicinal material and formula granule of sculellaria barbata medicinal material. The content determination method is characterized in that common isocratic elution is adopted, acetonitrile-methyl alcohol-0.1 percent phosphoric acid of which the volume ratio is 12.5:(15 to 16.2):(71.3 to 72.5) is taken as a mobile phase, and the contents of the scutellarin and the scutellarein in the sculellaria barbata medicinal material and the formula granule of the sculellaria barbata medicinal material are simultaneously determined at a wavelength of 340+/-2nm. The method is simple, convenient, fast, and easy to popularize and master; the separations of wave crests on three different chromatographic columns are good. Compared with a method of recording under a sculellaria barbata medicinal material item of the first part of the pharmacopeia, the prominent improvement is that a sample treatment process is simplified, the time and cost are saved, the determination is advanced from single component determination of the scutellarin to the simultaneous determination of the two components, the quality controllability is improved, and the defects that impurity peaks exist and the content results are inaccurate are overcome.
Owner:HEBEI UNIV OF CHINESE MEDICINE +1
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