The application belongs to the technical field of
sodium ion batteries, and discloses a preparation method of a double-site co-doped
sodium ion battery positive
electrode material. The method comprises the following steps: (1) according to the
molar ratio of each
metal element in the
chemical formula of the target product, corresponding
metal salts are weighed and dissolved in an
ethanol solution to obtain a
metal salt solution;
oxalic acid is dissolved in an
ethanol solution to obtain an
oxalic acid solution; (2) under ultrasonic conditions, the metal
salt solution is added dropwise into the
oxalic acid solution, and stirring is continuously performed; after the metal
salt solution is completely added dropwise, ultrasonic treatment is continuously performed; the suspension treated by ultrasonic treatment is placed in an oven for
drying, and the
powder obtained by
drying is ground; (3) the ground
powder is placed in a
corundum box and then placed in a
tube furnace for
sintering; first, heating is performed to 500 DEG C for heat preservation; after cooling, the tablet is taken out, the pressed tablet is continuously placed in the
tube furnace, heating is performed to 900 DEG C for heat preservation, after cooling, the tablet is taken out and ground, and the target product is obtained.