The utility model discloses a
distillation and purification device for
triethyl orthoformate. Comprising a bottom plate, a bearing block fixedly connected to the upper end of the bottom plate, a
distillation still fixedly connected to the upper end of the bearing block, a groove body formed in the
peripheral wall of the
distillation still in a penetrating mode, a sliding door hinged to the inner wall of the groove body, a feeding
assembly arranged on the
peripheral wall of the distillation still, a steam output
assembly arranged at the upper end of the distillation still and a discharging
assembly arranged at the lower end of the distillation still. The first bearing ring is fixedly connected to the middle part of the inner wall of the distillation kettle; the movable ring is placed at the upper end of the first bearing ring; the fixed cylinder is arranged on the inner wall of the movable ring in a sliding manner; the separation cylinder is fixedly connected to the lower end of the movable ring; the guide cylinder is fixedly connected to the upper end of the fixed cylinder; the air guide assembly is arranged at the upper part of the inner wall of the distillation kettle. The utility model has the advantages that the internal
airflow can be actively guided and adjusted, the
mass and
heat transfer efficiency is high, and the cleaning and maintenance are convenient.