The invention discloses a production process of high-purity
antimony powder, and relates to the technical field of high-purity
antimony powder production. The production process of the high-purity
antimony powder comprises the following steps that S1, presetting is conducted, specifically, a high-purity antimony powder production device is prepared in advance; s2, feeding, wherein crude antimony is fed into a high-purity antimony powder production device; and S3, purification is conducted, specifically, after the step S2, the fed crude antimony is purified through a high-purity antimony powder production device, and the purified high-purity antimony powder is collected. According to the production process of the high-purity antimony powder, under the negative pressure state, partition heating and heat preservation are conducted on the
crucible body,
arsenic and other impurities with the low
boiling point can be volatilized firstly, condensed and collected, then the temperature of the bottom of the
crucible continues to rise, antimony is volatilized, condensed and smashed, and the high-purity antimony powder is formed and collected; according to the high-purity antimony powder production device, the partition temperature can be conveniently controlled during partition heating, the annular cover and the conical
titanium plate can be cooled, the condensation efficiency is improved, and then the production efficiency and quality of high-purity antimony powder are improved.